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41. 发明授权

US09363997B2 Methods and compositions for the generation of peracetic acid on site at the point-of-use 有权
标题翻译：在使用时在现场产生过乙酸的方法和组合物
公开(公告)号：US09363997B2
公开(公告)日：2016-06-14
申请号：US14681938
申请日：2015-04-08
申请人： Michael S. Harvey , Jonathan N. Howarth
发明人： Michael S. Harvey , Jonathan N. Howarth
IPC分类号： A61K31/19 , A01N37/16 , C11D3/39 , C11D11/00 , A01N59/00 , C11D3/395 , D06L3/02
CPC分类号： A01N37/16 , A01N37/12 , A01N59/00 , B01J19/24 , B01J2219/24 , C11D3/3947 , C11D3/3955 , C11D3/3956 , C11D11/0041 , D06L4/15 , A01N37/02 , A01N2300/00
摘要： Methods for the generation of non-equilibrium solutions of peroxyacetic acid are disclosed. These methods comprise introducing triacetin sad aqueous hydrogen peroxide to water, mixing, and then adding an aqueous source of an alkali metal or earth alkali metal hydroxide. Triacetin is converted rapidly and with a high conversion rate into peracetic acid. These methods produce solutions with a high level of peracetic acid.
摘要翻译：公开了产生过氧乙酸的非平衡溶液的方法。这些方法包括将三醋酸甘油难溶性过氧化氢引入水中，混合，然后加入碱金属或碱土金属氢氧化物的水源。三醋酸甘油酯快速转化并以高转化率转化成过乙酸。这些方法产生具有高水平过乙酸的溶液。

42. 发明授权

US08574605B2 Methods for the preparation of concentrated aqueous bromine solutions and high activity bromine-containing solids 有权
标题翻译：制备浓缩溴水溶液和高活性含溴固体的方法
公开(公告)号：US08574605B2
公开(公告)日：2013-11-05
申请号：US11975499
申请日：2007-10-19
申请人： Jonathan N. Howarth , Michael S. Harvey
发明人： Jonathan N. Howarth , Michael S. Harvey
IPC分类号： A61K33/00 , A61K33/04 , A61K33/14 , A61K33/40 , A01N25/02 , A01N59/00 , A01N59/02 , A01N59/08 , A01N39/00
CPC分类号： A01N59/00 , A01N59/02 , A01N2300/00
摘要： The invention includes convenient methods of preparing: (1) highly concentrated liquid bromine-containing biocidal solutions, (2) highly concentrated mixed halogen liquid bromine and chlorine-containing biocidal solutions, and (3) high-activity bromine-containing biocidal solids, all having excellent physical and chemical stability. One method yields solutions that have concentrations of bromine in excess of 18% as Br2 (8% as Cl2) in which the mole ratio of hydroxide ion to hydrogen ion source is at least 1.9:1. Another method employs elemental bromine in conjunction with a solid organic or inorganic halogenating agent to yield halogen solutions at concentrations greater than 22.9% as Br2 (10.2% as Cl2). This method can be performed under conditions that exceed the solubility of the active ingredient such that it crystallizes and is recovered as a hydrated or anhydrous salt in good yield.
摘要翻译：本发明包括制备方便的方法：（1）高浓度液体含溴杀生物溶液，（2）高度浓缩的混合卤素液体溴和含氯杀生物溶液，和（3）高活性含溴杀生物固体，全部具有良好的物理和化学稳定性。一种方法产生具有溴离子浓度超过18％的溶液，其中氢离子与氢离子源的摩尔比至少为1.9:1，Br2（8％为Cl2）。另一种方法是使用元素溴与固体有机或无机卤化剂结合产生浓度大于22.9％的卤素溶液作为Br 2（10.2％为Cl 2）。该方法可以在超过活性成分的溶解度的条件下进行，使其结晶并作为水合或无水盐以良好的收率回收。

