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41. 发明申请

US20120172636A1 HIGH PURITY E-1-CHLORO-3,3,3-TRIFLUOROPROPENE AND METHODS OF MAKING THE SAME 有权
标题翻译：高纯度E-1-氯代-3,3,3-三氟苯酚及其制备方法
公开(公告)号：US20120172636A1
公开(公告)日：2012-07-05
申请号：US12984024
申请日：2011-01-04
申请人： Konstantin A. Pokrovski , Rajiv Ratna Singh , Ian Shankland , Hsueh Sung Tung
发明人： Konstantin A. Pokrovski , Rajiv Ratna Singh , Ian Shankland , Hsueh Sung Tung
IPC分类号： C07C21/18 , C07C17/25 , C07C17/20
CPC分类号： C07C17/361 , C07B2200/09 , C07C17/206 , C07C17/25 , C07C19/10 , C07C21/18
摘要： The present invention discloses high purity E-1-chloro-3,3,3-trifluoropropene (1233zd(E)) and methods to produce the same. More specifically, the present invention discloses the methods of making 1233zd(E) essentially free of toxic impurities (e.g. 2-chloro-3,3,3-trifluoropropene (1233xf), chlorotetrafluoro-propene (1224), and 3,3,3-trifluoropropyne). The present invention further provides methods for making high purity 1233zd(E) with concentration of 1233xf and 1224 at or below 200 parts per million (ppm) and 3,3,3-trifluoropropyne impurities at or below 20 ppm. Formation of 1233xf impurity can be avoided if pure 1,1,1,3,3-pentachloropropane is used as a starting material. It was also found that formation of 1233xf is avoided if a liquid phase manufacturing process is used.
摘要翻译：本发明公开了高纯度E-1-氯-3,3,3-三氟丙烯（1233zd（E））及其制备方法。更具体地说，本发明公开了制备基本上不含有毒杂质的1233zd（E）的方法（例如2-氯-3,3,3-三氟丙烯（1233xf），氯四氟丙烯（1224）和3,3,3 三氟丙炔）。本发明还提供了制备浓度为1233xf和1224等于或低于200ppm（ppm）的高纯度1233zd（E）和等于或低于20ppm的3,3,3-三氟丙炔杂质的方法。如果使用纯1,1,1,3,3-五氯丙烷作为原料，则可以避免形成1233xf杂质。还发现如果使用液相制造方法，则避免形成1233xf。

42. 发明授权

US07985299B2 Solvent compositions containing chlorofloroolefins or fluoroolefins 有权
标题翻译：含有氯氟烯烃或氟烯烃的溶剂组合物
公开(公告)号：US07985299B2
公开(公告)日：2011-07-26
申请号：US12368094
申请日：2009-02-09
申请人： Robert C. Johnson , Hsueh Sung Tung , Rajiv Ratna Singh , Ian Shankland
发明人： Robert C. Johnson , Hsueh Sung Tung , Rajiv Ratna Singh , Ian Shankland
IPC分类号： C11D7/50
CPC分类号： C09K5/044 , A62D1/06 , B01F17/0035 , C08J9/144 , C09K3/00 , C09K5/045 , C09K21/08 , C09K2205/102 , C09K2205/104 , C09K2205/12 , C09K2205/122 , C09K2205/126 , C10M101/02 , C10M171/008 , C10M2203/003 , C10N2220/302 , C10N2240/30 , C11D3/43 , C11D7/30 , C11D7/5018 , C11D11/0047 , C23G5/02809 , C23G5/02825 , F25B1/00 , F25B31/002 , G03F7/426 , H05K3/26 , Y02C20/30
摘要： Compositions and methods based on the use of fluoroalkene containing from 3 to 4 carbon atoms and at least one carbon-carbon double bond, such as HFO-1214, HFO-HFO-1233, or HFO-1354, having properties highly beneficial in solvent cleaning applications.
摘要翻译：基于使用含有3至4个碳原子的氟代烯烃和至少一个碳 - 碳双键的组合物和方法，例如HFO-1214，HFO-HFO-1233或HFO-1354，具有在溶剂清洗中非常有益的性质应用程序。

