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41. 发明授权

US07662272B2 Crystalline wax 有权
标题翻译：结晶蜡
公开(公告)号：US07662272B2
公开(公告)日：2010-02-16
申请号：US11273895
申请日：2005-11-14
申请人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Timothy L. Lincoln , Kevin F. Marcell , Louis V. Isganitis
发明人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Timothy L. Lincoln , Kevin F. Marcell , Louis V. Isganitis
IPC分类号： C10G73/36
CPC分类号： G03G9/08782 , C08F6/04 , C08L23/04 , C08L25/14 , C08L91/06 , C08L2666/02
摘要： Embodiments include a distilled wax having a crystallinity of from about 55 to about 100 percent, wherein the degree of crystallinity is calculated using the following formulas: [Heat of enthalpy (Hm) J/g/294 J/g]×100=degree of crystallinity (Xc); [Heat of recrystallization (Hrc) J/g/294 J/g]×100=degree of crystallinity (Xc); and Sc/(Sc+Sa)]×100%, wherein Sc is a diffraction peak area of a crystalline component of the wax and the Sa is a diffraction peak area of an amorphous component of the wax; and wherein the Mp, Mn and Mw of the wax are all within the range of from about 500 to about 800, and wherein the wax has a polydispersity of from about 1 to about 1.05.
摘要翻译：实施方案包括结晶度为约55至约100％的蒸馏蜡，其中结晶度用下列公式计算：[热焓（Hm）J / g / 294J / g]×100 =结晶度（Xc）; [重结晶热（Hrc）J / g / 294J / g] x100 =结晶度（Xc）; 和Sc /（Sc + Sa）]×100％，其中Sc是蜡的结晶成分的衍射峰面积，Sa是蜡的无定形成分的衍射峰面积; 并且其中所述蜡的Mp，Mn和Mw均在约500至约800的范围内，并且其中所述蜡具有约1至约1.05的多分散性。

42. 发明授权

US5747215A Toner compositions and processes 失效
标题翻译：调色剂组成和工艺
公开(公告)号：US5747215A
公开(公告)日：1998-05-05
申请号：US841300
申请日：1997-04-29
申请人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
发明人： Beng S. Ong , Walter Mychajlowskijj , Grazyna E. Kmiecik-Lawrynowicz , Raj D. Patel , David J. Sanders , Stephan V. Drappel
IPC分类号： G03G9/08 , G03G9/087 , G03G9/09 , G03G9/097
CPC分类号： G03G9/08793 , G03G9/0804 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08731 , G03G9/08733
摘要： A process for the preparation of toner comprising (i) blending (a) a colorant dispersion containing a first ionic surfactant and an optional charge control agent with (b) a latex blend comprised of linear polymer and crosslinked polymer particles, optional nonionic surfactant and a second ionic surfactant with a charge polarity opposite to that of said first ionic surfactant in said colorant dispersion; (ii) heating the resulting mixture at about below the glass transition temperature (Tg) of the linear latex polymer to form toner sized aggregates; and (iii) subsequently heating said aggregate suspension about above the Tg of the linear latex polymer to effect fusion or coalescence of said aggregates, and wherein said linear polymer is of an M.sub.w of from about 20,000 to about 40,000.
摘要翻译：一种制备调色剂的方法，包括（i）将（a）含有第一离子型表面活性剂和任选的电荷控制剂的着色剂分散体与（b）由直链聚合物和交联聚合物颗粒组成的胶乳共混物，任选的非离子表面活性剂和第二离子表面活性剂，其电荷极性与所述着色剂分散体中所述第一离子表面活性剂的极性相反; （ii）将所得混合物加热至低于线性胶乳聚合物的玻璃化转变温度（Tg），以形成调色剂尺寸的聚集体; 和（iii）随后将所述聚集体悬浮液加热至高于线性胶乳聚合物的Tg以实现所述聚集体的熔融或聚结，并且其中所述线性聚合物的Mw为约20,000至约40,000。

