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41. 发明授权

US08841227B2 Production of aromatics from methane 有权
标题翻译：从甲烷生产芳烃
公开(公告)号：US08841227B2
公开(公告)日：2014-09-23
申请号：US12863467
申请日：2008-12-22
申请人： Neeraj Sangar , Jocelyn A. Kowalski , Larry L. Iaccino , Kenneth R. Clem
发明人： Neeraj Sangar , Jocelyn A. Kowalski , Larry L. Iaccino , Kenneth R. Clem
IPC分类号： B01J29/06 , B01J37/08 , C07C2/76 , B01J35/00 , B01J29/076 , B01J29/48 , B01J37/00 , B01J21/06
CPC分类号： B01J29/48 , B01J21/063 , B01J21/066 , B01J29/076 , B01J35/0006 , B01J35/002 , B01J37/0009 , B01J37/08 , B01J2229/20 , B01J2229/42 , C07C2/76 , C07C2529/48 , C10G2300/1025 , C10G2400/30 , C07C15/00
摘要： A catalyst for the conversion of methane to higher hydrocarbons including aromatic hydrocarbons comprises a support and molybdenum or a compound thereof dispersed on the support. The support comprises an aluminosilicate zeolite combined with a binder selected from silica, titania, zirconia and mixtures thereof. The catalyst is substantially free of aluminum external to the framework of the aluminosilicate zeolite.
摘要翻译：用于将甲烷转化为包括芳烃的高级烃的催化剂包括分散在载体上的载体和钼或其化合物。载体包括与选自二氧化硅，二氧化钛，氧化锆及其混合物的粘合剂组合的铝硅酸盐沸石。催化剂基本上不含铝硅酸盐沸石骨架外的铝。

42. 发明授权

US08691079B2 Compression reactor and process for hydroprocessing 有权
标题翻译：压缩反应器和加氢处理方法
公开(公告)号：US08691079B2
公开(公告)日：2014-04-08
申请号：US12689154
申请日：2010-01-18
申请人： Larry L. Iaccino
发明人： Larry L. Iaccino
IPC分类号： C10G69/06
CPC分类号： B01J3/08 , C10G9/00 , C10G47/00 , C10G69/06
摘要： The present invention is directed to a process for hydroprocessing of a liquid hydrocarbon feedstock, comprising: (a) mixing liquid, partially vaporized and/or vaporized hydrocarbon feedstock with molecular hydrogen; (b) feeding said mixture into a compression reactor; (c) compressing said mixture to a pressure, a temperature and for a residence time sufficient to: i) thermally crack at least a portion of hydrocarbon molecules in said hydrocarbon feedstock, and ii) react hydrogen in the presence of a hydrogenation catalyst with unstable portions of the cracked molecules, forming a hydroprocessed product; and (d) expanding said mixture to reduce the pressure and temperature thereby reducing subsequent undesirable reactions.
摘要翻译：本发明涉及一种用于液体烃原料的加氢处理的方法，包括：（a）将液体，部分蒸发和/或蒸发的烃原料与分子氢混合; （b）将所述混合物进料到压缩反应器中; （c）将所述混合物压缩至足够的压力，温度和停留时间，足以：i）热裂解所述烃原料中的至少一部分烃分子，和ii）在氢化催化剂存在下使不稳定的氢气反应部分裂解分子，形成加氢处理产物; 和（d）膨胀所述混合物以降低压力和温度，从而减少随后的不期望的反应。

