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41. 发明授权

US06414110B1 Purification means 失效
标题翻译：净化手段
公开(公告)号：US06414110B1
公开(公告)日：2002-07-02
申请号：US09667856
申请日：2000-09-20
申请人： Michael T. Sheehan , James R. Sounik , Keith M. Russ
发明人： Michael T. Sheehan , James R. Sounik , Keith M. Russ
IPC分类号： C08F600
CPC分类号： C08F6/12 , C08F6/10
摘要： The invention provides a novel process for improving the glass transition temperatures of polymers by partitioning the polymer between immiscible solvents to remove the low molecular weight polymer from the desired product.
摘要翻译：本发明提供了一种用于通过将聚合物分配在不混溶溶剂之间以从所需产物中除去低分子量聚合物来提高聚合物玻璃化转变温度的新方法。

42. 发明授权

US5625007A Process for making low optical polymers and copolymers for photoresists and optical applications 失效
标题翻译：制备用于光致抗蚀剂和光学应用的低光学聚合物和共聚物的方法
公开(公告)号：US5625007A
公开(公告)日：1997-04-29
申请号：US295362
申请日：1994-08-24
申请人： Michael T. Sheehan , James H. Rea
发明人： Michael T. Sheehan , James H. Rea
IPC分类号： C08F8/12 , C08F8/14
CPC分类号： C08F8/14 , C08F2810/50
摘要： The present invention pertains to polymers comprising poly(4-hydroxystyrene) or substituted poly(4-hydroxystyrene) or both. The polymers have low optical density (absorbance) over a wavelength range from about 240 to about 260 nm, as well as low optical density over the near UV and visible spectrum (310 to 800 nm). Such polymers are produced by polymerizing 4-acetoxystyrene and/or substituted 4-acetoxystyrene monomers, with or without other comonomers, and subsequently performing transesterification. In the most preferred embodiment of the present invention, the polymers are produced using at least one alcohol as a reaction medium, a chain transfer agent and a transesterification reactant, providing an unusually economic process. These polymers are particularly useful as photoresist components for use in combination with deep UV, X-ray, and E-Beam imaging systems.
摘要翻译：本发明涉及包含聚（4-羟基苯乙烯）或取代的聚（4-羟基苯乙烯）或两者的聚合物。聚合物在约240至约260nm的波长范围内具有低光密度（吸光度），以及在近紫外和可见光谱（310至800nm）下的低光密度。这样的聚合物通过聚合4-乙酰氧基苯乙烯和/或取代的4-乙酰氧基苯乙烯单体，与或不与其它共聚单体共聚，然后进行酯交换。在本发明的最优选的实施方案中，使用至少一种醇作为反应介质，链转移剂和酯交换反应物来生产聚合物，提供非常经济的方法。这些聚合物特别可用作与深UV，X射线和E-Beam成像系统组合使用的光致抗蚀剂组分。

43. 发明授权

US5424387A Di-amino compounds and processes for preparing the same 失效
标题翻译：二氨基化合物及其制备方法
公开(公告)号：US5424387A
公开(公告)日：1995-06-13
申请号：US277715
申请日：1994-07-20
申请人： Michael T. Sheehan , James R. Sounik , Bret F. Hann
发明人： Michael T. Sheehan , James R. Sounik , Bret F. Hann
IPC分类号： C07C45/70 , C07C45/71 , C07C49/825 , C07C49/84 , C07C217/58 , C08G18/32 , C08G18/50 , C08G59/50 , C08G65/26 , C08G65/325 , C08G69/40 , C08G73/10 , C08L63/00
CPC分类号： C08G73/1046 , C07C217/58 , C07C45/70 , C07C45/71 , C07C49/825 , C07C49/84 , C08G18/324 , C08G18/329 , C08G18/5024 , C08G59/504 , C08G65/2603 , C08G65/2612 , C08G65/3255 , C08G69/40 , C08L63/00
摘要： Di-amines endowed with chain extension activity for formulations such as polyureas and polyurethanes are disclosed, and which have the general formula: ##STR1## wherein n is 0-1000 and m is 0-100; R.sub.1, R.sub.2, R.sub.5, and R.sub.6 are each independently selected from the group consisting of H, --CH.sub.3, --CH.sub.2 CH.sub.3, --CH.sub.2 OH, and --CH.sub.2 --CH.sub.2 --OH; and R.sub.3 and P.sub.4 are each independently selected from the group consisting of --C.sub.2 H.sub.4 --; and --C.sub.3 H.sub.6 --; and the diasteromeric salts thereof.
摘要翻译：公开了赋形剂如聚脲和聚氨酯的具有延伸活性的二胺，其具有以下通式：其中n为0-1000，m为0-100; R 1，R 2，R 5和R 6各自独立地选自H，-CH 3，-CH 2 CH 3，-CH 2 OH和-CH 2 -CH 2 -OH; 并且R 3和P 4各自独立地选自-C 2 H 4 - ; 和-C 3 H 6 - ; 及其非对映盐。

