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41. 发明授权

US5876801A Self lubricating device 失效
标题翻译：自润滑装置
公开(公告)号：US5876801A
公开(公告)日：1999-03-02
申请号：US936024
申请日：1997-09-23
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： B05D1/18 , B05D5/08 , C09D4/00 , B05D3/00
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , C09D4/00 , B05D5/08 , Y10T428/261 , Y10T428/266 , Y10T428/268 , Y10T428/31536 , Y10T428/31663
摘要： A chemically adsorbed film having a surface layer containing fluorine groups and a stem layer chemically bonded by siloxane bonds to a substrate is formed on the surface of a frictional portion of a machine part such as a gear or a bearing or on the surface of a game ball. An excellently self-lubricating low frictional resistance machine part or game ball thus can be obtained. A frictional portion of a gear or the like, made of SiO.sub.2 or like ceramic material, is dipped and held in a solution containing a surface active material, e.g., CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 SiCl.sub.3 dissolved in a non-aqueous solvent. A hydrochloric acid removal reaction is brought about between SiCl groups of the material, which contains a fluorocarbon and a chlorosilane group, and hydroxyl groups numerously present on the SiO2 surface, thus forming bonds ofCF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 Si (O--).sub.3over the entire frictional portion surface. A fluorine-containing monomolecular film thus is formed, which is chemically bonded to the substrate and has a thickness of about 1.5 nm.
摘要翻译：在机械部件例如齿轮或轴承的摩擦部分的表面上或游戏表面上形成具有含氟基团的表面层和通过硅氧烷键合到基材上的茎层的化学吸附膜球。因此可以获得优异的自润滑低摩擦阻力机器部件或游戏球。将由SiO 2或类似陶瓷材料制成的齿轮等的摩擦部分浸渍并保持在含有溶解在非水溶剂中的表面活性物质例如CF 3（CF 2）7（CH 2）2 ClCl 3）的溶液中。在含有碳氟化合物和氯硅烷的材料的SiCl基团和SiO 2表面上大量存在的羟基之间产生盐酸去除反应，从而形成CF 3（CF 2）7（CH 2）2 Si（O- ）3在整个摩擦部分表面上。因此，形成与基板化学键合并且具有约1.5nm的厚度的含氟单分子膜。

42. 发明授权

US5836827A Self-lubricating device 失效
标题翻译：自润滑装置
公开(公告)号：US5836827A
公开(公告)日：1998-11-17
申请号：US935551
申请日：1997-09-23
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： B05D1/18 , B05D5/08 , C09D4/00 , F16H7/22
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , C09D4/00 , B05D5/08 , Y10T428/261 , Y10T428/266 , Y10T428/268 , Y10T428/31536 , Y10T428/31663
摘要： A chemically adsorbed film having a surface layer containing fluorine groups and a stem layer chemically bonded by siloxane bonds to a substrate is formed on the surface of a frictional portion of a machine part such as a gear or a bearing or on the surface of a game ball. An excellently self-lubricating low frictional resistance machine part or game ball thus can be obtained. A frictional portion of a gear or the like, made of SiO.sub.2 or like ceramic material, is dipped and held in a solution containing a surface active material, e.g., CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 SiCl.sub.3 dissolved in a non-aqueous solvent. A hydrochloric acid removal reaction is brought about between SiCl groups of the material, which contains a fluorocarbon and a chlorosilane group, and hydroxyl groups numerously present on the SiO.sub.2 surface, thus forming bonds of CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 Si (O--).sub.3 over the entire frictional portion surface. A fluorine-containing monomolecular film thus is formed, which is chemically bonded to the substrate and has a thickness of about 1.5 nm.
摘要翻译：在机械部件例如齿轮或轴承的摩擦部分的表面上或游戏表面上形成具有含氟基团的表面层和通过硅氧烷键合到基材上的茎层的化学吸附膜球。因此可以获得优异的自润滑低摩擦阻力机器部件或游戏球。将由SiO 2或类似陶瓷材料制成的齿轮等的摩擦部分浸渍并保持在含有溶解在非水溶剂中的表面活性物质例如CF 3（CF 2）7（CH 2）2 SiCl 3）的溶液中。在含有碳氟化合物和氯硅烷的材料的SiCl基团和SiO 2表面上大量存在的羟基之间产生盐酸去除反应，从而形成CF 3（CF 2）7（CH 2）2 Si（O - ）3在整个摩擦部分表面上。因此，形成与基板化学键合并且具有约1.5nm的厚度的含氟单分子膜。

