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41. 发明授权

US5464717A Electrophotographic photoreceptor with subbing layer and charge generating layer 失效
标题翻译：具有底层和电荷产生层的电子照相感光体
公开(公告)号：US5464717A
公开(公告)日：1995-11-07
申请号：US252781
申请日：1994-06-02
申请人： Yasuo Sakaguchi , Katsumi Daimon , Michiaki Takahashi , Kazuo Yamasaki , Yasuhiro Yamaguchi
发明人： Yasuo Sakaguchi , Katsumi Daimon , Michiaki Takahashi , Kazuo Yamasaki , Yasuhiro Yamaguchi
IPC分类号： G03G5/05 , G03G5/06 , G03G5/14 , G03G5/10
CPC分类号： G03G5/142 , G03G5/0696
摘要： An electrophotographic photoreceptor comprising a conductive substrate having thereon at least a subbing layer comprising an organometallic compound (e.g., organozirconium or organotitanium compound) and 3 to 30% by weight, based on the organometallic compound, of a compatible binder resin, a charge generating layer prepared by using a coating composition comprising hydroxygallium phthalocyanine crystals (preferably those having a novel crystal form) as a charge generating material, a binder resin, and a halogenated benzene as a dispersing medium, and a charge transporting layer in this order. The photoreceptor is excellent in sensitivity and stability on repeated use and is free from coating defects.
摘要翻译：一种电子照相感光体，包括导电性基材，其上至少含有有机金属化合物（例如有机锆或有机钛化合物）和基于有机金属化合物的3〜30重量％的相容性粘合剂树脂，电荷产生层通过使用包含羟基镓酞菁晶体（优选具有新型晶体形式的）的涂料组合物作为电荷产生材料，粘合剂树脂和作为分散介质的卤代苯，以及电荷输送层。感光体在重复使用时的灵敏度和稳定性优异，并且不含涂层缺陷。

42. 发明授权

US5463043A Process for producing a dichlorotin phthalocyanine crystal 失效
标题翻译：二氯苯酞菁结晶的制造方法
公开(公告)号：US5463043A
公开(公告)日：1995-10-31
申请号：US240483
申请日：1994-05-10
申请人： Katsumi Nukada , Akira Imai , Katsumi Daimon , Masakazu Iijima , Kiyokazu Mashimo , Yasuo Sakaguchi , Ichiro Takegawa
发明人： Katsumi Nukada , Akira Imai , Katsumi Daimon , Masakazu Iijima , Kiyokazu Mashimo , Yasuo Sakaguchi , Ichiro Takegawa
IPC分类号： C09B67/50 , G03G5/05 , G03G5/06 , C09B47/04
CPC分类号： C09B67/0026 , G03G5/0614 , G03G5/0696 , G03G5/0542
摘要： A novel dichlorotin phthalocyanine crystal having distinct diffraction peaks at 8.5.degree., 11.2.degree., 14.5.degree., and 27.2.degree. of the Bragg angles (2.theta..+-.0.2) in the X-ray diffraction spectrum; a process for producing the dichlorotin phthalocyanine crystal, comprising mechanically grinding a known dichlorotin phthalocyanine crystal together with an inorganic salt, followed by, if desired, a solvent treatment; an electrophotographic photoreceptor containing, in the photosensitive layer thereof, the dichlorotin phthalocyanine crystal; and a coating composition for producing an electrophotographic photoreceptor, comprising the dichlorotin phthalocyanine crystal, a binder resin, and an acetic ester solvent. The photoreceptor exhibits high sensitivity and excellent durability. The coating composition maintains the dichlorotin phthalocyanine crystal in its desired form either while being prepared or after being coated.
摘要翻译：在X射线衍射光谱中，在布拉格角（2θ+/- 0.2）的8.5°，11.2°，14.5°和27.2°处具有不同衍射峰的新型二氯苯酞菁结晶; 制备二氯靛菁酞菁晶体的方法，包括机械研磨已知的二氯靛菁酞菁结晶与无机盐，随后如果需要，进行溶剂处理; 在感光层中含有二氯靛菁酞菁的电子照相感光体; 以及用于制造电子照相感光体的涂料组合物，其包含二氯苯酞菁结晶，粘合剂树脂和乙酸酯溶剂。感光体表现出高灵敏度和优异的耐久性。涂料组合物在制备或涂覆之后将二氯色素酞菁晶体保持为所需形式。