43. 发明授权

US08546449B2 Methods and compositions for the generation of peracetic acid on site at the point-of-use 有权
标题翻译：在使用时在现场产生过乙酸的方法和组合物
公开(公告)号：US08546449B2
公开(公告)日：2013-10-01
申请号：US13065553
申请日：2011-03-24
申请人： Michael S. Harvey , Jonathan N. Howarth
发明人： Michael S. Harvey , Jonathan N. Howarth
IPC分类号： A61K31/19
CPC分类号： A01N37/16 , A01N37/12 , A01N59/00 , B01J19/24 , B01J2219/24 , C11D3/3947 , C11D3/3955 , C11D3/3956 , C11D11/0041 , D06L4/15 , A01N37/02 , A01N2300/00
摘要： Methods and compositions for the generation of a peroxyacetic acid sanitizer in proximity to the point-of-use are disclosed. These methods comprise introducing a hydrogen peroxide-acetyl precursor solution to water, mixing, and then adding an aqueous source of a alkali metal or earth alkali metal hydroxide. Triacetin is a preferred acetyl precursor and is converted rapidly and with a high conversion rate into peracetic acid. These methods produce solutions with a high level of peracetic acid. Methods for preparing the hydrogen peroxide-acetyl precursor solution are also provided. Also disclosed are solid compositions comprising a liquid acetyl precursor, a water-soluble source of hydrogen peroxide, and a water-soluble source of alkalinity. The solid composition is a freely-flowable solid that is used as a bleaching agent and a stain remover for the treatment of articles such as fabrics, dentures, textile garments, and equipment used in the food and beverage industry.
摘要翻译：公开了在使用点附近产生过氧乙酸消毒剂的方法和组合物。这些方法包括将过氧化氢 - 乙酰基前体溶液引入水中，混合，然后加入碱金属或碱土金属氢氧化物的水源。三醋精是优选的乙酰基前体，并迅速转化并以高转化率转化成过乙酸。这些方法产生具有高水平过乙酸的溶液。还提供了制备过氧化氢 - 乙酰前体溶液的方法。还公开了固体组合物，其包含液体乙酰基前体，水溶性过氧化氢源和水溶性碱度源。固体组合物是可自由流动的固体，其用作漂白剂和用于处理食品和饮料工业中使用的织物，假牙，纺织品衣服和设备的制品的去污剂。

44. 发明申请

US20110200685A1 Methods and compositions for the reduction of pathogenic microorganisms from meat and poultry carcasses, trim and offal 审中-公开
标题翻译：用于从肉和家禽屠体，修剪和内脏减少病原微生物的方法和组合物
公开(公告)号：US20110200685A1
公开(公告)日：2011-08-18
申请号：US12925301
申请日：2010-10-19
申请人： Michael S. Harvey , Jonathan N. Howarth , Courtney E. Mesrobian
发明人： Michael S. Harvey , Jonathan N. Howarth , Courtney E. Mesrobian
IPC分类号： A01N59/00 , A01P1/00
CPC分类号： A01N59/00 , A22B5/0082 , A22C21/0061 , C02F1/76 , C02F1/766 , C02F2103/22 , C11D3/3956 , C11D3/48 , C11D11/0023 , C11D11/0041 , A01N25/22
摘要： The invention includes a method of preparing hypochlorite-activated solutions of hypobromous acid and/or hypobromite ion. The method includes the steps of mixing a solution of a source of bromide ion with a solution of a source of hypochlorite ion to activate the bromide ion, allowing sufficient time to maximize the activation of the bromide ion, and storing the solution before use. The invention also includes a method of using the solution to wash meat and poultry carcasses, trim, and offal to reduce pathogenic microorganisms. The solutions may also be used to reduce pathogenic microorganisms in industrial cooling water and on food contact hard surfaces and equipment. The solutions may be stored for up to about three hours before use and are stable for that period of time.
摘要翻译：本发明包括制备次溴酸和/或次溴酸根离子的次氯酸盐活化溶液的方法。该方法包括以下步骤：将溴离子源的溶液与次氯酸根离子的溶液混合以活化溴离子，允许足够的时间使溴离子的活化最大化，并在使用前储存溶液。本发明还包括使用该溶液洗涤肉和家禽屠体，修剪和内脏以减少致病微生物的方法。解决方案也可用于减少工业冷却水中的病原微生物和食物接触硬表面和设备。解决方案可能在使用前储存长达约三个小时，并且在该时间段内是稳定的。