43. 发明授权

US5804252A Water- and oil repellent substrate and method of treatment 失效
标题翻译：拒水拒油基材和处理方法
公开(公告)号：US5804252A
公开(公告)日：1998-09-08
申请号：US625891
申请日：1996-04-01
申请人： Kazufumi Ogawa , Mamoru Soga
发明人： Kazufumi Ogawa , Mamoru Soga
IPC分类号： A61N1/365 , B05D1/18 , B05D5/08 , C09D4/00 , D06M15/657 , D06M23/00 , B05D3/02
CPC分类号： B82Y30/00 , A61N1/36514 , B05D1/185 , B82Y40/00 , C09D4/00 , D06M15/657 , D06M23/005 , B05D5/08 , Y10S428/913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2962 , Y10T428/31663
摘要： A durable and extremely water- and oil repellent ultra thin film is formed on the surface of a substates such as glass, ceramics, fabrics, fur and cloth by a dehydrochlorination reaction between a functional group such as a hydroxyl group or an imino group on the surface of the substrate. The coating film of the material comprises a plurality of chlorosilyl groups was formed on the surface of the substrate by dipping and holding the substrate comprising functional groups on its surface in a solution prepared by dissolving a material comprising fluorocarbon groups and a plurality of chlorosilyl groups in a non-aqueous solvent and drying the substrate which is then taken out from the solution in a substantially moistureless or low moisture atomosphere and removing the non-aqueous solvent remaining on the substrate. Further, when the coating film is left in an atomosphere comprising moisture, i.e., humid air, the coating film is polymerized by a dehydrochlorination reaction between the coating film and the moisture in the atomosphere. The film is formed on the surface of the substrate containing hydroxyl groups, imino groups or carboxyl groups through --SiO-- bonds or --SiN
摘要翻译：通过在诸如羟基或亚氨基之类的官能团之间的脱氯化氢反应，在玻璃，陶瓷，织物，毛皮和布等基底的表面上形成耐久且极其防水和防油的超薄膜基板的表面。该材料的涂膜包括在基材的表面上形成多个氯甲硅烷基，在其表面上浸渍并保持包含官能团的基材，通过将包含氟烃基和多个氯代甲硅烷基的材料溶解在非水溶剂并干燥基材，然后将其从基本上无水或低湿气体的空气溶液中取出并除去残留在基材上的非水溶剂。此外，当涂膜留在包含湿气的空气即湿空气中时，涂膜通过涂膜和大气层中的水分之间的脱氯化氢反应而聚合。该薄膜通过-SiO键或-SiN <键在含有羟基，亚氨基或羧基的基材表面上形成。

44. 发明授权

US5731077A Self-lubricating device 失效
标题翻译：自润滑装置
公开(公告)号：US5731077A
公开(公告)日：1998-03-24
申请号：US458703
申请日：1995-06-02
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： B05D1/18 , B05D5/08 , C09D4/00 , B32B9/04
CPC分类号： B82Y30/00 , B05D1/185 , B82Y40/00 , C09D4/00 , B05D5/08 , Y10T428/261 , Y10T428/266 , Y10T428/268 , Y10T428/31536 , Y10T428/31663
摘要： A chemically adsorbed film having a surface layer containing fluorine groups and a stem layer chemically bonded by siloxane bonds to a substrate is formed on the surface of a frictional portion of a machine part such as a gear or a bearing or on the surface of a game ball. An excellently self-lubricating low frictional resistance machine part or game ball thus can be obtained. A frictional portion of a gear or the like, made of SiO.sub.2 or like ceramic material, is dipped and held in a solution containing a surface active material, e.g., CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 SiCl.sub.3 dissolved in a non-aqueous solvent. A hydrochloric acid removal reaction is brought about between SiCl groups of the material, which contains a fluorocarbon and a chlorosilane group, and hydroxyl groups numerously present on the SiO2 surface, thus forming bonds of CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 Si(O--).sub.3 over the entire frictional portion surface. A fluorine-containing monomolecular film thus is formed, which is chemically bonded to the substrate and has a thickness of about 1.5 nm.
摘要翻译：在机械部件例如齿轮或轴承的摩擦部分的表面上或游戏表面上形成具有含氟基团的表面层和通过硅氧烷键合到基材上的茎层的化学吸附膜球。因此可以获得优异的自润滑低摩擦阻力机器部件或游戏球。将由SiO 2或类似陶瓷材料制成的齿轮等的摩擦部分浸渍并保持在含有溶解在非水溶剂中的表面活性物质例如CF 3（CF 2）7（CH 2）2 ClCl 3）的溶液中。在含有碳氟化合物和氯硅烷的材料的SiCl基团和SiO 2表面上大量存在的羟基之间产生盐酸去除反应，从而形成CF 3（CF 2）7（CH 2）2 Si（O - ）在整个摩擦部分表面上。因此，形成与基板化学键合并且具有约1.5nm的厚度的含氟单分子膜。

