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    • 45. 发明专利
    • INCIDENCE DEVICE FOR FOURIER TRANSFORMATION TYPE OPTICAL FIBER LOSS MEASURING INSTRUMENT
    • JPS63144231A
    • 1988-06-16
    • JP29177886
    • 1986-12-08
    • NIPPON TELEGRAPH & TELEPHONE
    • OISHI YASUTAKESAKAGUCHI SHIGEKI
    • G02B6/42G01M11/00G01M11/02
    • PURPOSE:To measure the loss spectrum of an optical fiber with high accuracy by providing an aperture behind a concave mirror which converges luminous flux projected by a Michelson interferometer and reducing the diameter of converged light incident on the optical fiber. CONSTITUTION:The Michelson interferometer consists of a light source 1, the concave mirror 2, fixed mirrors 3 and 3', a movable mirror 4, and a beam splitter 5. Composite wave luminous flux from the interferometer is converged by an elliptic mirror 6, and made incident on a convex lens 8 after being transmitted through the aperture 7 to obtain parallel luminous flux. Then part of the luminous flux is branched by an optical demultiplexer and this luminous flux is guided to a photodetector 14' through an optical attenuator 10 and the convex lens 8. The remaining luminous flux demultiplexed by the optical demultiplexer 9, on the other hand, is converged by the convex lens 9 and incident on an optical fiber 13 arranged by an optical fiber holder 12 so that its incidence end surface is on the focus, and its projection light is detected by a photodetector 14. The outputs of photodetectors 14 and 14' are guided to a computer through a preamplifier and an A/D converter and processed by Fourier transformation to obtain a projection light spectram.
    • 47. 发明专利
    • PREPARATION OF ZIRCONIUM FLUORIDE HAVING HIGH PURITY
    • JPS62176916A
    • 1987-08-03
    • JP1973186
    • 1986-01-31
    • NIPPON TELEGRAPH & TELEPHONE
    • FUJIURA KAZUOOISHI YASUTAKESAKAGUCHI SHIGEKI
    • C01G25/04
    • PURPOSE:To prepare ZrF4 having high purity and desired particle size capable of providing ZrF4 infrared optical fiber having extremely small transmission loss in large amt. by allowing vaporized ZrBr4 to react with F-contg. gas in gaseous phase. CONSTITUTION:ZrBr4 is formed by feeding gaseous mixture consisting of Br2 and Ar to an electric furnace 3 packed with metallic Zr powder 4 between quartz filters 2, 2 provided in the inside of a ZrBr4-forming section 1 and heating the Zr powder at ca. 330 deg.C. Then, the vaporized ZrBr4 at high temp. is introduced into a Pt reaction tube 6 provided in a reaction zone 10 through an introducing pipe 5 which is held at a temp. (e.g. ca. 400 deg.C) sufficient for preventing condensation of ZrBr4, and the gaseous mixture is heated at 100-800 deg.C (e.g. 500 deg.C) in a horizontal electric furnace 7, and allowed to react in the gaseous phase with introduced F-contg. gas such as HF diluted with Ar. Thus, the particle size is controlled within a range from fine powder to granular body easily by the control of the reaction condition, and obtd. product is collected by a cyclone 8 and a collector 9 to prepare the titled ZrF4.