43. 发明申请

US20110174682A1 Compression Reactor And Process For Hydroprocessing 有权
标题翻译：压缩反应器和加氢处理方法
公开(公告)号：US20110174682A1
公开(公告)日：2011-07-21
申请号：US12689154
申请日：2010-01-18
申请人： Larry L. Iaccino
发明人： Larry L. Iaccino
IPC分类号： C10G69/06 , B01J8/08
CPC分类号： B01J3/08 , C10G9/00 , C10G47/00 , C10G69/06
摘要： The present invention is directed to a process for hydroprocessing of a liquid hydrocarbon feedstock, comprising: (a) mixing liquid, partially vaporized and/or vaporized hydrocarbon feedstock with molecular hydrogen; (b) feeding said mixture into a compression reactor; (c) compressing said mixture to a pressure, a temperature and for a residence time sufficient to: i) thermally crack at least a portion of hydrocarbon molecules in said hydrocarbon feedstock, and ii) react hydrogen in the presence of a hydrogenation catalyst with unstable portions of the cracked molecules, forming a hydroprocessed product; and (d) expanding said mixture to reduce the pressure and temperature thereby reducing subsequent undesirable reactions.
摘要翻译：本发明涉及一种用于液体烃原料的加氢处理的方法，包括：（a）将液体，部分蒸发和/或蒸发的烃原料与分子氢混合; （b）将所述混合物进料到压缩反应器中; （c）将所述混合物压缩至足够的压力，温度和停留时间，足以：i）热裂解所述烃原料中的至少一部分烃分子，和ii）在氢化催化剂存在下使不稳定的氢气反应部分裂解分子，形成加氢处理产物; 和（d）膨胀所述混合物以降低压力和温度，从而减少随后的不期望的反应。

44. 发明授权

US07977519B2 Production of aromatic hydrocarbons from methane 有权
标题翻译：从甲烷生产芳烃
公开(公告)号：US07977519B2
公开(公告)日：2011-07-12
申请号：US12701841
申请日：2010-02-08
申请人： Larry L. Iaccino , Neeraj Sangar , Elizabeth L. Stavens
发明人： Larry L. Iaccino , Neeraj Sangar , Elizabeth L. Stavens
IPC分类号： C07C4/22
CPC分类号： C07C2/76 , C07C2/78 , C10G2400/30 , Y10S585/943 , C07C15/02
摘要： In a process for converting methane to higher hydrocarbons including aromatic hydrocarbons, a feed containing methane is contacted with a dehydrocyclization catalyst in a reaction zone under conditions effective to convert said methane to aromatic hydrocarbons. A first portion of the catalyst is transferred from the reaction zone to a heating zone, where the first catalyst portion is heated by contacting the catalyst with hot combustion gases generated by burning a supplemental source of fuel. The heated first catalyst portion is then returned to the reaction zone.
摘要翻译：在将甲烷转化为包括芳烃的高级烃的方法中，在有效将甲烷转化为芳族烃的条件下，含有甲烷的进料在反应区中与脱氢环化催化剂接触。催化剂的第一部分从反应区转移到加热区，其中第一催化剂部分通过使催化剂与通过燃烧补充燃料源燃烧产生的热燃烧气体接触来加热。然后将加热的第一催化剂部分返回到反应区。

45. 发明授权

US07968759B2 Production of aromatics from methane 失效
标题翻译：从甲烷生产芳烃
公开(公告)号：US07968759B2
公开(公告)日：2011-06-28
申请号：US12851244
申请日：2010-08-05
申请人： Larry L. Iaccino , Elizabeth L. Stavens , Neeraj Sangar , Jeremy J. Patt
发明人： Larry L. Iaccino , Elizabeth L. Stavens , Neeraj Sangar , Jeremy J. Patt
IPC分类号： C07C2/78
CPC分类号： C07C2/76 , C07C2529/48 , C10G45/44 , Y02P20/142 , Y02P20/52 , Y10S585/943 , C07C15/04 , C07C15/02
摘要： In a process for converting methane to aromatic hydrocarbons, a feed containing methane is supplied to one or more reaction zone(s) containing catalytic material operating under reaction conditions effective to convert at least a portion of the methane to aromatic hydrocarbons; the reaction zone(s) being operated with an inverse temperature profile.
摘要翻译：在将甲烷转化为芳族烃的方法中，含有甲烷的进料被供应到一个或多个反应区，该反应区含有在有效将甲烷的至少一部分转化为芳烃的反应条件下运行的催化材料; 反应区域以反向温度曲线运行。