43. 发明申请

US20110023507A1 COMPOSITIONS AND METHODS FOR REFRIGERATION 有权
标题翻译：用于制冷的组合物和方法
公开(公告)号：US20110023507A1
公开(公告)日：2011-02-03
申请号：US12776320
申请日：2010-05-07
申请人： Samuel F. Yana Motta , Mark W. Spatz , Rajiv Ratna Singh , Robert Gerard Richard , Elizabet del Carmen Vera Becerra , Daniel Burger
发明人： Samuel F. Yana Motta , Mark W. Spatz , Rajiv Ratna Singh , Robert Gerard Richard , Elizabet del Carmen Vera Becerra , Daniel Burger
IPC分类号： F25B1/00 , C09K5/04
CPC分类号： C09K5/045 , C09K3/30 , C09K2205/126 , C09K2205/22 , C09K2205/40 , F25B1/00 , F25B40/00 , F25B2400/121 , F25B2400/18 , F28D1/00
摘要： Heat transfer systems, methods and compositions which utilize a heat transfer fluid comprising: (a) from about 30% to about 65% by weight of HFC-134a; (b) from about 0% to about 70% by weight of HFO1234ze; and (c) from about 0% to about 70% by weight of HFO-1234yf, provided that the amount of HFO-1234ze and HFO-1234yf in the composition together is at least about 35% by weight, with the weight percent being based on the total of the components (a)-(c) in the composition.
摘要翻译：使用传热流体的热传递系统，方法和组合物包括：（a）约30重量％至约65重量％的HFC-134a; （b）约0％至约70％重量的HFO1234ze; 和（c）HFO-1234yf重量的约0％至约70％，条件是组合物中HFO-1234ze和HFO-1234yf的量为至少约35重量％，重量百分比为关于组合物中组分（a） - （c）的总和。

44. 发明授权

US06689822B1 Azeotrope-like compositions of pentafluoropropane and water 有权
标题翻译：五氟丙烷和水的类共沸组合物
公开(公告)号：US06689822B1
公开(公告)日：2004-02-10
申请号：US09575399
申请日：2000-10-02
申请人： Leslie Bruce Bement , Mary Charlotte Bogdan , Clayton Herbert Carson , Peter Brian Logsdon , Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung , Ronald Riegal , David John Williams , Kevin Donald Uhrich
发明人： Leslie Bruce Bement , Mary Charlotte Bogdan , Clayton Herbert Carson , Peter Brian Logsdon , Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung , Ronald Riegal , David John Williams , Kevin Donald Uhrich
IPC分类号： C08G1810
CPC分类号： C11D7/5036 , C11D7/505
摘要： This invention provides azeotrope-like compositions of 1,1,1,3,3-pentafluoropropane and water that are environmentally desirable for use as refrigerants, aerosol propellants, metered dose inhalers, blowing agents for polymer foam, heat transfer media, and gaseous dielectrics.
摘要翻译：本发明提供1,1,1,3,3-五氟丙烷和水的类共沸组合物，其作为制冷剂，气溶胶推进剂，计量吸入器，用于聚合物泡沫的发泡剂，传热介质和气体电介质是环境需要的。

