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41. 发明专利

JPS6297887A TRANSFER-TYPE THERMAL RECORDING METHOD 失效
公开(公告)号：JPS6297887A
公开(公告)日：1987-05-07
申请号：JP23865185
申请日：1985-10-24
申请人： MITSUBISHI ELECTRIC CORP
发明人： ENMANJI KIMIE , NOMURA KENJI
IPC分类号： B41M5/124 , B41M5/40
摘要： PURPOSE:To achieve transfer-type thermal recording to give gradated full-color stable images, by a method wherein a sublimable dye of a transfer-type thermal recording sheet is thermally transferred to a transfer-type thermal recording medium by heating, and amino groups of the dye and glycidyl groups of the recording medium are brought into reaction with each other to fix the transferred dye. CONSTITUTION:A transfer-type thermal recording sheet 8 is obtained by coating a shielding film 2 with a binder 3 containing a sublimable dye 4 having an amino group dispersed therein, whereas a transfer-type thermal recording medium 9 is obtained by coating a base 6 with a resin material having glycidyl groups. When the binder 3 is heated by a thermal head 1 through the film 2, the sublimable dye 4 having the amino group is sublimed, and reacts with the resin material 7 having the glycidyl group, whereby the dye is fixed. In addition to the heating by the thermal head, the recording medium may be heated by a heated roll, a flash lamp or the like after recording, whereby the above reaction can be made to proceed sufficiently.

42. 发明专利

JPS6121184A Preparation of water-soluble anstioxidant 失效
标题翻译：水溶性抗氧化剂的制备
公开(公告)号：JPS6121184A
公开(公告)日：1986-01-29
申请号：JP14145684
申请日：1984-07-10
申请人： Mitsubishi Electric Corp
发明人： ENMANJI KIMIE , YAMAGUCHI HIROYUKI
IPC分类号： C09K15/06 , C07D311/72 , C08B37/16
摘要： PURPOSE: To obtain a water-soluble antioxidant having high oxidation prevention ability, by bringing a water-insoluble tocopherol into contact with cyclodextrin under specific conditions, so that tocopherol is included in cyclodextrin.
CONSTITUTION: For example, cyclodextrin is packed into a column, tocopherol is dissolved in a solvent such as ethyl ether, etc. to dissolve only tocopherol, made to flow into the column, then, cyclodextrin is taken out, and the colvent is removed to give the aimed antioxidant wherein tocopherol is included in cyclodextrin.
USE: An inhibitor for fading of water-soluble dye, an inhibitor for deterioration of water-soluble plastic.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了获得具有高氧化防止能力的水溶性抗氧化剂，通过在特定条件下使水不溶性生育酚与环糊精接触，使得生育酚被包括在环糊精中。构成：例如，将环糊精填充到柱中，将生育酚溶于乙醚等溶剂中，仅溶解生育酚，使其流入柱中，取出环糊精，取出溶菌液给出其中生育酚包括在环糊精中的目标抗氧化剂。用途：水溶性染料的褪色抑制剂，水溶性塑料的劣化抑制剂。

43. 发明专利

JPS6119605A Production of water-soluble photopolymerization initiator 失效
标题翻译：生产水溶性光聚合引发剂
公开(公告)号：JPS6119605A
公开(公告)日：1986-01-28
申请号：JP14081984
申请日：1984-07-05
申请人： Mitsubishi Electric Corp
发明人： ENMANJI KIMIE , ANDOU TORAHIKO
IPC分类号： C08F2/00 , C07C45/00 , C07C49/84 , C07C67/00 , C08F2/50 , G01N27/30 , G01N27/327
摘要： PURPOSE: To obtain a water-soluble photopolymerization inititor which has excellent reproducibility and does not suffer decrease in polymerization initiating ability, by dissolving a photopolymerization initiator in a solvent which can not dissolve cyclodextrin and passing this solution through a column packed with cyclodextrin.
CONSTITUTION: A photopolymerization initiator is dissolved in a solvent which can dissolve the initiator but can no dissolve cyclodextrin. This solution is passed through a columnm packed with cyclodextrin, and this cyclodextrin is withdrawn and dried. Examples of the cyclodextrins which can be applied include α-, β- and γ-cyclodextrins. Examples of the photopolymerization initiators include benzoin and benzoin ethyl ether. Examples of the solvents used include ethyl ether, dichloroethane and chloroform. The amount of the cyclodextrin with which the column is packed is preferably about 10W1,000mol per mol of the photopolymerization initiator passed in the form of a solution, though it varies with the particle diameter of the cyclodextrin used, etc.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：通过将光聚合引发剂溶解在不溶于环糊精的溶剂中并使该溶液通过填充有环糊精的柱，获得具有优异的再现性和聚合引发能力降低的水溶性光聚合引发剂。构成：将光聚合引发剂溶解在可溶解引发剂但不溶解环糊精的溶剂中。将该溶液通过填充有环糊精的柱，并将该环糊精取出并干燥。可以应用的环糊精的实例包括α-，β-和γ-环糊精。光聚合引发剂的实例包括苯偶姻和苯偶姻乙醚。使用的溶剂的实例包括乙醚，二氯乙烷和氯仿。尽管随着所使用的环糊精的粒径而变化，但柱的填充量的环糊精的量优选为溶液形式通过的每摩尔光聚合引发剂约10-1,000mol。