45. 发明授权

US07309503B2 Methods for the preparation of concentrated aqueous bromine solutions and high activity bromine-containing solids 有权
标题翻译：制备浓缩溴水溶液和高活性含溴固体的方法
公开(公告)号：US07309503B2
公开(公告)日：2007-12-18
申请号：US10843030
申请日：2004-05-10
申请人： Jonathan N. Howarth , Michael S. Harvey
发明人： Jonathan N. Howarth , Michael S. Harvey
IPC分类号： A61K33/00 , A61K33/04 , A61K33/14 , A61K33/40 , A01N59/00 , A01N59/02 , A01N59/08 , A01N39/00
CPC分类号： A01N59/00 , A01N59/02 , A01N2300/00
摘要： The invention includes convenient methods of preparing: (1) highly concentrated liquid bromine-containing biocidal solutions, (2) highly concentrated mixed halogen liquid bromine and chlorine-containing biocidal solutions, and (3) high-activity bromine-containing biocidal solids, all having excellent physical and chemical stability. One method yields solutions that have concentrations of bromine in excess of 18% as Br2 (8% as Cl2) in which the mole ratio of hydroxide ion to hydrogen ion source is at least 1.9:1. Another method employs elemental bromine in conjunction with a solid organic or inorganic halogenating agent to yield halogen solutions at concentrations greater than 22.9% as Br2 (10.2% as Cl2). This method can be performed under conditions that exceed the solubility of the active ingredient such that it crystallizes and is recovered as a hydrated or anhydrous salt in good yield.
摘要翻译：本发明包括制备方便的方法：（1）高浓度液体含溴杀生物溶液，（2）高度浓缩的混合卤素液体溴和含氯杀生物溶液，和（3）高活性含溴杀生物固体，全部具有良好的物理和化学稳定性。一种方法产生具有超过18％的溴浓度的溶液，其中氢离子与氢离子源的摩尔比为Br 2 Cl 2（8％作为Cl 2 H 2）至少为1.9：1。另一种方法是使用元素溴与固体有机或无机卤化剂结合产生浓度大于22.9％的卤素溶液作为Br 2（10.2％为Cl 2 H 2）。该方法可以在超过活性成分的溶解度的条件下进行，使其结晶并作为水合或无水盐以良好的收率回收。

46. 发明授权

US06965035B1 Compacted forms of halogenated hydantoins 失效
标题翻译：压缩形式的卤代乙内酰脲
公开(公告)号：US06965035B1
公开(公告)日：2005-11-15
申请号：US10202954
申请日：2002-07-25
申请人： Jonathan N. Howarth , Bruce C. Peters
发明人： Jonathan N. Howarth , Bruce C. Peters
IPC分类号： A01N25/12 , A01N43/50 , C07D233/86
CPC分类号： A01N25/12 , Y02P20/582 , A01N59/00 , A01N43/50
摘要： This invention provides a method of producing granules. This method comprises roll compaction of a 1,3-dihalo-5,5-dimethylhydantoin/binder blend, followed by feeding the compacted product obtained from the roll compactor into a mechanical device, where the compacted product is broken into granules. The blend comprises (i) at least one powdery or finely-divided 1,3-dihalo-5,5-dialkylhydantoin in which each halogen atom is either chlorine or bromine, in which one of the alkyl groups in the 5-position is a methyl group, in which the other alkyl group in the 5-position has in the range of 1 to 4 carbon atoms, and in which the particle size is larger than about 20 microns, and (ii) a binder quantity of a micronized synthetic polyolefin-based hydrocarbon wax. The binder quantity of wax is in the range of about 0.5 to about 2 wt %, based on the total weight of the 1,3-dihalo-5,5-dialkylhydantoin and the wax. The granules are produced at an increased granulation productivity in comparison to granules of the same 1,3-dihalo-5,5-dialkylhydantoin produced without a binder.
摘要翻译：本发明提供一种生产颗粒的方法。该方法包括1,3-二卤代-5,5-二甲基乙内酰脲/粘合剂混合物的辊压，然后将从辊压机获得的压实产物进料到机械装置中，其中压实产物被破碎成颗粒。共混物包含（i）至少一种粉末状或细分散的1,3-二卤代-5,5-二烷基乙内酰脲，其中每个卤素原子为氯或溴，其中5-位中的一个烷基为甲基，其中5位中的另一个烷基具有1至4个碳原子的范围，并且其中粒径大于约20微米，和（ii）微粉化合成聚烯烃的粘合剂量的烃蜡。基于1,3-二卤代-5,5-二烷基乙内酰脲和蜡的总重量，蜡的粘合剂量在约0.5至约2重量％的范围内。与不含粘合剂的相同的1,3-二卤代-5,5-二烷基乙内酰脲的颗粒相比，颗粒以更高的造粒生产率生产。