45. 发明授权

US06545063B1 Hydrofluorocarbon blown foam and method for preparation thereof 有权
标题翻译：氢氟烃吹泡沫及其制备方法
公开(公告)号：US06545063B1
公开(公告)日：2003-04-08
申请号：US09393762
申请日：1999-09-10
申请人： Mary Charlotte Bogdan , Leslie Bruce Bement , Barbara Ruth Decaire , Dennis Paul Konopa , Harold John Kieta , Rajiv Ratna Singh
发明人： Mary Charlotte Bogdan , Leslie Bruce Bement , Barbara Ruth Decaire , Dennis Paul Konopa , Harold John Kieta , Rajiv Ratna Singh
IPC分类号： C08J912
CPC分类号： C08J9/146 , C08J9/0023 , C08J2205/052 , C08J2375/04
摘要： The invention relates to the addition of &agr;-methyl styrene, isobutanol and/or isopropanol to reduce vapor pressure, improve k-factor, enhance the solubility of the blowing agent in the premix and/or improve the processing characteristics of polyurethane and polyisocyanurate closed-cell foams prepared with a blowing agent comprising a hydrofluorocarbon selected from the group consisting of 1,1,1,3,3-pentafluoropropane, 1,1,1,2-tetrafluoroethane, 1,1,2,2-tetrafluoroethane, and mixtures thereof.
摘要翻译：本发明涉及α-甲基苯乙烯，异丁醇和/或异丙醇的加入以降低蒸气压，改善k因子，提高发泡剂在预混物中的溶解度和/或改善聚氨酯和聚异氰脲酸酯封闭的加工特性，用包含选自1,1,1,3,3-五氟丙烷，1,1,1,2-四氟乙烷，1,1,2,2-四氟乙烷和1,1,2,2-四氟乙烷的氢氟烃的发泡剂制备的泡沫体，其中。

46. 发明授权

US06488817B1 Purification of hydrofluorocarbons 失效
标题翻译：氢氟烃的净化
公开(公告)号：US06488817B1
公开(公告)日：2002-12-03
申请号：US09052757
申请日：1998-03-31
申请人： Charles Francis Swain , Rajiv Ratna Singh , Hang Thanh Pham
发明人： Charles Francis Swain , Rajiv Ratna Singh , Hang Thanh Pham
IPC分类号： B01D336
CPC分类号： C07C17/383 , Y10S203/13 , C07C19/08 , C07C19/10
摘要： A process for the purification of difluoromethane comprising: (a) subjecting a mixture comprising at least difluoromethane (HFC-32) and dichlorodifluoromethane (CFC-12) to a first distillation step in which a majority of either CFC-12 or HFC-32 is concentrated in a first distillate and a majority of the other component is concentrated in a first bottoms; and (b) subjecting the first distillate in step (a) to at least one additional second distillation step conducted at a different pressure in which a majority of the component concentrated in said first distillate is concentrated in a second bottoms and in which the other component is concentrated in a second distillate; and (c) recovering purified HFC-32 from one of said first or second bottoms.
摘要翻译：一种净化二氟甲烷的方法，包括：（a）使包含至少二氟甲烷（HFC-32）和二氯二氟甲烷（CFC-12）的混合物经历第一蒸馏步骤，其中大部分CFC-12或HFC-32是浓缩在第一馏出物中，并且大部分其它组分浓缩在第一塔底物中; 和（b）将步骤（a）中的第一馏出物经受至少一个额外的第二蒸馏步骤，其在不同的压力下进行，其中浓缩在所述第一馏出物中的大部分组分集中在第二塔底物中，其中另一组分集中在第二个馏出物中; 和（c）从所述第一或第二底部之一回收纯化的HFC-32。

47. 发明授权

US06101818A Process for separating water from chemical mixtures 失效
标题翻译：从化学混合物中分离水的方法
公开(公告)号：US06101818A
公开(公告)日：2000-08-15
申请号：US967632
申请日：1997-11-10
申请人： Raymond Hilton Percival Thomas , Rajiv Ratna Singh , Jeffrey Warren McKown , Roy Phillip Robinson , Stephen Alan Cottrell
发明人： Raymond Hilton Percival Thomas , Rajiv Ratna Singh , Jeffrey Warren McKown , Roy Phillip Robinson , Stephen Alan Cottrell
IPC分类号： B01D17/022 , B01D15/00 , B01D17/02 , B01D53/26 , B01D53/28 , B01J20/26 , C07C17/38 , C08F20/06 , F25B47/00 , B01D3/00 , C07C17/10
CPC分类号： B01D15/00 , B01D17/0202 , B01D53/261 , B01D53/28 , B01J20/26 , C07C17/38
摘要： A method for separating water from a chemical mixture is provided. In the process of the invention, water is separated from a chemical mixture by contacting the chemical mixture with a water-soluble polymer.
摘要翻译：提供了从化学混合物中分离水的方法。在本发明的方法中，通过使化学混合物与水溶性聚合物接触将水与化学混合物分离。