44. 发明专利

JPS6119603A Production of water-soluble photopolymerization initiator 失效
标题翻译：生产水溶性光聚合引发剂
公开(公告)号：JPS6119603A
公开(公告)日：1986-01-28
申请号：JP13983584
申请日：1984-07-04
申请人： Mitsubishi Electric Corp
发明人： ENMANJI KIMIE , ANDOU TORAHIKO
IPC分类号： C08F2/00 , C07C45/00 , C07C49/84 , C07C67/00 , C08F2/50 , G01N27/30 , G01N27/327
摘要： PURPOSE: To obtain the titled initiator which has excellent reproducibility and does not suffer decrease in polymerization initiation ability, by dissolving a photopolymerization initiator and cyclodextrin in solvents each of which can dissolve only one of the compounds and mixing both of the solutions together while evaporating the solvent for the former compound.
CONSTITUTION: A photopolymerization initiator and cyclodextrin are dissolved in solvents each of which can dissolve only one of the compounds. Both of the resulting solutions are mixed together while the solvent which can dissolve only the photopolymerization initiator is being evaporated. Examples of the cyclodextrins which can be applied include α-, β- and γ-cyclodextrins. Examples of the photopolymerization initiators include benzoin, benzoin ethyl ether and benzophenone. Examples of the solutions which can dissolve only the photopolymerization initiator include ethyl ether and chloroform. Examples of the solvents which can dissolve only cyclodextrin include water and glycerin.
COPYRIGHT: (C)1986,JPO&Japio
摘要翻译：目的：为了获得具有优异的再现性并且不会降低聚合引发能力的标题引发剂，通过将光聚合引发剂和环糊精溶解在溶剂中，每种溶剂仅溶解一种化合物并将两种溶液混合在一起，同时蒸发前者化合物的溶剂。构成：将光聚合引发剂和环糊精溶解在溶剂中，只能溶解一种化合物。将所得到的溶液混合在一起，而仅溶解光聚合引发剂的溶剂被蒸发。可以应用的环糊精的实例包括α-，β-和γ-环糊精。光聚合引发剂的实例包括苯偶姻，苯偶姻乙醚和二苯甲酮。仅溶解光聚合引发剂的溶液的实例包括乙醚和氯仿。仅溶解环糊精的溶剂的实例包括水和甘油。

45. 发明专利

JPS616885A Pigment q switch for neodymium laser 失效
标题翻译：颜料激光开关
公开(公告)号：JPS616885A
公开(公告)日：1986-01-13
申请号：JP12641084
申请日：1984-06-21
申请人： Mitsubishi Electric Corp
发明人： ENMANJI KIMIE , ETOU SHIYOUHEI
IPC分类号： H01S3/113
CPC分类号： H01S3/113
摘要： PURPOSE:To prevent the attack of radicals, and to obtain optical bleaching resistance by inserting a dithiolate complex group pigment among bases in deoxyribonucleic acid DNA and forming a dithiolate complex group pigment/DNA complex. CONSTITUTION:A dithiolate complex/deoxyribonucleic acid complex, in which a dithiolate complex group pigment is inserted among base pairs in deoxyribonucleic acid, or a dithiolate complex group pigment/caffeine complex having sandwich structure in which the dithiolate group pigment is held among caffiene of two molecules is used. Consequently, the attack of radicals can be prevented. The attack of radicals will be obviated for the reason that the dithiolate complex group pigment 2 is probably inserted between base pairs 3 (A represents adenine, C cytosine, G guanine, T thymine and 1 a nucleic acid phosphoric acid group) arranged in parallel and a radical generating agent cannot easily approach to the dithiolate complex group pigment 2 in the dithiolate complex group pigment/DNA complex.
摘要翻译：目的：为了防止自由基的侵袭，并通过在脱氧核糖核酸DNA的碱基中插入二硫醇复合基色素并形成二硫醇盐复合物色素/ DNA复合物来获得光学耐漂白性。构成：二脱硫酸复合体/脱氧核糖核酸复合物，其中在脱氧核糖核酸的碱基对之间插入二硫醇酸复合基团颜料，或具有夹心结构的二硫醇盐复合群颜料/咖啡因络合物，其中二硫醇基颜料保持在二氯化碳分子被使用。因此，可以防止自由基的攻击。由于二极性复合基团颜料2可能插入平行布置的碱基对3（A代表腺嘌呤，C胞嘧啶，G鸟嘌呤，T胸腺嘧啶和1核酸磷酸基）的原因，因此可以消除自由基的攻击，自由基产生剂不容易接近二硫醇酸复合基团颜料/ DNA复合物中的二硫醇盐复合基团颜料2。