45. 发明授权

US5681442A Method of producing an organic device 失效
标题翻译：生产有机装置的方法
公开(公告)号：US5681442A
公开(公告)日：1997-10-28
申请号：US565636
申请日：1995-11-29
申请人： Kazufumi Ogawa , Norihisa Mino
发明人： Kazufumi Ogawa , Norihisa Mino
IPC分类号： H01L51/05 , C08F38/00 , H01L21/368 , H01L51/00 , H01L51/30 , C25D9/02
CPC分类号： H01L51/0075 , H01L51/0094 , H01L51/0545 , H01L51/0036 , H01L51/0062 , Y10S428/901 , Y10T428/24917
摘要： A process for producing an organic device includes forming a first electrode and a second electrode on a substrate having an insulating film formed on a surface thereof, etching out the insulating film with the first electrode and the second electrode being used as masks, forming a monomolecular or built-up monomolecular film containing electrolytically polymerizable unsaturated groups directly or indirectly on the surface of the substrate by a chemical absorption method or the Langmuir-Blodgett method. The process further includes a procedure of spreading a surfactant containing the electrolytically polymerizable unsaturated groups on the surface of a water bath to form a monomolecular film, transferring at least one layer of the monomolecular film into the surface of the substrate, and chemically bonding molecules of the surfactant to form at least one layer of the monomolecular film of the surfactant containing electroconductive conjugated groups, applying a voltage between the first electrode and the second electrode to polymerize the electrolytically polymerizable unsaturated groups, and deriving a third electrode from the substrate such that the substrate acts as the third electrode.
摘要翻译：一种制造有机器件的方法包括：在其表面上形成有绝缘膜的基板上形成第一电极和第二电极，用第一电极和第二电极作为掩模蚀刻绝缘膜，形成单分子或通过化学吸收法或Langmuir-Blodgett法直接或间接地在基材表面上含有电解聚合性不饱和基团的单分子膜。该方法还包括将含有电解可聚合不饱和基团的表面活性剂扩散到水浴表面以形成单分子膜，将至少一层单分子膜转移到基材表面的方法，以及化学键合所述表面活性剂形成至少一层含有导电共轭基团的表面活性剂的单分子膜，在所述第一电极和所述第二电极之间施加电压以聚合所述电解聚合的不饱和基团，并从所述基板导出第三电极，衬底作为第三电极。

46. 发明授权

US5578340A Medical member and method of manufacturing the same 失效
标题翻译：医疗会员及其制造方法
公开(公告)号：US5578340A
公开(公告)日：1996-11-26
申请号：US485787
申请日：1995-06-07
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： A61L33/00 , B05D1/18 , C09D4/00 , B05D3/06 , B05D3/10 , B05D1/36
CPC分类号： B82Y30/00 , A61L33/0088 , B05D1/185 , B82Y40/00 , B82Y5/00 , C09D4/00 , Y10S623/923
摘要： A medical member having active hydrogen groups such as hydroxyl, amino or imino groups at its surface, is dipped, either directly or after formation of an inner layer on its surface, into a solution. The solution is prepared by dissolving a surface active material, e.g., CF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 SiCl.sub.3 in a non-aqueous solvent. A dehydrochlorination reaction is brought about between active hydrogen groups at the surface of the member and SiCl groups of the surface active material, thus producing bonds ofCF.sub.3 (CF.sub.2).sub.7 (CH.sub.2).sub.2 Si(O--).sub.3over the entire surface. A fluorine-containing monomolecular film is formed, which is chemically (or covalently) bonded to the member surface and has a thickness at the nanometer level. Since the chemically adsorbed film is covalently bonded to the member or inner layer, it is chemically stable and difficult to separate. Medical members can be obtained when the invention is applied to an artificial tooth, a joint, a bone, a blood bag, a catheter, a blood transportation tool, a dialysis equipment part, an operation thread, a medical implant and an operation tool.
摘要翻译：在其表面具有羟基，氨基或亚氨基的活性氢基团的医学成分在其表面上直接或内层形成后溶解成溶液。通过将表面活性物质例如CF 3（CF 2）7（CH 2）2 ClCl 3溶解在非水溶剂中来制备溶液。在成员表面的活性氢基团和表面活性材料的SiCl基团之间产生脱氯化氢反应，从而在整个表面上产生CF 3（CF 2）7（CH 2）2 Si（O-）3的键。形成化学（或共价）结合到构件表面并具有纳米级厚度的含氟单分子膜。由于化学吸附的膜共价结合到构件或内层，因此化学稳定且难以分离。当将本发明应用于人造牙齿，关节，骨骼，血袋，导管，血液输送工具，透析设备部件，手术线，医疗植入物和操作工具时，可获得医疗部件。

