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    • 44. 发明授权
    • Production of foamed polymer structures
    • 泡沫聚合物结构的生产
    • US4822537A
    • 1989-04-18
    • US209018
    • 1988-06-20
    • Carroll W. LanierH. Eugene BroemmelsiekRaymond Lee
    • Carroll W. LanierH. Eugene BroemmelsiekRaymond Lee
    • B29C33/06B29C35/08B29C44/34C08J9/00C08J9/04B29C35/12
    • C08J9/00B29C35/08B29C44/3415B29C33/06B29K2079/00C08J2379/08Y10S264/05Y10S521/915
    • Described are ways of improving the yields of specification grade polyimide on a consistent basis from one run to the next, by use of improved microwave-based foaming processes. In one such process, during the application of the microwave radiation, the body of polyimide precursor and of the foam structure as it is developing therefrom are maintained under a substantially vapor-impermeable microwave-compatible shroud that does not substantially restrict or impede development of the foam structure; and the microwave radiation is directed upon the top, sides and ends of the body of polyimide precursor and of the foam structure as it is developing, but the extent to which such radiation impinges upwardly into the bottom of said body and said foam structure is curtailed, preferably by means of a metallic shield located below the precursor and developing foam structure. Mechanism by which the shields and shrouds function to provide the improvements of the process are discussed, and methods based thereon are set forth.
    • 描述的是通过使用改进的基于微波的发泡方法,在一个运行到下一个的一致的基础上提高了规格级聚酰亚胺的产率。 在一个这样的方法中,在施加微波辐射期间,将聚酰亚胺前体和泡沫结构体从其显影的本体保持在基本上不透气的微波相容的护罩下,其基本上不会限制或阻碍 泡沫结构; 并且微波辐射在聚酰亚胺前体和泡沫结构的主体的顶部,侧面和端部被引导时,它们正在显影,但是这种辐射向上侵入所述主体的底部和所述泡沫结构的程度被限制 ,优选地通过位于前体下方的金属屏蔽和显影泡沫结构。 讨论了屏蔽罩和护罩作用于提供过程改进的机理,并阐述了基于此的方法。