46. 发明专利

JPS613792A ELECTROLYTIC RECORDING PAPER 失效
公开(公告)号：JPS613792A
公开(公告)日：1986-01-09
申请号：JP12685884
申请日：1984-06-18
申请人： MITSUBISHI ELECTRIC CORP
发明人： ENMANJI KIMIE , ETOU SHIYOUHEI
IPC分类号： B41M5/20
摘要： PURPOSE:To prevent the alteration after fixing, by providing a conductive layer showing the compatibility with a meltable layer under heating and a color forming layer containing a solid electrolyte and a redox dye. CONSTITUTION:A meltable layer 6 melted under heating, a conductive layer 2 showing the compatibility with the meltable layer and a color forming layer 1 containing a solid electrolyte and a redox dye are provided to a support. When pulse voltage is applied between a recording needle 4 and a return electrode 5, a current flows in the route of color forming layer 1 conductive layer 2 return electrode 5 and the dye in the color forming layer 1 develops a color by electrolytic oxidation or reduction. After the completion of recording, the whole of recording paper is heated to melt and mix the conductive layer 2 and the meltable layer 6 having compatibility to each other. The meltable layer 6 is formed so as to be sufficiently thick as compared with the conductive layer 2 and the conductive substance in the conductive layer 2 is diluted by mixing and the current sufficient for inducing the electrolysis of the color forming layer 1 does not flow any longer.

47. 发明专利

JPS60235132A FORMATION OF PATTERN 失效
公开(公告)号：JPS60235132A
公开(公告)日：1985-11-21
申请号：JP9204284
申请日：1984-05-07
申请人： MITSUBISHI ELECTRIC CORP
发明人： ENMANJI KIMIE , ETOU SHIYOUHEI
IPC分类号： G03F7/30 , G03C1/00 , G03C1/73 , G03C5/00 , G03F7/004 , G03F7/26 , G03F7/38
摘要： PURPOSE:To obtain a good pattern by forming a polythymidylic acid layer on a base, forming an image by exposing it io UV rays, and decomposing the unexposed parts with a nucleic acid decomposing enzyme to remove them. CONSTITUTION:The polythymidylic acid (...T-T-T-T...) layer 2 is formed on the base 1, patternwisely, exposed to UV rays 3 to dimerize (T-T) the thymine residues, the unexposed acid is decomposed with the nucleic acid decomposing enzyme, and the enzyme is deactivated. The acid decomposed with the enzyme is removed with an acid to form a desired pattern (T-T-T-T) on the base 1. As said nucleic acid decomposing enzyme, pancreatic deoxyribonuclease I is, preferably, used. As a result, a superior negative type pattern can be obtained and used for formation of resist patterns of LSI, etc.