48. 发明授权

US5918481A Process for separating hydrogen fluoride from fluorocarbons 失效
标题翻译：从氟化碳中分离氟化氢的方法
公开(公告)号：US5918481A
公开(公告)日：1999-07-06
申请号：US974935
申请日：1997-11-20
申请人： Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung , Daniel Christopher Merkel , David Goldschmidt , Tadeusz Piotr Rygas
发明人： Hang Thanh Pham , Rajiv Ratna Singh , Hsueh Sung Tung , Daniel Christopher Merkel , David Goldschmidt , Tadeusz Piotr Rygas
IPC分类号： C01B7/19 , C07C17/38 , C07C17/383 , C07C19/08 , C07C21/18 , F25J1/00
CPC分类号： C01B7/196 , C07C17/38
摘要： The invention provides a method for separating fluorocarbons from mixtures of fluorocarbon and hydrogen fluoride. In particular, the invention provides a method for separating fluorocarbons, such as pentafluoropropane, from azeotropic mixtures of the fluorocarbon and hydrogen fluoride using compositional variations with pressure.
摘要翻译：本发明提供了从碳氟化合物和氟化氢的混合物中分离碳氟化合物的方法。特别地，本发明提供了使用组合变化与压力从碳氟化合物和氟化氢的共沸混合物分离氟烃如五氟丙烷的方法。

49. 发明授权

US09994751B2 Absorption refrigeration cycles using a LGWP refrigerant 有权
公开(公告)号：US09994751B2
公开(公告)日：2018-06-12
申请号：US12432466
申请日：2009-04-29
申请人： Ryan J. Hulse , Rajiv Ratna Singh
发明人： Ryan J. Hulse , Rajiv Ratna Singh
IPC分类号： F25B15/02 , C09K5/04 , F25B15/00
CPC分类号： C09K5/047 , F25B15/008 , F25B15/02 , Y02A30/277 , Y02B30/62 , Y02P20/124
摘要： An absorptive refrigeration method that employs a refrigerant comprising one or more hydrofluoroolefin or hydrochlorofluoroolefin refrigerants, and an oil selected from the group consisting of a polyalkyene glycol oil, a poly alpha olefin oil, a mineral oil and a polyolester oil.

50. 发明授权

US08618040B2 Solvent compositions containing chlorofluoroolefins or fluoroolefins 有权
标题翻译：含有氯氟烯烃或氟烯烃的溶剂组合物
公开(公告)号：US08618040B2
公开(公告)日：2013-12-31
申请号：US13177848
申请日：2011-07-07
申请人： Robert C. Johnson , Hsueh Sung Tung , Rajiv Ratna Singh , Ian Shankland
发明人： Robert C. Johnson , Hsueh Sung Tung , Rajiv Ratna Singh , Ian Shankland
IPC分类号： C09K5/04
CPC分类号： C09K5/044 , A62D1/06 , B01F17/0035 , C08J9/144 , C09K3/00 , C09K5/045 , C09K21/08 , C09K2205/102 , C09K2205/104 , C09K2205/12 , C09K2205/122 , C09K2205/126 , C10M101/02 , C10M171/008 , C10M2203/003 , C10N2220/302 , C10N2240/30 , C11D3/43 , C11D7/30 , C11D7/5018 , C11D11/0047 , C23G5/02809 , C23G5/02825 , F25B1/00 , F25B31/002 , G03F7/426 , H05K3/26 , Y02C20/30
摘要： Compositions and methods based on the use of fluoroalkene containing from 3 to 4 carbon atoms and at least one carbon-carbon double bond, such as HFO-1214, HFO-HFO-1233, or HFO-1354, having properties highly beneficial in foaming and blowing agent applications, articles and methods.
摘要翻译：基于使用含有3至4个碳原子的氟代烯烃和至少一个碳 - 碳双键的组合物和方法，例如HFO-1214，HFO-HFO-1233或HFO-1354，具有在发泡和发泡剂应用，物品和方法。

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