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    • 44. 发明授权
    • Nondestructive device and method for evaluating ultra-hard polycrystalline constructions
    • 非破坏性设备和超硬多晶结构评估方法
    • US08130903B2
    • 2012-03-06
    • US12567613
    • 2009-09-25
    • Loel CorbettRonald K. Eyre
    • Loel CorbettRonald K. Eyre
    • G01N23/223
    • E21B10/567G01N23/223G01N2223/076G01N2223/652G01T1/00
    • A device, system and method for nondestructively obtaining qualitative and/or quantitative information relating to the material properties of a region in a diamond body comprises directing x-rays onto the body. The body can comprise sintered or unsintered diamond. The body can ultimately be in the form of a cutting element used with a subterranean drill bit. The x-rays penetrate the body and cause a target element within the desired region including the same to emit x-ray fluorescence. The emitted x-ray fluorescence is received and information relating to content, location, and/or distribution of the target element in the region within the body is determined therefrom. The measured region can extend axially or radially from a surface of the body, and the target elements are nondiamond materials that can be constituents of a substrate attached to the body, or of a container used during HPHT sintering of the body.
    • 用于非破坏性地获得与金刚石体中的区域的材料性质相关的定性和/或定量信息的装置,系统和方法包括将x射线引导到身体上。 身体可以包括烧结或未烧结的金刚石。 身体最终可以是与地下钻头一起使用的切割元件的形式。 X射线穿透身体并使包含该靶的所需区域内的靶元素发射出x射线荧光。 接收到发射的X射线荧光,并从其中确定与体内区域内的目标元素的内容,位置和/或分布有关的信息。 所测量的区域可以从主体的表面轴向或径向延伸,并且目标元件是非金刚石材料,其可以是连接到主体的基底的组分或者在身体的HPHT烧结期间使用的容器。
    • 45. 发明授权
    • Thermally stable diamond polycrystalline diamond constructions
    • 耐热稳定的金刚石多晶金刚石结构
    • US07740673B2
    • 2010-06-22
    • US11776425
    • 2007-07-11
    • Ronald K. Eyre
    • Ronald K. Eyre
    • B24D3/02G11B11/105B32B9/00
    • B24D3/10B22F2003/244B22F2005/001B22F2998/00C22C26/00E21B10/567Y10T407/27Y10T428/24488Y10T428/24612Y10T428/26Y10T428/30Y10T428/31678B22F2207/03
    • Thermally stable diamond constructions comprise a diamond body having a plurality of bonded diamond crystals, a plurality of interstitial regions disposed among the crystals, and a substrate attached to the body. The body includes a working surface and a side surface extending away from the working surface to the substrate. The body comprises a first region adjacent the side surface that is substantially free of a catalyst material and that extends a partial depth into the diamond body. The first region can further extend to at least a portion of the working surface and a partial depth therefrom into the diamond body. The diamond body can be formed from natural diamond grains and/or a mixture of natural and synthetic diamond grains. A surface of the diamond body is treated to provide the first region, and before treatment is finished to an approximate final dimension.