43. 发明授权

US07553596B2 Toner having crystalline wax 有权
标题翻译：具有结晶蜡的调色剂
公开(公告)号：US07553596B2
公开(公告)日：2009-06-30
申请号：US11273748
申请日：2005-11-14
申请人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Louis V. Isganitis , Timothy L. Lincoln , Kevin F. Marcell
发明人： Raj D. Patel , David J. Sanders , T Hwee Ng , Stephan V. Drappel , Sandra J. Gardner , Sonja Hadzidedic , Louis V. Isganitis , Timothy L. Lincoln , Kevin F. Marcell
IPC分类号： G03G9/08
CPC分类号： G03G9/08782 , G03G9/0806 , G03G9/08704 , G03G9/08708 , G03G9/08711 , G03G9/08728 , G03G9/08733 , G03G9/08795 , G03G9/08797
摘要： Embodiments include a toner with a distilled wax having a crystallinity of from about 55 to about 100 percent, wherein the degree of crystallinity is calculated using the following formulas: [Heat of enthalpy (Hm) J/g/294 J/g]×100=degree of crystallinity (Xc); [Heat of recrystallization (Hrc) J/g/294 J/g]×100=degree of crystallinity (Xc); and Sc/(Sc+Sa)]×100%, wherein Sc is a diffraction peak area of a crystalline component of the wax and the Sa is a diffraction peak area of an amorphous component of the wax; and wherein the Mp, Mn and Mw of the wax are all within the range of from about 500 to about 800, and wherein the wax has a polydispersity of from about 1 to about 1.05.
摘要翻译：实施方案包括具有结晶度为约55至约100％的蒸馏蜡的调色剂，其中结晶度用下式计算：[热焓（Hm）J / g / 294J / g] x100 = 结晶度（Xc）; [重结晶热（Hrc）J / g / 294J / g] x100 =结晶度（Xc）; 和Sc /（Sc + Sa）]×100％，其中Sc是蜡的结晶成分的衍射峰面积，Sa是蜡的无定形成分的衍射峰面积; 并且其中所述蜡的Mp，Mn和Mw均在约500至约800的范围内，并且其中所述蜡具有约1至约1.05的多分散性。

44. 发明授权

US06899987B2 Toner processes 失效
标题翻译：墨粉处理
公开(公告)号：US06899987B2
公开(公告)日：2005-05-31
申请号：US10393635
申请日：2003-03-20
申请人： Daryl Vanbesien , Raj D. Patel , Michael A. Hopper , Stephan V. Drappel
发明人： Daryl Vanbesien , Raj D. Patel , Michael A. Hopper , Stephan V. Drappel
IPC分类号： G03G9/08 , C03J3/215
CPC分类号： G03G9/0804 , G03G9/0806
摘要： A process for the preparation of toner by, for example, mixing a latex with a colorant mixture comprised of colorant, an ionic surfactant, and a polytetrafluoroethylene; adding a coagulant; heating the resulting mixture below about the glass transition temperature (Tg) of the latex resin; adding a stabilizer; heating above about the Tg of the latex resin; and isolating the toner.
摘要翻译：通过例如将胶乳与由着色剂，离子表面活性剂和聚四氟乙烯组成的着色剂混合物混合来制备调色剂的方法; 加入凝结剂; 将所得混合物加热至胶乳树脂的玻璃化转变温度（Tg）以下; 添加稳定剂; 加热高于胶乳树脂的Tg; 并分离调色剂。