44. 发明授权

US5354907A Amines derived from THPE and processes for preparing the same 失效
标题翻译：衍生自THPE的胺和其制备方法
公开(公告)号：US5354907A
公开(公告)日：1994-10-11
申请号：US179789
申请日：1994-01-11
申请人： Michael T. Sheehan , James R. Sounik , William W. Wilkison, III
发明人： Michael T. Sheehan , James R. Sounik , William W. Wilkison, III
IPC分类号： C07C217/50 , C08G18/50 , C08G65/325 , C08G65/333 , C07C217/44 , C08G18/10 , C08G18/30
CPC分类号： C07C217/50 , C08G18/5024 , C08G18/5033 , C08G65/3255 , C08G65/33306 , C08G2120/00
摘要： Amines endowed with chain extension activity for formulations such as polyureas are disclosed, which have the general formula: ##STR1## wherein n is 0-1000; R.sub.1 .dbd.R.sub.2, and R.sub.1 and R.sub.2 are from the group --CH.sub.2 --CH.sub.2 --; --CH.sub.2 --C(CH.sub.3)H--; and --C(CH.sub.3)H--CH.sub.2 --; and R.sub.3 and R.sub.4 are each independently selected from the group consisting of H, --CH.sub.3, --CH.sub.2 CH.sub.3, --CH.sub.2 OH, and --CH.sub.2 --CH.sub.2 --OH.
摘要翻译：公开了具有如下通式的制剂如聚脲的制剂的链延伸活性的胺：其中n为0-1000; R1 = R2，R1和R2来自基团-CH2-CH2-; -CH2-C（CH3）H-; 和-C（CH 3）H-CH 2 - ; 并且R 3和R 4各自独立地选自H，-CH 3，-CH 2 CH 3，-CH 2 OH和-CH 2 -CH 2 -OH。

45. 发明授权

US5312990A Di-amino compounds 失效
标题翻译：二氨基化合物
公开(公告)号：US5312990A
公开(公告)日：1994-05-17
申请号：US69948
申请日：1993-05-28
申请人： Michael T. Sheehan , James R. Sounik , Bret F. Hann , William W. Wilkison, III
发明人： Michael T. Sheehan , James R. Sounik , Bret F. Hann , William W. Wilkison, III
IPC分类号： C07C45/70 , C07C45/71 , C07C49/825 , C07C49/84 , C07C217/58 , C08G18/32 , C08G18/50 , C08G65/26 , C08G65/325 , C07C217/44
CPC分类号： C08G65/3255 , C07C217/58 , C07C45/70 , C07C45/71 , C07C49/825 , C07C49/84 , C08G18/324 , C08G18/329 , C08G18/5024 , C08G65/2603 , C08G65/2612
摘要： Di-amines endowed with chain extension activity for formulations such as polyureas and polyurethanes are disclosed, and which have the general formula: ##STR1## wherein n is 0-1000; R.sub.1, R.sub.2, R.sub.5, and R.sub.6 are each independently selected from the group consisting of H, --CH.sub.3, --CH.sub.2 CH.sub.3, --CH.sub.2 OH, and --CH.sub.2 --CH.sub.2 --OH; R.sub.3 .dbd.R.sub.4, and R.sub.3 and R.sub.4 are from the group --CH.sub.2 --CH.sub.2 --; --CH.sub.2 --C(CH.sub.3)H--; and --C(CH.sub.3)H--CH.sub.2 --; and the diasteromeric salts thereof.
摘要翻译：公开了赋形剂如聚脲和聚氨酯的赋链链延伸活性的二胺，其具有以下通式：其中n为0-1000; R 1，R 2，R 5和R 6各自独立地选自H，-CH 3，-CH 2 CH 3，-CH 2 OH和-CH 2 -CH 2 -OH; R3 = R4，R3和R4来自基团-CH2-CH2-; -CH2-C（CH3）H-; 和-C（CH 3）H-CH 2 - ; 及其非对映盐。