43. 发明授权

US5459004A Process for preparing hydroxygallium phthalocyanine crystals and electrophotographic photoreceptor using the crystals 失效
标题翻译：使用晶体制备羟基镓酞菁晶体和电子照相感光体的方法
公开(公告)号：US5459004A
公开(公告)日：1995-10-17
申请号：US038299
申请日：1993-03-29
申请人： Katsumi Daimon , Katsumi Nukada , Akira Imai , Masakazu Iijima , Toru Ishii
发明人： Katsumi Daimon , Katsumi Nukada , Akira Imai , Masakazu Iijima , Toru Ishii
IPC分类号： C09B67/50 , C09B67/12 , G03G5/06 , G03G5/00
CPC分类号： C09B67/0016 , G03G5/0696
摘要： A process for preparing hydroxygallium phthalocyanine crystals showing intense diffraction peaks at Bragg angles (2.theta..+-.0.2) of 7.5.degree., 25.1.degree., and 28.3.degree. with respect to CuK.sub..alpha. characteristic X-rays which comprises mechanically grinding hydroxygallium phthalocyanine and then treating the grains with a solvent is disclosed. The hydroxygallium phthalocyanine crystals obtained by the process of the present invention has a novel crystal form and exhibits high sensitivity and excellent durability on repeated use as well as crystal form stability. The electrophotographic photoreceptor prepared by using the resulting hydroxygallium phthalocyanine exhibits excellent electrophotographic characteristics.
摘要翻译：相对于CuKα特征X射线，制备羟基镓酞菁晶体的显示强度为7.5°，25.1°和28.3°的布拉格角（2θ+/- 0.2）衍射峰的方法，其包括机械研磨羟基镓酞菁然后处理公开了具有溶剂的颗粒。通过本发明的方法获得的羟基镓酞菁晶体具有新颖的晶体形式，并且在重复使用以及晶体形式稳定性方面表现出高灵敏度和优异的耐久性。通过使用所得羟基镓酞菁制备的电子照相感光体显示出优异的电子照相特性。

44. 发明授权

US5358813A Crystals of chlorogallium phthalocyanine and method of preparing them 失效
标题翻译：氯镓酞菁的晶体及其制备方法
公开(公告)号：US5358813A
公开(公告)日：1994-10-25
申请号：US3123
申请日：1993-01-12
申请人： Masakazu Iijima , Katsumi Nukada , Katsumi Daimon , Akira Imai , Toru Ishii , Yasuo Sakaguchi , Kiyokazu Mashimo , Ichiro Takegawa
发明人： Masakazu Iijima , Katsumi Nukada , Katsumi Daimon , Akira Imai , Toru Ishii , Yasuo Sakaguchi , Kiyokazu Mashimo , Ichiro Takegawa
IPC分类号： C09B67/12 , C09B67/50 , G03G5/06
CPC分类号： G03G5/0696 , C09B67/0016 , C09B67/0026
摘要： Crystals of chlorogallium phthalocyanine, having distinct diffraction peaks at (i) 7.4.degree., 16.6.degree., 25.5.degree. and 28.3.degree., (ii) 6.8.degree., 17.3.degree., 23.6.degree. and 26.9.degree., or (iii) 8.7.degree. to 9.2.degree., 17.6.degree., 24.0.degree., 27.4.degree. and 28.8.degree. of the Bragg angle (2.theta..+-.0.2) to a CuK.alpha. characteristic X-ray; a photoconductive material for electrophotographic photoreceptor comprising the chlorogallium phthalocyanine; and an electrophotographic photoreceptor comprising an electroconductive support having thereon a light-sensitive layer containing at least one or more of chlorogallium phthalocyanine crystals. The electrophotographic photoreceptor has excellent sensitivity and durability.
摘要翻译：（i）7.4°，16.6°，25.5°和28.3°，（ii）6.8°，17.3°，23.6°和26.9°，或（iii）8.7°至9.2°处具有不同衍射峰的氯镓酞菁晶体，相对于CuKα特征X射线，布拉格角（2θ+/- 0.2）的17.6°，24.0°，27.4°和28.8°; 用于电子照相感光体的光电导材料，其包含氯镓酞菁; 以及电子照相感光体，其包含导电性载体，其上具有至少含有一种或多种氯镓酞菁晶体的感光层。电子照相感光体具有优异的灵敏度和耐久性。

