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    • 44. 发明授权
    • Joined body of aluminum nitride series ceramics, method of joining aluminum nitride series ceramics and joining agent
    • 氮化铝系列陶瓷的接合体,氮化铝系陶瓷的接合方法和接合剂
    • US06261708B1
    • 2001-07-17
    • US09013042
    • 1998-01-26
    • Tsuneaki OhashiTsutomu Imai
    • Tsuneaki OhashiTsutomu Imai
    • B32B516
    • C04B35/645C04B37/005C04B2235/6562C04B2235/658C04B2237/06C04B2237/064C04B2237/08C04B2237/10C04B2237/366C04B2237/708C04B2237/765Y10T403/479Y10T428/256
    • A novel method is provided for joining substrates made of aluminum nitride series ceramics to each other, which can perform the joining substantially without leaving an intervening third phase other than aluminum nitride series ceramics at the joining interface of the substrates. The method is performed, for example, by providing a joining agent 3 containing at least an aluminum nitride series ceramics and a flux between the substrates 1 and 2, heat treating the joining agent to eutectically melt the aluminum nitride series ceramics and the flux, then precipitating a reprecipitated phase of the aluminum nitride series ceramics at the joining interface of the substrates. Alternatively, the method is performed by providing a joining agent 3 containing at least an aluminum nitride series ceramics and a flux between the substrates 1 and 2, heating the joining agent to a temperature range T1 which is higher than the melting point of the flux, subsequently heating the joining agent to a temperature range T2 which is higher than the temperature range T1 to exit the components of the flux from the joining interface, ten precipitating the reprecipitated phase of the aluminum nitride series ceramics at the joining interface.
    • 提供了一种用于将由氮化铝系列陶瓷制成的衬底彼此接合的新方法,其可以在基板的接合界面处基本上不会留下除氮化铝系列陶瓷之外的中间第三相而进行接合。 该方法例如通过提供至少包含氮化铝系陶瓷的接合剂3和在基板1和2之间的焊剂,对接合剂进行热处理以使氮化铝系列陶瓷和焊剂共晶化,然后 在基板的接合界面处沉淀出氮化铝系陶瓷的再沉淀相。 或者,该方法通过提供至少包含氮化铝系陶瓷的接合剂3和在基板1和2之间的焊剂,将接合剂加热到高于焊剂的熔点的温度范围T1, 随后将接合剂加热到高于温度范围T1的温度范围T2以从接合界面离开焊剂的组分,在接合界面处使氮化铝系陶瓷的再沉淀相沉淀10次。