    • 耐热稳定的金刚石构造包括具有多个结合的金刚石晶体的金刚石体,设置在晶体之间的多个间隙区域,以及附着到主体上的基底。 主体包括工作表面和从工作表面延伸到基板的侧表面。 主体包括邻近侧表面的第一区域,其基本上不含催化剂材料,并且将部分深度延伸到钻石体中。 第一区域可以进一步延伸至工作表面的至少一部分,并将其部分深度延伸到钻石体中。 金刚石体可以由天然金刚石颗粒和/或天然和合成金刚石颗粒的混合物形成。 处理钻石体的表面以提供第一区域,并且在处理完成到近似最终尺寸之前。
    • 47. 发明授权
    • Thermally stable diamond polycrystalline diamond constructions
    • 耐热稳定的金刚石多晶金刚石结构
    • US07517589B2
    • 2009-04-14
    • US11022272
    • 2004-12-22
    • Ronald K. Eyre
    • Ronald K. Eyre
    • B32B9/00
    • E21B10/567B22F2003/244B22F2005/001B22F2998/00C22C26/00Y10T407/27Y10T428/252Y10T428/265Y10T428/30B22F7/06
    • Thermally stable diamond constructions comprise a diamond body having a plurality of bonded diamond crystals and interstitial regions disposed among the crystals. A metallic substrate is attached to the body. The body includes a first region substantially free of a catalyst material that extends a partial depth from a surface into the body, and a second region that includes the catalyst material. The body can include natural diamond grains and/or a blend of natural and synthetic diamond grains, and is treated to form the first region. Before treatment, a portion of the body to be treated is finished to an approximate final dimension so that the depth of the first region of the finished product is substantially the same as when treated. During treatment, catalyst materials as well as non-catalyst metallic materials are removed from the diamond body to provide a further enhanced degree of thermal stability.
    • 热稳定的金刚石结构包括具有多个结合的金刚石晶体和布置在晶体之间的间隙区域的金刚石体。 金属基底附着在身上。 主体包括基本上不含催化剂材料的第一区域,其从表面延伸到主体中的部分深度,以及包括催化剂材料的第二区域。 身体可以包括天然金刚石颗粒和/或天然和合成金刚石颗粒的混合物,并且被处理以形成第一区域。 在处理之前,待处理的身体的一部分被完成到近似的最终尺寸,使得成品的第一区域的深度与处理时基本相同。 在处理期间,从金刚石体中除去催化剂材料以及非催化剂金属材料以提供进一步提高的热稳定性。
    • 50. 发明授权
    • Cutting element having a substrate, a transition layer and an ultra hard material layer
    • 具有基板,过渡层和超硬材料层的切割元件
    • US06892836B1
    • 2005-05-17
    • US09735389
    • 2000-12-12
    • Ronald K. EyreMadapusi K. Keshavan
    • Ronald K. EyreMadapusi K. Keshavan
    • E21B10/56E21B10/573E21B10/46
    • E21B10/5735Y10S76/11Y10S76/12
    • A non-uniform interface is formed between a polycrystalline ultra hard material layer and a cemented tungsten carbide substrate, or a polycrystalline ultra hard material layer and a transition layer, or a transition layer and a substrate of a cutting element. A first sheet made from an intermediate material is formed and embossed on one face forming a non-uniform pattern raised in relief on the face. The embossed sheet is placed on a face of a presintered substrate. An ultra hard material sheet is formed and embossed, forming a non-uniform face complementary to the non-uniform face on the sheet of intermediate material. The ultra hard material sheet is placed over the intermediate material sheet so that the complementary faces are adjacent to each other. The assembly of substrate and sheets is sintered in a HPHT process. The sintering process causes the first sheet to become integral with the substrate and results in a substrate having a non-uniform cutting face onto which is bonded a polycrystalline ultra hard material layer. Embossed transition material sheets may be employed between the ultra hard material sheet and the first sheet to form transition layers with uniform or non-uniform interfaces.
    • 在多晶超硬材料层和粘结碳化钨基板,多晶超硬材料层和过渡层,或切割元件的过渡层和基板之间形成非均匀的界面。 由中间材料制成的第一片材​​在一个面上形成并压印,形成在表面上浮雕的不均匀图案。 将压花片放置在预烧结基板的表面上。 形成并压花超硬材料片,形成与中间材料片上的不均匀面互补的不均匀面。 将超硬材料片放置在中间材料片上,使得互补面彼此相邻。 基板和片的组装在HPHT工艺中烧结。 烧结过程使得第一片材与衬底成为一体,并导致具有不均匀切割面的衬底,多晶超硬材料层与其结合。 可以在超硬材料片和第一片之间采用压花过渡材料片,以形成具有均匀或非均匀界面的过渡层。