46. 发明授权

US07893308B2 Production of aromatics from methane 有权
标题翻译：从甲烷生产芳烃
公开(公告)号：US07893308B2
公开(公告)日：2011-02-22
申请号：US11891752
申请日：2007-08-13
申请人： Neeraj Sangar , Larry L. Iaccino , Jeffrey P. Jones
发明人： Neeraj Sangar , Larry L. Iaccino , Jeffrey P. Jones
IPC分类号： C07C2/52
CPC分类号： C07C2/76 , C07C2521/04 , C07C2521/08 , C07C2523/06 , C07C2523/28 , C07C2523/30 , C07C2523/36 , C07C2529/40 , C10G50/00 , C10G2300/1025 , C10G2400/30
摘要： In a process for converting methane to aromatic hydrocarbons, a feed containing methane is contacted with a dehydrocyclization catalyst in a reaction zone under conditions effective to convert the methane to aromatic hydrocarbons. The reaction zone is contained within a reactor and the reactor or an internal component of the reactor has at least one surface that is chemically exposed to the feed and is formed from a refractory material that exhibits a carbon uptake (mass of carbon absorbed per unit of exposed metal surface area) of less than 25 g/m2 when exposed to mixture of 50 vol % methane and 50 vol % H2 at 900° C. for 168 hours.
摘要翻译：在将甲烷转化为芳族烃的方法中，在有效将甲烷转化为芳族烃的条件下，含有甲烷的进料在反应区与脱氢环化催化剂接触。反应区包含在反应器内，反应器或反应器的内部组分具有化学暴露于进料的至少一个表面，并且由表现出碳吸收的耐火材料形成（每单位面积吸收的碳的质量暴露的金属表面积）当暴露于50体积％甲烷和50体积％H 2的混合物在900℃下168小时时小于25g / m 2。

47. 发明申请

US20100331592A1 Production of Aromatics from Methane 有权
标题翻译：从甲烷生产芳烃
公开(公告)号：US20100331592A1
公开(公告)日：2010-12-30
申请号：US12863467
申请日：2008-12-22
申请人： Neeraj Sangar , Jocelyn A. Kowalski , Larry L. Iaccino , Kenneth R. Clem
发明人： Neeraj Sangar , Jocelyn A. Kowalski , Larry L. Iaccino , Kenneth R. Clem
IPC分类号： B01J29/076 , B01J29/48 , C07C2/00
CPC分类号： B01J29/48 , B01J21/063 , B01J21/066 , B01J29/076 , B01J35/0006 , B01J35/002 , B01J37/0009 , B01J37/08 , B01J2229/20 , B01J2229/42 , C07C2/76 , C07C2529/48 , C10G2300/1025 , C10G2400/30 , C07C15/00
摘要： A catalyst for the conversion of methane to higher hydrocarbons including aromatic hydrocarbons comprises a support and molybdenum or a compound thereof dispersed on the support. The support comprises an aluminosilicate zeolite combined with a binder selected from silica, titania, zirconia and mixtures thereof. The catalyst is substantially free of aluminum external to the framework of the aluminosilicate zeolite.
摘要翻译：用于将甲烷转化为包括芳烃的高级烃的催化剂包括分散在载体上的载体和钼或其化合物。载体包括与选自二氧化硅，二氧化钛，氧化锆及其混合物的粘合剂组合的铝硅酸盐沸石。催化剂基本上不含铝硅酸盐沸石骨架外的铝。

48. 发明申请

US20100305374A1 Production Of Aromatics From Methane 失效
标题翻译：从甲烷生产芳烃
公开(公告)号：US20100305374A1
公开(公告)日：2010-12-02
申请号：US12851244
申请日：2010-08-05
申请人： Larry L. Iaccino , Elizabeth L. Stavens , Neeraj Sangar , Jeremy J. Patt
发明人： Larry L. Iaccino , Elizabeth L. Stavens , Neeraj Sangar , Jeremy J. Patt
IPC分类号： C07C5/02 , C07C2/00
CPC分类号： C07C2/76 , C07C2529/48 , C10G45/44 , Y02P20/142 , Y02P20/52 , Y10S585/943 , C07C15/04 , C07C15/02
摘要： In a process for converting methane to aromatic hydrocarbons, a feed containing methane is supplied to one or more reaction zone(s) containing catalytic material operating under reaction conditions effective to convert at least a portion of the methane to aromatic hydrocarbons; the reaction zone(s) being operated with an inverse temperature profile.
摘要翻译：在将甲烷转化为芳族烃的方法中，含有甲烷的进料被供应到一个或多个反应区，该反应区含有在有效将甲烷的至少一部分转化为芳烃的反应条件下运行的催化材料; 反应区域以反向温度曲线运行。

