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41. 发明公开

EP1478614A1 VERFAHREN ZUR HERSTELLUNG VON PHTHALS UREANHYDRID 无效
标题翻译：用于生产苯酐
公开(公告)号：EP1478614A1
公开(公告)日：2004-11-24
申请号：EP03706423.5
申请日：2003-02-04
申请人： BASF AKTIENGESELLSCHAFT
发明人： STORCK, Sebastian , ROSOWSKI, Frank , BAIER, Michael , TENTEN, Andreas , WOLF, Hans-Josef
IPC分类号： C07C51/265 , C07C51/31 , C07C63/16
CPC分类号： C07C51/265 , B01J23/22 , B01J35/0006 , C07C51/313 , C07C63/16
摘要： The invention relates to a method for producing phthalic anhydride by subjecting xylene, naphthalene or mixtures thereof, to gas phase oxidation in a multitube fixed-bed reactor which is thermostatted by means of a heat-transfer medium, on at least three different fixed-bed catalysts arranged in layers. Said method is carried out in such a way that the maximum temperature of the second catalyst layer, in the direction of flow, is up to 50 °C lower than the maximum temperature of the first catalyst layer, and the maximum temperature of the third layer, as seen from the gas inlet, is between 30 and 100 °C lower than that of the first catalyst layer. The inventive method enables large amounts of phthalic anhydride to be produced under practice-relevant conditions.

42. 发明公开

EP1337332A1 KATALYSATOR UND VERFAHREN ZUR HERSTELLUNG VON MALEINSÄUREANHYDRID 审中-公开
标题翻译：催化剂及其生产顺酐
公开(公告)号：EP1337332A1
公开(公告)日：2003-08-27
申请号：EP01988623.3
申请日：2001-10-26
申请人： BASF AKTIENGESELLSCHAFT
发明人： STORCK, Sebastian , WEIGUNY, Jens , DUDA, Mark , COX, Gerhard
IPC分类号： B01J27/198 , B01J35/02 , B01J37/08
CPC分类号： B01J37/08 , B01J27/198 , B01J35/026 , C07C51/215 , C07C57/145
摘要： The invention relates to a vanadium-, phosphorus- and oxygen-containing catalyst that is used for producing maleic anhydride by heterogeneous catalytic gas phase oxidation of a hydrocarbon carrying at least four carbon atoms in which the ratio of phosphorus/vanadium is 0.9 to 1.5. Said catalyst comprises particles with an average diameter of at least 2 mm and the composition has a x-ray powder diffraction pattern, obtained by irradiation with CuKα radiation (μ = 1.54 . 10-10 m), that produces in the 2υ range of 10° to 70° a signal/noise ratio of ≤ 10 for all diffraction lines that can be attributed to a vanadium- and phosphorus-containing phase. The invention further relates to a method for producing such a catalyst and to a method for producing maleic anhydride on such a catalyst.

43. 发明授权

EP1654061B1 KATALYSATOR FÜR GASPHASENOXIDATIONEN 有权
标题翻译：催化剂的气相氧化
公开(公告)号：EP1654061B1
公开(公告)日：2007-04-25
申请号：EP04763675.8
申请日：2004-07-30
申请人： BASF Aktiengesellschaft
发明人： NETO, Samuel , ZÜHLKE, Jürgen , STORCK, Sebastian , ROSOWSKI, Frank
IPC分类号： B01J31/06 , C07C51/215
CPC分类号： B01J23/22 , B01J21/063 , B01J23/002 , B01J27/198 , B01J37/0219 , B01J37/0221 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/51 , B01J2523/53 , B01J2523/55
摘要： Disclosed is a catalyst for gas phase oxidations, comprising an inert carrier and a catalytically active material that is applied thereupon and contains transition metal oxides, or a precatalyst. Said (pre)catalyst is obtained by processing the inert carrier with an aqueous suspension or solution of the transition metal oxides or the precursor compounds thereof. The suspension contains a binder dispersion while the binder is a copolymer of an α-olefin and a vinyl-C2-C4-carboxylate, the vinyl-C2-C4-carboxylate content of which amounts to at least 62 mole percent.