45. 发明授权

US5298617A Oxytitaniumphthalocyanine hydrate crystal and electrophotographic photoreceptor using said crystal 失效
标题翻译：氧化钛酞菁水合物晶体和使用所述晶体的电子照相感光体
公开(公告)号：US5298617A
公开(公告)日：1994-03-29
申请号：US757218
申请日：1991-09-10
申请人： Katsumi Nukada , Katsumi Daimon , Masakazu Iijima , Yasuo Sakaguchi , Hidemi Nukada , Akihiko Tokida
发明人： Katsumi Nukada , Katsumi Daimon , Masakazu Iijima , Yasuo Sakaguchi , Hidemi Nukada , Akihiko Tokida
IPC分类号： G03C1/735 , C09B47/073 , C09B67/12 , C09B67/50 , G03G5/06 , C09B47/04
CPC分类号： C09B67/0026 , C09B67/0016 , G03G5/0696
摘要： Oxytitanium phthalocyanine hydrate crystal and an electrophotographic photoreceptor using said crystal are disclosed. The structural formula of the crystal is TiOPc(H.sub.2 O).sub.n wherein Pc represents a phthalocyanine residual group, and n represents from 0.15 to 1; and the elemental analysis values of C, H and N are as follows: C: 65.0 to 66.3%; H: 2.5 to 3.1%; and N: 18.5 to 19.3%.
摘要翻译：公开了氧钛酞菁水合物晶体和使用该晶体的电子照相感光体。结晶的结构式为TiOPc（H 2 O）n，其中Pc表示酞菁残基，n表示0.15〜1。 C，H，N的元素分析值如下：C：65.0〜66.3％ H：2.5〜3.1％; N：18.5〜19.3％。

46. 发明授权

US5290928A Process for preparing oxytitanium phthalocyanine hydrate crystal 失效
标题翻译：氧化钛酞菁水合物晶体的制备方法
公开(公告)号：US5290928A
公开(公告)日：1994-03-01
申请号：US928416
申请日：1992-08-12
申请人： Katsumi Nukada , Masakazu Iijima , Akira Imai , Katsumi Daimon
发明人： Katsumi Nukada , Masakazu Iijima , Akira Imai , Katsumi Daimon
IPC分类号： C09B67/12 , C09B67/50 , G03G5/06
CPC分类号： C09B67/0016 , C09B67/0026 , G03G5/0696
摘要： A process for preparing an oxytitanium phthalocyanine hydrate crystal which, when dried at 100.degree. C. and 0.1 mmHg for 8 hours and then allowed to stand in air at room temperature for 12 hours, has a structural formula of TiOPc.multidot.(H.sub.2 O).sub.n, wherein Pc represents a phthalocyanine nucleus, and n represents a number of from 0.15 to 1, and elemental analysis values of C: 65.0 to 66.3%, H: 2.5 to 3.1%, and N: 18.5 to 19.3% is disclosed, which process comprises the steps of: mechanically grinding a mixture of oxytitanium phthalocyanine and an inorganic salt to convert the crystal form of the oxytitanium phthalocyanine to a crystal form showing a distinct peak in its X-ray diffraction pattern at a Bragg angle (2.theta..+-.0.2.degree. ) of 27.3.degree. and treating the resulting oxytitanium phthalocyanine crystal with a mixed solvent of water and a water-insoluble organic solvent. The oxytitanium phthalocyanine hydrate crystal obtained has doped therein a specific amount of water of crystallization and is stable in a solvent and also stable when used as an electrophotographic photoreceptor.
摘要翻译：一种制备氧钛酞菁水合物晶体的方法，其在100℃和0.1mmHg下干燥8小时，然后在室温下放置12小时，其结构式为TiOPcx（H 2 O）n，其中 Pc表示酞菁核，n表示0.15〜1的数，C：65.0〜66.3％，H：2.5〜3.1％，N：18.5〜19.3％的元素分析值，步骤：机械研磨氧钛酞菁和无机盐的混合物，以将氧钛酞菁的晶体形式转变为在其布拉格角（2θ+/- 0.2°）的X射线衍射图中显示出不同峰的晶体形式）为27.3℃，用水和水不溶性有机溶剂的混合溶剂处理得到的氧钛酞菁结晶。获得的氧钛酞菁水合物晶体在其中掺入特定量的结晶水，并且在溶剂中是稳定的，并且当用作电子照相感光体时也是稳定的。