47. 发明授权

US5571622A Water- and oil repellent substrate and method of treatment 失效
标题翻译：拒水拒油基材和处理方法
公开(公告)号：US5571622A
公开(公告)日：1996-11-05
申请号：US309545
申请日：1994-09-20
申请人： Kazufumi Ogawa , Mamoru Soga
发明人： Kazufumi Ogawa , Mamoru Soga
IPC分类号： A61N1/365 , B05D1/18 , B05D5/08 , C09D4/00 , D06M15/657 , D06M23/00 , B32B9/00
CPC分类号： B82Y30/00 , A61N1/36514 , B05D1/185 , B82Y40/00 , C09D4/00 , D06M15/657 , D06M23/005 , B05D5/08 , Y10S428/913 , Y10T428/2918 , Y10T428/2933 , Y10T428/2962 , Y10T428/31663
摘要： A durable and extremely water- and oil repellent ultra thin film is formed on the surface of a substates such as glass, ceramics, fabrics, fur and cloth by a dehydrochlorination reaction between a functional group such as a hydroxyl group or an imino group on the surface of the substrate. The coating film of the material comprises a plurality of chlorosilyl groups was formed on the surface of the substrate by dipping and holding the substrate comprising functional groups on its surface in a solution prepared by dissolving a material comprising fluorocarbon groups and a plurality of chlorosily groups in a non-aqueous solvent and drying the substrate which is then taken out from the solution in a substantially moistureless or low moisture atmosphere and removing the non-aqueous solvent remaining on the substrate. Further, when the coating film is left in an atmosphere comprising moisture, i.e., humid air, the coating film is polymerized by a dehydrochlorination reaction between the coating film and the moisture in the atmosphere. The film is formed on the surface of the substrate containing hydroxyl groups, imino groups or carboxyl groups through --SiO-- bonds or --SiN
摘要翻译：通过在诸如羟基或亚氨基之类的官能团之间的脱氯化氢反应，在玻璃，陶瓷，织物，毛皮和布等基底的表面上形成耐久且极其防水和防油的超薄膜基板的表面。该材料的涂膜包括通过将包含官能团的基材在其表面上浸渍并保持在通过将包含氟碳基团和多个氯基团的材料溶解在其中而制备的溶液中而在基材表面上形成多个氯甲硅烷基非水溶剂并干燥基材，然后将其从基本上无水或低湿气氛中从溶液中取出并除去留在基材上的非水溶剂。此外，当涂膜保持在包含湿气的空气即潮湿的空气中时，通过涂膜和大气中的水分之间的脱氯化氢反应使涂膜聚合。该薄膜通过-SiO键或-SiN <键在含有羟基，亚氨基或羧基的基材表面上形成。

48. 发明授权

US5552236A Organic magnetic film and method of manufacturing the same 失效
标题翻译：有机磁性膜及其制造方法
公开(公告)号：US5552236A
公开(公告)日：1996-09-03
申请号：US25662
申请日：1993-03-03
申请人： Tadashi Ohtake , Norihisa Mino , Kazufumi Ogawa
发明人： Tadashi Ohtake , Norihisa Mino , Kazufumi Ogawa
IPC分类号： B05D1/18 , G11B5/62 , H01F1/42 , H01F10/00 , G11B5/66 , B05D5/12 , C09J5/02
CPC分类号： B82Y30/00 , B05D1/185 , B82Y10/00 , B82Y40/00 , G11B5/62 , H01F1/42 , H01F10/005 , H01F1/0009 , Y10S428/90
摘要： According to the invention, the surface of a substrate possessing an active hydrogen group is contacted with a chemical adsorbent containing a radical generation precursor group or metal ion capturing group within a molecule--also possessing a reactive functional group such as halosilyl or alkoxy silyl at its end--to form a chemical adsorption film by removing the unreacted chemical adsorbent, radicals are then generated and magnetism is expressed on the chemical adsorption film.
摘要翻译：根据本发明，具有活性氢基团的基材的表面在分子内与含有自由基产生前体基团或金属离子捕获基团的化学吸附剂接触，并且在其分子中也具有反应性官能团如卤代甲硅烷基或烷氧基甲硅烷基通过除去未反应的化学吸附剂形成化学吸附膜，然后产生自由基，并在化学吸附膜上表现磁性。