45. 发明授权

US5482812A Wax Containing toner aggregation processes 失效
标题翻译：蜡含有调色剂聚集工艺
公开(公告)号：US5482812A
公开(公告)日：1996-01-09
申请号：US344060
申请日：1994-11-23
申请人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
发明人： Michael A. Hopper , Raj D. Patel , Grazyna E. Kmiecik-Lawrynowicz , Stephan V. Drappel , Paul J. Gerroir
IPC分类号： G03G9/08 , G03G9/087
CPC分类号： G03G9/0804 , G03G9/0815
摘要： A process for the preparation of toner compositions or toner particles comprising:(i) providing an aqueous pigment dispersion comprised of a pigment, an ionic surfactant, and optionally a charge control agent;(ii) providing a wax dispersion comprised of wax, a dispersant comprised of nonionic surfactant, ionic surfactant or mixtures thereof;(iii) shearing a mixture of the wax dispersion and the pigment dispersion with a latex or emulsion blend comprised of resin, a counterionic surfactant with a charge polarity of opposite sign to that of said ionic surfactant and a nonionic surfactant;(iv) heating the above sheared blend below about the glass transition temperature (Tg) of the resin to form electrostatically bound toner size aggregates with a narrow particle size distribution;(v) adding additional ionic surfactant to the aggregated suspension of (iv) to ensure that no, or minimal additional particle growth of the electrostatically bound toner size aggregates occurs on further increasing the temperature to coalesce the aggregates into toner particles (vi);(vi) heating the mixture of (v) with bound aggregates above about or at the Tg of the resin; and optionally(vii) separating the toner particles from the aqueous slurry by filtration and thereafter optionally washing.
摘要翻译：一种制备调色剂组合物或调色剂颗粒的方法，包括：（i）提供由颜料，离子表面活性剂和任选的电荷控制剂组成的水性颜料分散体; （ii）提供由蜡组成的蜡分散体，由非离子表面活性剂，离子表面活性剂或其混合物组成的分散剂; （iii）用由树脂，具有与所述离子表面活性剂的电荷极性相反的电荷极性的抗衡离子表面活性剂和非离子表面活性剂组成的胶乳或乳液共混物来剪切蜡分散体和颜料分散体的混合物; （iv）将上述剪切混合物加热至低于树脂的玻璃化转变温度（Tg），以形成具有窄粒度分布的静电结合的调色剂尺寸聚集体; （v）向（iv）的聚集悬浮液中加入另外的离子表面活性剂，以确保在进一步升高温度以使聚集体聚结成调色剂颗粒（vi）时，静电结合的调色剂尺寸聚集体不会发生或最小的附加颗粒生长。（vi）将（v）混合物加热至高于树脂Tg或高于Tg的结合聚集体; 并且任选地（vii）通过过滤从调色剂颗粒与含水浆料分离，然后任选地洗涤。

46. 发明授权

US06549327B2 Photochromic gyricon display 有权
标题翻译：光致变色显示屏
公开(公告)号：US06549327B2
公开(公告)日：2003-04-15
申请号：US09864386
申请日：2001-05-24
申请人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , Erwin Buncel , James Wojtyk
发明人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , Erwin Buncel , James Wojtyk
IPC分类号： G09G308
CPC分类号： G02B26/026 , C07D491/10
摘要： Disclosed is a display comprising an arrangement of a plurality of optically anisotropic rotatable elements, each of the rotatable elements having a surface in contact with an enabling fluid, the rotatable elements being electrically dipolar in the presence of the enabling fluid and thus being subject to rotation upon application of an electric field, the rotatable elements being free to rotate in place but not free to translate substantially so as to disrupt the arrangement of rotatable elements, wherein a first portion of the surface contains a mixture of a chelating agent and a spiropyran material of the formula wherein n is an integer representing the number of repeat —CH2— units and R is —H or —CH═CH2, and wherein a second portion of the surface contains substantially no spiropyran.
摘要翻译：公开了一种显示器，其包括多个光学各向异性可旋转元件的布置，每个可旋转元件具有与启用流体接触的表面，可旋转元件在有效流体存在的情况下是电偶极性的，因此被旋转在施加电场时，可旋转元件可自由旋转到位，但不能自由平移以便基本上平移以便破坏可旋转元件的布置，其中表面的第一部分包含螯合剂和螺吡喃材料的混合物其中n是表示重复-CH 2 - 单元的数目的整数，并且R是-H或-CH = CH 2，并且其中该表面的第二部分基本上不含螺吡喃。

47. 发明授权

US06652959B2 Marking particles 有权
公开(公告)号：US06652959B2
公开(公告)日：2003-11-25
申请号：US10042341
申请日：2002-01-11
申请人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier
发明人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier
IPC分类号： B32B516
CPC分类号： G03G9/0914 , G03G9/0906 , G03G9/0916 , G03G9/0922 , Y10T428/25 , Y10T428/254 , Y10T428/2982 , Y10T428/2989
摘要： Disclosed are marking particles comprising a resin, a chelating agent, and a spiropyran material which is of the formula The marking particles are prepared by an emulsion aggregation process.