47. 发明授权

US06680070B1 Particulate blends and compacted products formed therefrom, and the preparation thereof 失效
标题翻译：由此形成的颗粒状混合物和压实产物及其制备
公开(公告)号：US06680070B1
公开(公告)日：2004-01-20
申请号：US09487816
申请日：2000-01-18
申请人： Jonathan N. Howarth , Bruce C. Peters
发明人： Jonathan N. Howarth , Bruce C. Peters
IPC分类号： A61K910
CPC分类号： A61K31/4166 , A01N25/34 , A01N59/00 , A61K9/2022 , A61K9/2027 , A61K31/192 , A61K31/402 , A61K31/403 , A01N2300/00
摘要： The dry blends comprise a powdery or finely-divided active ingredient such as a pharmaceutical, dietary supplement, agricultural chemical, water-treating agent or biocidal agent, and a micronized synthetic polyolefin-based hydrocarbon wax and/or a micronized synthetic polyfluorocarbon wax that is compatible with the active ingredient. Shape-retentive compacted compositions are formed by pressure compacting such blends. Preferred active ingredients are 1,3-dihalo-5,5-dialkylhydantoins and profen pharmaceuticals such as naproxen.
摘要翻译：干混合物包含粉末状或微细分散的活性成分如药物，膳食补充剂，农用化学品，水处理剂或杀生物剂，以及微粉化合成聚烯烃基烃蜡和/或微粉化合成多氟碳蜡，其为与活性成分相容。形状保持性压实组合物通过压制这种共混物形成。优选的活性成分是1,3-二卤代-5,5-二烷基乙内酰脲和普通药物如萘普生。

48. 发明授权

US5641520A Halogen compositions for water treatment 失效
标题翻译：用于水处理的卤素组合物
公开(公告)号：US5641520A
公开(公告)日：1997-06-24
申请号：US486136
申请日：1995-06-07
申请人： Jonathan N. Howarth , Enrico J. Termine , Alan M. Yeoman
发明人： Jonathan N. Howarth , Enrico J. Termine , Alan M. Yeoman
IPC分类号： A01N59/00 , C01B11/04 , C01B11/20 , C02F1/50 , C02F1/76 , A01N43/50
CPC分类号： C02F1/766 , A01N59/00 , C01B11/04 , C01B11/20 , C02F1/50 , C02F1/76 , C02F2103/023 , C02F2103/42
摘要： A method for providing aqueous solutions of HOBr or HOCl which includes adding bleach (NaOCl) to a solution of HBr or HCl an identified absorbance or color change in the resulting solution is detected. Dialkylhydantoins are optionally added to the resulting solution to suppress the formation of halate ions. The method provides a simple and reliable method for producing accurately defined solutions of hypohalous acids, which are useful in a variety of ways, including for disinfecting, cleaning, and odor control purposes.
摘要翻译：提供HOBr或HOCl的水溶液的方法，其包括向HBr或HCl的溶液中加入漂白剂（NaOCl），在所得溶液中检测出吸光度或颜色变化。任选将二烷基乙内酰脲加入到所得溶液中以抑制卤酸根离子的形成。该方法提供了一种用于产生准确定义的次卤酸溶液的简单可靠的方法，其可以以各种方式有用，包括用于消毒，清洁和气味控制目的。