49. 发明申请

US20100240935A1 Use of Isotopic Analysis for Determination of Aromatic Hydrocarbons Produced From Methane 审中-公开
标题翻译：使用同位素分析测定甲烷产生的芳香烃
公开(公告)号：US20100240935A1
公开(公告)日：2010-09-23
申请号：US12790204
申请日：2010-05-28
申请人： Larry L. Iaccino , Jeremy J. Patt
发明人： Larry L. Iaccino , Jeremy J. Patt
IPC分类号： C07C15/04
CPC分类号： C07C2/66 , C07C2/76 , Y10S585/941 , C07C15/08 , C07C15/04
摘要： Benzene and xylene are described having a unique distribution of deuterium and 13C such that δ(deuterium) for each of the benzene and xylene is less than −250 and δ(13C) for the benzene is greater than −36 and for xylene is less than −24, wherein δ(deuterium)=(R′sample/R′standard−1)×1000 where R′sample is the ratio of deuterium to hydrogen in the benzene/xylene; and R′standard is the ratio of the natural abundance of deuterium to the natural abundance of hydrogen; and wherein δ(13C)=(R″sample/R″standard−1)×1000 where R″sample is the ratio of 13C to 12C in the benzene/xylene; and R″standard is the ratio of the natural abundance of 13C to the natural abundance of 12C.
摘要翻译：描述苯和二甲苯具有氘和13C的独特分布，使得苯和二甲苯中的每一个的δ（氘）小于-250，苯的δ（13℃）大于-36，并且对于二甲苯小于 -24，其中δ（氘）=（R'sample / R'standard-1）×1000其中R'示例是苯/二甲苯中氘与氢的比例; R'standard是氘的天然丰度与氢的天然丰度之比; 其中δ（13C）=（R“样品/ R”标准-1）×1000其中R“样品是苯/二甲苯中13C至12C的比例; 而R“标准是13C的天然丰度与12C的天然丰度之比。

50. 发明授权

US07772447B2 Production of liquid hydrocarbons from methane 有权
标题翻译：从甲烷生产液态碳氢化合物
公开(公告)号：US07772447B2
公开(公告)日：2010-08-10
申请号：US11792357
申请日：2005-12-19
申请人： Larry L. Iaccino , Elizabeth L. Stavens , Matthew J. Vincent
发明人： Larry L. Iaccino , Elizabeth L. Stavens , Matthew J. Vincent
IPC分类号： C07C2/76 , C07C2/64
CPC分类号： C10G45/44 , C07C2/76 , C07C5/10 , C07C5/11 , C10G2300/1025 , C10G2300/1092 , C10G2300/4081 , C10G2400/30 , Y10S585/943 , C07C15/02 , C07C13/00
摘要： In a process for converting methane to liquid hydrocarbons, a feed containing methane is contacted with 0 dehydrocyclization catalyst under conditions effective to convert said methane to aromatic hydrocarbons, including benzene and/or naphthalene, and produce a first effluent stream comprising hydrogen and 0t least 5 wt % m>35 aromatic hydrocarbons than said feed. At least part the aromatic hydrocarbons from the first effluent stream is then reacted with hydrogen to produce a second effluent stream having a reduced benzene and/or naphthalene content compared with said first effluent stream.
摘要翻译：在将甲烷转化为液体烃的方法中，含有甲烷的进料在有效地将所述甲烷转化为芳族烃（包括苯和/或萘）的条件下与0脱氢环化催化剂接触，并产生包含氢和0至少5 m> 35％芳族烃比所述进料。然后使来自第一流出物流的芳族烃的至少一部分与氢反应以产生与所述第一流出物流相比具有降低的苯和/或萘含量的第二流出物流。

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