48. 发明授权

US06517618B2 Photochromic electrophoretic ink display 有权
标题翻译：光致变色电泳油墨显示
公开(公告)号：US06517618B2
公开(公告)日：2003-02-11
申请号：US09864902
申请日：2001-05-24
申请人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , James Wojtyk , Erwin Buncel
发明人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , James Wojtyk , Erwin Buncel
IPC分类号： C09D1100
CPC分类号： C09D11/50 , G02F2001/1678
摘要： Disclosed is an electrophoretic ink comprising a suspending fluid and, suspended in the suspending fluid, a plurality of particles comprising a mixture of a chelating agent and a spiropyran material of the formula wherein n is an integer representing the number of repeat —CH2— units and R is —H or —CH═CH2, the particles being free to migrate within the suspending fluid under the influence of an electric field.
摘要翻译：公开了一种包含悬浮液并且悬浮在悬浮液中的多个包含螯合剂和糠醛的螺吡喃物质的混合物的颗粒的电泳墨水，n是表示重复-CH 2 - 单元数目的整数，并且R 是-H或-CH = CH 2，颗粒在电场的影响下在悬浮液中自由迁移。

49. 发明授权

US06458165B1 Marking particles 有权
标题翻译：标记颗粒
公开(公告)号：US06458165B1
公开(公告)日：2002-10-01
申请号：US10042343
申请日：2002-01-11
申请人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , James Wojtyk , Erwin Buncel
发明人： Daniel A. Foucher , Raj D. Patel , Naveen Chopra , Peter M. Kazmaier , James Wojtyk , Erwin Buncel
IPC分类号： G09F932
CPC分类号： G03G9/0906 , G03G9/0912 , G03G9/0914
摘要： Disclosed are marking particles comprising a first polymer a second polymer, a chelating agent, and a spiropyran material of the formula wherein n is an integer representing the number of repeat —CH2— units and R is —H or —CH═CH2. The marking particles comprise a core containing the first polymer in which is dispersed the chelating agent and the spiropyran and encapsulated within a shell of the second polymer formulated by an interfacial polymerization.
摘要翻译：公开了包含第一聚合物的标记颗粒，第二聚合物，螯合剂和糠醛的螺吡喃材料，n是表示重复-CH 2 - 单元的数目并且R为-H或-CH = CH 2的整数。标记颗粒包含含有第一聚合物的核心，其中分散有螯合剂和螺吡喃并包封在通过界面聚合配制的第二聚合物的壳体内。

50. 发明授权

US07410750B2 Multicolored photochromic display 有权
标题翻译：多彩多姿的光致变色显示
公开(公告)号：US07410750B2
公开(公告)日：2008-08-12
申请号：US10881682
申请日：2004-06-30
申请人： Naveen Chopra , Daniel A. Foucher , Raj D. Patel
发明人： Naveen Chopra , Daniel A. Foucher , Raj D. Patel
IPC分类号： G03C1/00
CPC分类号： C09K9/02 , C09K2211/1011 , C09K2211/1029 , C09K2211/1088 , C09K2211/1092 , G02F1/15 , G03G9/0906 , G03G9/0916
摘要： A multicolored display and process for forming such a display is provided. The multicolored display includes marking particles comprising a mixture of photochromic materials. The photochromic materials each exhibit a first “invisible” photochromic state at a first absorption spectrum and at least a second “visible” photochromic state at a second absorption spectrum. The second “visible” photochromic state of each photochromic material produces a different color relative to the other photochromic materials. In embodiments, the marking particles include a mixture of a spiropyran material and a dithienylethene material.
摘要翻译：提供了用于形成这种显示器的多彩显示和处理。多色显示器包括包含光致变色材料的混合物的标记颗粒。光致变色材料在第一吸收光谱和第二吸收光谱下呈现出至少第二“可见”光致变色状态的第一“不可见”光致变色状态。每种光致变色材料的第二种“可视”光致变色状态相对于其它光致变色材料产生不同的颜色。在实施方案中，标记颗粒包括螺吡喃材料和二噻吩乙烯材料的混合物。

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