47. 发明授权

US08512926B2 Electrophotographic toner, electrophotographic developer, toner cartridge, and image forming method 有权
标题翻译：电子照相调色剂，电子照相显影剂，调色剂盒和成像方法
公开(公告)号：US08512926B2
公开(公告)日：2013-08-20
申请号：US12046957
申请日：2008-03-12
申请人： Katsumi Daimon , Yutaka Sugizaki , Susumu Yoshino , Hiroshi Nakazawa
发明人： Katsumi Daimon , Yutaka Sugizaki , Susumu Yoshino , Hiroshi Nakazawa
IPC分类号： G03G9/00
CPC分类号： G03G9/08755 , G03G9/08795 , G03G9/08797
摘要： The invention provides an electrophotographic toner having a crystalline polyester resin; a non-crystalline polyester resin; a colorant; and a releasing agent. A resin (i), that is included in a toluene-soluble component of the toner and having a molecular weight of 30,000 to 100,000 as measured by gel permeation chromatography relative to polystyrene standards, has an acid value A. A resin (ii), that is included in a toluene-soluble component of the toner and having a molecular weight of 8,000 to 12,000 as measured by gel permeation chromatography relative to polystyrene standards, has an acid value B. A resin (iii), that is included in a toluene-insoluble component of the toner, has an acid value C. The acid values A, B, and C satisfy the inequation of B>A>C. The invention further provides an electrophotographic developer using the toner, a toner cartridge storing the toner, and an image forming method using the developer.
摘要翻译：本发明提供具有结晶聚酯树脂的电子照相调色剂; 非结晶聚酯树脂; 着色剂和脱模剂。包含在调色剂的甲苯可溶组分中，通过凝胶渗透色谱法测定的分子量为30,000至100,000的树脂（ⅰ）的酸值为A。树脂（ⅱ），包括在调色剂的甲苯可溶性组分中并且通过凝胶渗透色谱法相对于聚苯乙烯标准测量的分子量为8,000至12,000，具有酸值B.将包含在甲苯中的树脂（ⅲ）调色剂的不溶成分，具有酸值C.酸值A，B和C满足B> A> C的不等式。本发明还提供使用调色剂的电子照相显影剂，存储调色剂的调色剂盒和使用显影剂的图像形成方法。