46. 发明授权

US5304610A Amphoteric copolymer derived from vinylpyridine and acetoxystyrene 失效
标题翻译：衍生自乙烯基吡啶和乙酰氧基苯乙烯的两性共聚物
公开(公告)号：US5304610A
公开(公告)日：1994-04-19
申请号：US42358
申请日：1993-04-02
申请人： Apurba Bhattacharya , Kenneth G. Davenport , Michael T. Sheehan , James R. Sounik
发明人： Apurba Bhattacharya , Kenneth G. Davenport , Michael T. Sheehan , James R. Sounik
IPC分类号： G03F7/033 , A61K8/00 , A61K8/37 , A61K8/49 , A61K47/30 , A61Q5/02 , A61Q5/12 , B01F17/40 , B01F17/52 , C08F8/12 , C08F12/00 , C08F26/06 , C08F212/14 , C08F226/06 , C08L39/00 , C08L39/04 , C08L101/00 , C09D5/00 , C09K17/20 , C11D3/37
CPC分类号： C08F226/06 , C08F212/14 , C08F8/12 , G03C2001/0471
摘要： A unique polymer was synthesized via copolymerization of vinylpyridine and acetoxystyrene under radical-initiated conditions followed by acidic or basic hydrolysis of the acetoxy group to afford the corresponding hydroxy group. The built-in acid-base dual functionality (phenolic and pyridyl units) in this polymer backbone gives rise to its unique solubility properties over a wide pH range in both aqueous and non-aqueous media. Due to its amphoteric nature, this polymer finds application as an anti-stat, viscosity modifier, and/or ion-exchange resin.
摘要翻译：通过乙烯基吡啶和乙酰氧基苯乙烯在自由基引发条件下的共聚合，然后酸性或碱性水解乙酰氧基来合成独特的聚合物，得到相应的羟基。该聚合物骨架中的内置酸碱双官能团（酚类和吡啶基单元）在水性和非水性介质中都能在宽的pH范围内产生独特的溶解性。由于其两性性质，该聚合物可用作抗静电，粘度调节剂和/或离子交换树脂。