48. 发明专利

JPS60210495A Transfer-type thermal recording sheet 失效
标题翻译：转印式热记录片
公开(公告)号：JPS60210495A
公开(公告)日：1985-10-22
申请号：JP6826184
申请日：1984-04-05
申请人： Mitsubishi Electric Corp
发明人： ENMANJI KIMIE , ETOU SHIYOUHEI
IPC分类号： B41M5/392 , B41J31/00 , B41M5/26 , B41M5/382
CPC分类号： B41M5/38207
摘要： PURPOSE:To prevent a dye from being transferred to a recording medium at room temperature and enhance resolution and sensitivity, by providing a water-soluble resin material with a sealing film for preventing a water-soluble resin material from leaking on the side faced to a thermal head. CONSTITUTION:The water-soluble resin material 7 obtained by dispersing a dye-containing liposome 6 in a water-soluble resin is provided with the sealing film 2 for preventing the material 7 from leaking on the side faced to a thermal head. The dye is isolated by the liposome 6 at room temperature, but when the sheet is heated from above the sealing film 1, the liposome 6 is melted, and a portion of the dye 3 is melted or sublimed to exude onto a transfer-type thermal recording medium, thereby recording. The liposome has a bimolecular-film consruction formed by association of a long- chain dialkyldimethylammonium salt and a phase transition temperature of Tc, and maintains the bimolecular-film costruction at temperatues not higher than Tc. At temperatures not lower than Tc. a phase transition occurs to make the liposome fluidic, so that a hydrophobic substance taken therein is released. The sealing film is a polymer film, a condenser paper or the like. Accordingly, a sheet free of transfer of a dye to a recording medium at room temperature and having excellent resolution and sensitivity can be obtained.
摘要翻译：目的：为了防止染料在室温下转印到记录介质中并提高分辨率和灵敏度，通过提供具有密封膜的水溶性树脂材料，以防止水溶性树脂材料在面向热头。构成：通过将含染料的脂质体6分散在水溶性树脂中而获得的水溶性树脂材料7设置有用于防止材料7在面向热敏头的一侧泄漏的密封膜2。染料在室温下由脂质体6分离，但是当从密封膜1上方加热片材时，脂质体6被熔化，并且一部分染料3被熔化或升华以渗透到转印型热记录介质，从而进行记录。脂质体具有通过长链二烷基二甲基铵盐和Tc的相变温度的关联形成的双分子膜引发剂，并且在不高于Tc的温度下保持双分子膜辅助。在不低于Tc的温度下。发生相变以使脂质体流体化，使得其中吸收的疏水性物质被释放。密封膜是聚合物膜，冷凝纸等。因此，可以获得没有在室温下将染料转移到记录介质并具有优异的分辨率和灵敏度的片材。

49. 发明专利

JPS60199694A THERMAL RECORDING MEDIUM AND THERMAL RECORDING METHOD 失效
公开(公告)号：JPS60199694A
公开(公告)日：1985-10-09
申请号：JP5672484
申请日：1984-03-23
申请人： MITSUBISHI ELECTRIC CORP
发明人： ENMANJI KIMIE , ETOU SHIYOUHEI
IPC分类号： B41M5/382 , B41J31/00 , B41M5/26
摘要： PURPOSE:To markedly enhance stability of recording, by a method wherein a material comprising DNA and a hygroscopic agent infiltrated in a nitrocellulose support having micropores is used, and is heated. CONSTITUTION:The nitrocellulose support 1 having micropores 2 is impregnated with a hygroscopic agent 4 and DNA3, and when the support is heated, the DNA is converted into one-chain DNA only at the heated parts, and the one-chain DNA is firmly adsorbed onto the support 1. When the support 1 is washed with water, only the parts of two-chain DNA which have not been heated are washed away. When the support 1 in this state is immersed in a solution of ethidium bromide or porphyrin, the dye and the one-chain DNA form a strong bond, resulting in dyeing, and then the support 1 is washed with water, whereby a recorded state can be obtained. The hygroscopic agent 4 may be lithium chloride, calcium bromide, magnesium chloride, copper chloride or sodium iodide.

50. 发明专利

JPS60187592A TRANSFER-TYPE THERMAL RECORDING SHEET 失效
公开(公告)号：JPS60187592A
公开(公告)日：1985-09-25
申请号：JP4252384
申请日：1984-03-06
申请人： MITSUBISHI ELECTRIC CORP
发明人： ENMANJI KIMIE , ETOU SHIYOUHEI , KUSAKAWA HIDEAKI
IPC分类号： B41M5/392 , B41M5/00 , B41M5/26 , B41M5/385 , B41M5/388 , B41M5/395 , B41M5/40 , B41M5/44 , B41M5/52
摘要： PURPOSE:To easily transfer with favorable sensitivity and enable to repeat transferring, by a method wherein a dye transfer type thermal recording sheet is provided with a sealing film for preventing a water-soluble resin material from leaking. CONSTITUTION:The transfer-type thermal recording sheet 4 comprises a water- soluble resin material 6 obtained by dispersing a dye having a melting point of not higher than 140 deg.C in a water-soluble resin and the sealing film 1 provided on the resin material 6 on the side faced to a thermal head so as to prevent the resin material 6 from leaking. When the sheet 4 is heated from the upper side of the sealing film 1, a portion of the dye contained in the resin material 6 is melted, and exudes through minute pores of the resin material 6 onto a recording paper, thereby performing recording. The water-soluble resin may be casein, gelatine, denatured starch or the like. The dye may be an anthraquinone or azo- disperse dye. The sealing film may consists of a polymer film or a condenser paper.

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