44. 发明授权

EP1478614B1 VERFAHREN ZUR HERSTELLUNG VON PHTHALSÄUREANHYDRID 无效
标题翻译：用于生产苯酐
公开(公告)号：EP1478614B1
公开(公告)日：2007-02-21
申请号：EP03706423.5
申请日：2003-02-04
申请人： BASF Aktiengesellschaft
发明人： STORCK, Sebastian , ROSOWSKI, Frank , BAIER, Michael , TENTEN, Andreas , WOLF, Hans-Josef
IPC分类号： C07C51/265 , C07C51/31 , C07C63/16
CPC分类号： C07C51/265 , B01J23/22 , B01J35/0006 , C07C51/313 , C07C63/16
摘要： The invention relates to a method for producing phthalic anhydride by subjecting xylene, naphthalene or mixtures thereof, to gas phase oxidation in a multitube fixed-bed reactor which is thermostatted by means of a heat-transfer medium, on at least three different fixed-bed catalysts arranged in layers. Said method is carried out in such a way that the maximum temperature of the second catalyst layer, in the direction of flow, is up to 50 °C lower than the maximum temperature of the first catalyst layer, and the maximum temperature of the third layer, as seen from the gas inlet, is between 30 and 100 °C lower than that of the first catalyst layer. The inventive method enables large amounts of phthalic anhydride to be produced under practice-relevant conditions.

45. 发明授权

EP1487575B1 VERFAHREN ZUR HERSTELLUNG EINES VANADIUM, PHOSPHOR UND SAUERSTOFF ENTHALTENDEN KATALYSATORS 有权
标题翻译：用于生产钒，磷和氧的含催化剂
公开(公告)号：EP1487575B1
公开(公告)日：2005-12-14
申请号：EP03708212.0
申请日：2003-03-12
申请人： BASF Aktiengesellschaft
发明人： WEIGUNY, Jens , STORCK, Sebastian , DUDA, Mark , DOBNER, Cornelia , FELDER, Raimund
IPC分类号： B01J27/198
CPC分类号： B01J8/10 , B01J8/067 , B01J19/22 , B01J27/198 , B01J35/023 , B01J35/026 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/08 , B01J37/14 , B01J37/18 , B01J2208/00849 , B01J2208/00876 , B01J2219/182 , C07C51/215 , C07C51/252 , C07C57/145

46. 发明公开

EP1487576A1 KATALYSATOR UND VERFAHREN ZUR HERSTELLUNG VON MALEINSÄUREANHYDRID 审中-公开
标题翻译：催化剂及其生产顺酐
公开(公告)号：EP1487576A1
公开(公告)日：2004-12-22
申请号：EP03708213.8
申请日：2003-03-12
申请人： BASF AKTIENGESELLSCHAFT
发明人： WEIGUNY, Jens , STORCK, Sebastian , DUDA, Mark , DOBNER, Cornelia
IPC分类号： B01J27/198 , B01J35/02 , B01J37/00 , C07C57/145
CPC分类号： B01J35/026 , B01J27/198 , B01J35/1014 , B01J35/1038 , B01J37/0009 , C07C51/215 , C07C57/145
摘要： The invention relates to a catalyst for producing maleic anhydride by the heterogeneous catalytic gas phase oxidation of a hydrocarbon having at least four carbon atoms. Said catalyst comprises a catalytically active mass containing vanadium, phosphorous and oxygen and has an essentially hollow-cylindrical structure with an outside diameter d1 and a diameter of the opening d2 that passes through said structure. The hollow cylindrical catalyst particles have a geometric density dp according to formula (I), in which parameter α equals 2.0 and parameter β equals 0.3. The invention also relates to a method for producing maleic anhydride on this catalyst.