49. 发明授权

US5607619A Inorganic perbromide compositions and methods of use thereof 失效
标题翻译：无机溴化物组合物及其使用方法
公开(公告)号：US5607619A
公开(公告)日：1997-03-04
申请号：US479837
申请日：1995-06-07
申请人： Ahmad Dadgar , Jonathan N. Howarth , Rodney H. Sergent , Nicolai A. Favstritsky , Julie A. McKeown , Dennis W. Borden , Brent M. Sanders , Jane Likens
发明人： Ahmad Dadgar , Jonathan N. Howarth , Rodney H. Sergent , Nicolai A. Favstritsky , Julie A. McKeown , Dennis W. Borden , Brent M. Sanders , Jane Likens
IPC分类号： C01B7/09 , C01B9/04 , C22B3/10 , C22B3/42 , C25B1/24 , C25C1/20 , C22B11/00 , C22B15/00
CPC分类号： C25B1/24 , C01B7/09 , C01B9/04 , C22B11/04 , C22B3/10 , C22B3/42 , C25C1/20 , Y02P10/234
摘要： A process for leaching gold, silver, platinum and palladium wherein an aqueous leaching solution containing bromine and bromide ion contacts a precious metal source to produce an aqueous leachate. A precursor composition for producing an aqueous leaching solution for leaching gold, silver, platinum and palladium. A process for electrogenerating bromine and a process for leaching gold, silver, platinum and palladium wherein bromine is electrogenerated and contacts a precious metal source to produce an aqueous leachate. A process for leaching gold, silver, platinum and palladium wherein bromine is electrogenerated from a solution containing chloride ions and bromide ions.
摘要翻译：一种用于浸出金，银，铂和钯的方法，其中含有溴和溴离子的含水浸出溶液接触贵金属源以产生含水浸出液。一种用于生产用于浸出金，银，铂和钯的水性浸出溶液的前体组合物。一种用于电生溴的方法和一种用于浸出金，银，铂和钯的方法，其中溴被电生并接触贵金属源以产生含水浸出液。一种浸出金，银，铂和钯的方法，其中溴由含有氯离子和溴离子的溶液电生成。

50. 发明授权

US5385650A Recovery of bromine and preparation of hypobromous acid from bromide solution 失效
标题翻译：从溴溶液中回收溴并制备次溴酸
公开(公告)号：US5385650A
公开(公告)日：1995-01-31
申请号：US56858
申请日：1993-04-30
申请人： Jonathan N. Howarth , Ahmad Dadgar , Rodney H. Sergent
发明人： Jonathan N. Howarth , Ahmad Dadgar , Rodney H. Sergent
IPC分类号： C02F1/76 , C25B1/22 , C25B1/24 , C25B9/06
CPC分类号： C25B1/24 , C02F1/766 , C25B1/22 , C25B9/06
摘要： A process for recovering bromine from an acidic solution containing bromide ion. Electric current is passed through the acidic solution between an anode and a cathode, thereby generating bromine by electrolysis at the anode to produce an electrolyzate containing bromine. Bromine is separated from the electrolyzate as a vapor under negative pressure. The bromide ion solution may be contaminated with organic material. An electrolytic process for producing a hypobromous acid solution. An electrolytic cell.
摘要翻译：从含有溴离子的酸性溶液中回收溴的方法。电流通过阳极和阴极之间的酸性溶液，从而通过在阳极电解产生溴以产生含溴的电解液。溴作为负压下的蒸气与电解液分离。溴离子溶液可能被有机物质污染。用于生产次溴酸溶液的电解方法。电解池。

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