47. 发明授权

US5239015A Process for making low optical density polymers and copolymers for photoresists and optical applications 失效
标题翻译：制备用于光致抗蚀剂和光学应用的低光密度聚合物和共聚物的方法
公开(公告)号：US5239015A
公开(公告)日：1993-08-24
申请号：US706601
申请日：1991-05-28
申请人： Michael T. Sheehan , James H. Rea
发明人： Michael T. Sheehan , James H. Rea
IPC分类号： C08F8/12 , C08F8/14
CPC分类号： C08F8/14 , C08F2810/50
摘要： The present invention pertains to a process for the preparation of polymers comprising poly(4-hydroxystyrene) or substituted poly(4-hydroxystyrene) or both. The polymers have low optical density (absorbance) over a wavelength range from about 240 to about 260 nm, as well as low optical density over the near UV and visible spectrum (310 to 800 nm). Such polymers are produced by polymerizing 4-acetoxystyrene and/or substituted 4-acetoxystyrene monomers, with or without other comonomers, and subsequently performing transesterification. In the most preferred embodiment of the present invention, the polymers are produced using at least one alcohol as a reaction medium, a chain transfer agent and a transesterification reactant, providing an unusually economic process. These polymers are particularly useful as photoresist components for use in combination with deep UV, X-ray, and E-Beam imaging systems.To obtain polymers having low optical density over the 240 to 260 nm radiation wavelength range, it is necessary to use an initiator which does not comprise a substantially absorbant structure over the 240 to 260 nm range or to use an initiator concentration of less than about 3 mole % of the monomer(s), to obtain a polymerization conversion of the initial polymerization monomers of at least about 90% by weight, or to remove residual monomer(s) from the reaction medium prior to transesterification, and to obtain a transesterification conversion of the polymerized monomers of at least 85% by weight. It is also necessary to avoid the use of transesterification catalyst which can cause the formation of chemical structures which can absorb over the 240 to 260 nm radiation wavelength range.
摘要翻译：本发明涉及制备包含聚（4-羟基苯乙烯）或取代的聚（4-羟基苯乙烯）或两者的聚合物的方法。聚合物在约240至约260nm的波长范围内具有低光密度（吸光度），以及在近紫外和可见光谱（310至800nm）下的低光密度。这样的聚合物通过聚合4-乙酰氧基苯乙烯和/或取代的4-乙酰氧基苯乙烯单体，与或不与其它共聚单体共聚，然后进行酯交换。在本发明的最优选的实施方案中，使用至少一种醇作为反应介质，链转移剂和酯交换反应物来生产聚合物，提供非常经济的方法。这些聚合物特别可用作与深UV，X射线和E-Beam成像系统组合使用的光致抗蚀剂组分。为了获得在240至260nm辐射波长范围内具有低光密度的聚合物，必须使用在240至260nm范围内不包含基本吸收结构的引发剂，或者使用小于约3的引发剂浓度摩尔％的单体，以获得至少约90重量％的初始聚合单体的聚合转化率，或者在酯交换之前从反应介质中除去残留的单体，并获得酯交换转化的聚合单体为至少85重量％。还有必要避免使用酯交换催化剂，其可导致可以在240至260nm辐射波长范围内吸收的化学结构的形成。

48. 发明授权

US5087772A Method for preparing 4-hydroxystyrene 失效
标题翻译：制备4-羟基苯乙烯的方法
公开(公告)号：US5087772A
公开(公告)日：1992-02-11
申请号：US614767
申请日：1990-11-16
申请人： Michael T. Sheehan , Lan Shen
发明人： Michael T. Sheehan , Lan Shen
IPC分类号： B01J23/02 , B01J31/02 , C07B61/00 , C07C37/055 , C07C39/06 , C07C39/20
CPC分类号： C07C37/0555
摘要： A method for preparing 4-hydroxystyrene is disclosed. The method comprises reacting 4-acetoxystyrene with a suitable alcohol in the presence of a catalytic amount of a suitable base.

49. 发明授权

US4880487A Hot melt adhesives containing poly(p-hydroxystyrene) homopolymers and copolymers and bonding methods employing same 失效
标题翻译：含有聚（对羟基苯乙烯）均聚物和共聚物的热熔粘合剂以及使用其的粘合方法
公开(公告)号：US4880487A
公开(公告)日：1989-11-14
申请号：US210897
申请日：1988-06-24
申请人： Michael T. Sheehan , Bakulesh N. Shah
发明人： Michael T. Sheehan , Bakulesh N. Shah
IPC分类号： C08L25/18 , C08L25/00 , C08L77/00 , C08L101/00 , C09J123/08
CPC分类号： C08L77/00 , C09J123/08
摘要： A hot melt adhesive composition which is especially useful for bonding polyamide article to surfaces, particularly polyamide surfaces. The composition contains an ethylene-vinyl ester copolymer or a polyamide polymer, and additionally contains a poly(p-hydroxystyrene) homopolymer or a copolymer of poly(p-hydroxystyrene) with a C.sub.1 to C.sub.4 alkyl acrylate.

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