47. 发明公开

EP1485203A1 KATALYSATOR-PRECURSOR FÜR DIE HERSTELLUNG VON MALEINSÄUREANHYDRID UND VERFAHREN ZU DESSEN HERSTELLUNG 审中-公开
标题翻译： KATALYSATOR-PRECURSORFÜRDIE HERSTELLUNG VON MALEINSURANHYDRID UND VERFAHREN ZU DESSEN HERSTELLUNG
公开(公告)号：EP1485203A1
公开(公告)日：2004-12-15
申请号：EP03744350.4
申请日：2003-03-12
申请人： BASF AKTIENGESELLSCHAFT
发明人： WEIGUNY, Jens , STORCK, Sebastian , DUDA, Mark , DOBNER, Cornelia
IPC分类号： B01J27/198 , B01J37/16 , B01J37/08 , C07C51/215 , C07C57/145 , B01J37/00
CPC分类号： C07C51/252 , B01J23/002 , B01J27/198 , B01J35/1014 , B01J35/1038 , B01J37/0009 , B01J37/009 , B01J37/08 , B01J2523/00 , C07C51/215 , C07C57/145 , B01J2523/51 , B01J2523/55
摘要： The invention relates to a method for producing a catalyst-precursor containing vanadium, phosphorous and oxygen for the production of maleic acid anhydride by means of heterogeneous catalytic gas phase oxidation of a hydrocarbon having at least four hydrocarbon atoms by reacting vanadium pentoxide (I) in the presence of a primary or secondary, non-cyclic or cyclic, non-branched or branched, saturated alcohol having 3 - 6 carbon atoms (II) with one five or 3-valent phosphorous compound (III) by agitating in a temperature range of between 80 - 160 °C and subsequently filtration of the obtained suspension, wherein a filtration resistance of αH.θ of ≤50.1013 mPa.s/m2 is adjusted by (a) the manner in which the phosphorous compound (III) and the vanadium pentoxide (I) are brought together in the presence of the alcohol (II), (b) by the influence of an agitator power of between 0.01 0.6 W/kg suspension and/or (c) by the filtration in a temperature range of between 65 °C - 160 °C. The invention also relates to a catalyst-precursor obtained according to said method for producing a catalyst from the catalyst-precursor, a catalyst which can be obtained according to said method, in addition to a method for producing maleic acid anhydride on said catalyst.
摘要翻译：本发明涉及一种生产含钒，磷和氧的催化剂前体用于生产马来酸酐的方法，该方法通过使五氧化二钒（I）与五氧化二钒（I）反应，通过多相催化气相氧化具有至少四个烃原子的烃（II）与一种五价或三价磷化合物（III）的伯或仲，非环状或环状，非支链或支链饱和醇通过在然后过滤得到的悬浮液，其中αH.θ的过滤阻力≤50.1013mPa.s/ m2通过（a）磷化合物（III）和五氧化钒（I）在醇（II）存在下聚集在一起，（b）通过0.01-0.6W / kg悬浮液之间的搅拌器功率和/或（c）通过65℃至65℃之间的温度范围 °C - 160°C。本发明还涉及一种催化剂前体，该催化剂前体除了在所述催化剂上生产马来酸酐的方法之外，还根据由所述催化剂前体制备催化剂的所述方法获得，催化剂可根据所述方法获得。

48. 发明授权

EP1261424B1 HOHLZYLINDERFÖRMIGER KATALYSATOR UND VERFAHREN ZUR HERSTELLUNG VON MALEINSÄUREANHYDRID 有权
标题翻译：中空的圆柱形催化剂及其制备方法顺酐
公开(公告)号：EP1261424B1
公开(公告)日：2004-06-09
申请号：EP01923638.9
申请日：2001-03-06
申请人： BASF AKTIENGESELLSCHAFT
发明人： WEIGUNY, Jens , STORCK, Sebastian , TENTEN, Andreas
IPC分类号： B01J27/198 , C07C51/215 , C07C51/25 , C07C57/145
CPC分类号： C07C51/215 , B01J23/002 , B01J27/198 , B01J35/026 , B01J35/1014 , B01J35/1038 , B01J2523/00 , C07C57/145 , B01J2523/51 , B01J2523/55

49. 发明授权

EP1628763B1 DREI- BZW. VIERSCHICHTIGE KATALYSATORSYSTEME ZUR HERSTELLUNG VON PHTHALSÄUREANHYDRID 有权
标题翻译：三，四层催化剂体系制备邻苯二甲酸酐
公开(公告)号：EP1628763B1
公开(公告)日：2007-09-12
申请号：EP04733250.7
申请日：2004-05-15
申请人： BASF Aktiengesellschaft
发明人： STORCK, Sebastian , ZÜHLKE, Jürgen , NETO, Samuel , ROSOWSKI, Frank
IPC分类号： B01J35/02 , C07C51/265
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/0006 , B01J35/10 , B01J35/1009 , B01J35/1014 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/51
摘要： The invention relates to catalyst systems for producing phthalic anhydride by means of gas phase oxidation of o-xylol and/or naphthalene, and to a method for producing phthalic anhydride while using these catalyst systems.

50. 发明公开

EP1814660A1 VERWENDUNG VON TITANDIOXIDGEMISCHEN ZUR HERSTELLUNG VON KATALYSATOREN 审中-公开
标题翻译：二氧化钛混合物用于催化剂的制备中使用
公开(公告)号：EP1814660A1
公开(公告)日：2007-08-08
申请号：EP05815892.4
申请日：2005-11-16
申请人： BASF AKTIENGESELLSCHAFT
发明人： NETO, Samuel , STORCK, Sebastian , ZÜHLKE, Jürgen , ROSOWSKI, Frank
IPC分类号： B01J23/00 , B01J23/22 , B01J21/06 , B01J35/00 , B01J35/10 , C07C51/00 , B01J37/02
CPC分类号： B01J21/063 , B01J23/002 , B01J23/22 , B01J35/0006 , B01J35/1014 , B01J37/0232 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/53 , B01J2523/55 , B01J2523/15 , B01J2523/47 , B01J2523/51
摘要： The invention relates to the use of titanium dioxide mixtures of the anatase form having defined physical properties for producing catalysts, which are particularly suitable for phthalic anhydride syntheses. The invention also relates to catalysts which contain titanium dioxide of the anatase form having defined physical properties.

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