48. 发明授权

US07642031B2 Electrophotographic toner and electrophotographic developer and image forming method 有权
标题翻译：电子照相调色剂和电子照相显影剂和成像方法
公开(公告)号：US07642031B2
公开(公告)日：2010-01-05
申请号：US11491146
申请日：2006-07-24
申请人： Katsumi Daimon , Yosuke Tsurmi , Yusuke Ikeda , Hiroyuki Tanaka , Satoshi Yoshida , Noriyuki Mizutani , Shinpei Takagi , Hideo Maehata , Soichiro Kitagawa , Masaru Takahashi , Susumu Yoshino
发明人： Katsumi Daimon , Yosuke Tsurmi , Yusuke Ikeda , Hiroyuki Tanaka , Satoshi Yoshida , Noriyuki Mizutani , Shinpei Takagi , Hideo Maehata , Soichiro Kitagawa , Masaru Takahashi , Susumu Yoshino
IPC分类号： G03G9/00
CPC分类号： G03G9/08711 , G03G9/0825 , G03G9/08722 , G03G9/08724 , G03G9/08728 , G03G9/08733 , G03G9/08795 , G03G9/08797
摘要： An electrophotographic toner that includes a colorant, a release agent, a non-crystalline resin and a crystalline resin, wherein the crystalline resin is a polyalkyl acrylate or polyalkyl methacrylate having an alkyl group of approximately 18 or more carbon atoms, and is produced by copolymerization with approximately 10 mol % or more, but no more than approximately 50 mol %, of a vinyl monomer having a carboxyl group.
摘要翻译：包含着色剂，脱模剂，非结晶性树脂和结晶性树脂的电子照相调色剂，其中所述结晶性树脂为具有约18以上碳原子的烷基的聚丙烯酸烷基酯或甲基丙烯酸烷基酯，并且通过共聚合具有约10摩尔％以上但不超过约50摩尔％的具有羧基的乙烯基单体。

49. 发明申请

US20080187854A1 Electrostatic image developing toner, electrostatic image developer, toner cartridge, process cartridge, and image forming apparatus 有权
标题翻译：静电图像显影调色剂，静电图像显影剂，调色剂盒，处理盒和成像设备
公开(公告)号：US20080187854A1
公开(公告)日：2008-08-07
申请号：US11905473
申请日：2007-10-01
申请人： Satoshi Yoshida , Shinpei Takagi , Noriyuki Mizutani , Yusuke Ikeda , Katsumi Daimon
发明人： Satoshi Yoshida , Shinpei Takagi , Noriyuki Mizutani , Yusuke Ikeda , Katsumi Daimon
IPC分类号： G03C8/36 , G03G15/08
CPC分类号： G03G9/0804 , G03G9/0819 , G03G9/08755 , G03G9/08795 , G03G9/08797
摘要： An embodiment of the present invention provides an electrostatic image developing toner including a binder resin containing amorphous polyester resin containing a tin-containing catalyst and crystalline polyester resin containing a titanium-containing catalyst, and a colorant and a releasing agent, an electrostatic image developer using the same, a toner cartridge, a process cartridge, and an image forming apparatus.
摘要翻译：本发明的一个实施方案提供了一种静电图像显影调色剂，其包含含有含锡催化剂的无定形聚酯树脂和含有钛的催化剂的结晶聚酯树脂和着色剂和脱模剂的粘合剂树脂，静电图像显影剂使用相同的，调色剂盒，处理盒和图像形成装置。

50. 发明申请

US20060292477A1 Electrophotographic toner, method for producing the same, electrophotographic developer, method for producing the developer, and image forming method 有权
公开(公告)号：US20060292477A1
公开(公告)日：2006-12-28
申请号：US11299625
申请日：2005-12-13
申请人： Katsumi Daimon , Shuji Sato , Shigeru Hayashi , Yosuke Tsurumi , Yusuke Ikeda , Hiroshi Nakazawa
发明人： Katsumi Daimon , Shuji Sato , Shigeru Hayashi , Yosuke Tsurumi , Yusuke Ikeda , Hiroshi Nakazawa
IPC分类号： G03G9/087
CPC分类号： G03G9/08795 , G03G9/0804 , G03G9/08755 , G03G9/08797 , G03G9/093 , G03G9/09328 , G03G9/09371 , G03G9/09392
摘要： Provided are an electrophotographic toner, comprising a binder resin containing a coloring agent, a crystalline resin and an amorphous resin, wherein the crystalline resin has two or more peaks in weight-average molecular weight as determined by gel permeation chromatography, one of the peaks has a weight-average molecular weight in the range of 15,000 to 40,000, and another peak has a weight-average molecular weight in the range of 2,000 to 10,000 and a production method thereof, and an electrophotographic developer and an image-forming process using the electrophotographic toner.

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