49. 发明授权

US5536982A Ultra thin polymer film electret 失效
标题翻译：超薄聚合物电极驻极体
公开(公告)号：US5536982A
公开(公告)日：1996-07-16
申请号：US507667
申请日：1995-07-25
申请人： Norihisa Mino , Yoshikazu Yamagata , Kazufumi Ogawa
发明人： Norihisa Mino , Yoshikazu Yamagata , Kazufumi Ogawa
IPC分类号： B29C41/12 , B29L9/00 , B29L31/34 , C08J5/18 , C08J7/00 , H01G7/02 , G11C13/02
CPC分类号： H01G7/023 , B82Y30/00 , B82Y40/00
摘要： The invention concerns an ultra thin polymer film electret comprising a polymer and a substrate having a surface electric charge, wherein a side chain of the polymer and the substrate are physically or chemically bonded. A method of manufacturing an ultra thin polymer film electret comprising: adsorbing a monomolecular film comprising a unsaturated group or a laminated film comprising the monomolecular film on to a substrate surface, irradiating the monomolecular film or the laminated film with an energy beam to polymerize the unsaturated groups and applying a high voltage to the film is also disclosed. Further, a method of manufacturing an ultra thin polymer film electret comprising: physically bonding a side chain of the polymer to a substrate surface to form a thin film and applying a high voltage to the thin film is also disclosed.
摘要翻译：本发明涉及一种包含聚合物和具有表面电荷的基底的超薄聚合物膜驻极体，其中聚合物和基底的侧链物理或化学键合。一种制造超薄聚合物膜驻极体的方法，包括：将包含不饱和基团的单分子膜或包含单分子膜的层压膜吸附到基材表面上，用能量束照射单分子膜或层压膜以聚合不饱和并且还公开了向薄膜施加高电压的组。此外，还公开了一种制造超薄聚合物膜驻极体的方法，其包括：将聚合物的侧链物理结合到基板表面以形成薄膜并向薄膜施加高电压。

50. 发明授权

US5500250A Chemically adsorbed film and method of manufacturing the same 失效
标题翻译：化学吸附膜及其制造方法
公开(公告)号：US5500250A
公开(公告)日：1996-03-19
申请号：US511912
申请日：1995-08-07
申请人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
发明人： Kazufumi Ogawa , Norihisa Mino , Mamoru Soga
IPC分类号： A61L33/00 , B05D1/18 , C09D4/00 , B05D3/00
CPC分类号： B82Y30/00 , A61L33/0088 , B05D1/185 , B82Y40/00 , B82Y5/00 , C09D4/00 , Y10T428/31544 , Y10T428/31612 , Y10T428/31699
摘要： Disclosed is an ornament with a thin film formed on the ornament surface. The thin film includes a fluorocarbon-based adsorbed monomolecular film, and the thin film is covalently bonded to the ornament. By contacting the ornament with the non-aqueous solution containing a chlorosilane group at one end and a fluorocarbon chain at the other end, a reaction occurs between hydroxyl groups at the ornament surface and the chlorosilyl groups of the material having a plurality of chlorosilyl grounds. A monomolecular film which is covalently bonded to the ornament surface is thereby obtained. A thin, fluorine-containing, monomolecular film thus can be formed on the ornament such that it is, chemically bonded to the ornament. The film is anti-contaminating, water-and oil-repelling, durable and does not spoil the intrinsic luster of the ornament.
摘要翻译：公开了一种在装饰表面上形成有薄膜的装饰品。薄膜包括氟碳基吸附单分子膜，并且该薄膜与装饰物共价键合。通过将装饰物与其一端含有氯硅烷基的非水溶液和另一端的碳氟化合物链接触，在装饰表面的羟基和具有多个氯代甲硅烷基的材料的氯甲硅烷基之间发生反应。由此获得共价键合到装饰表面的单分子膜。因此，可以在装饰品上形成薄的含氟单分子膜，使其与装饰物化学结合。该胶片具有防污，防水，防油，耐用，不会破坏装饰品的内在光泽。

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