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41. 发明专利

AU8255801A Process for preparation of fluorinated ketones 未知
公开(公告)号：AU8255801A
公开(公告)日：2002-03-13
申请号：AU8255801
申请日：2001-08-30
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , ITO MASAHIRO , SHIRAKAWA DAISUKE , TATEMATSU SHIN , TAKAGI HIROKAZU
IPC分类号： C07C45/54 , C07C51/09 , C07C67/287 , C07C69/708 , C07C49/167 , C07C51/58 , C07C59/135 , C07C67/14 , C07B39/00
摘要： The present invention provides a process whereby fluorinated ketones of various structures can be produced by short process steps and which is useful as an industrial production process. Namely, it is a process for producing a fluorinated ketone of the following formula (5), which comprises reacting a compound of the following formula (3) having a fluorine content of at least 30 mass%, with fluorine in a liquid phase to obtain a compound of the following formula (4), and then, subjecting the ester linkage of the compound of the formula (4) to a dissociation reaction: R COOCHR R R COOCFR R R R C=O wherein each of R and R are each a monovalent organic group such as an alkyl group, or R and R may be bonded to each other to form a bivalent organic group such as an alkylene group, R and R are a monovalent organic group such as a perfluoroalkyl group formed by fluorination of R and R , or they are bonded to each other to form a bivalent organic group such as a perfluoroalkylene group, and R and R are each a monovalent organic group such as a perfluoroalkyl group which may contain an etheric oxygen atom.

42. 发明专利

AU3610801A Process for preparing unsaturated compounds by pyrolysis 未知
公开(公告)号：AU3610801A
公开(公告)日：2001-12-17
申请号：AU3610801
申请日：2001-03-06
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , TATEMATSU SHIN , SATO MASAKUNI , MUROFUSHI HIDENOBU , YANASE KOICHI , SUZUKI YASUHIRO
IPC分类号： C07C41/18 , C07C43/17 , C07C43/172 , C07C41/01 , C07C27/00 , C07C51/58
摘要： The present invention produces an unsaturated compound (Formula 2) useful as a fluororesin starting material and the like by using a compound of the Formula 1 as a starting material. That is, the present invention provides a method for preparing a compound expressed by CR R =CR R (Formula 2) such as CF3CF2CF2OCF=CF2 by pyrolyzing a compound having at least one partial structure expressed by -COOCF2CR R -CXR R (Formula 1) such as CF3CF2CF2OCF(CF3)COOCF2CF(CF3)OCF2CF2CF3, wherein R to R are a hydrogen atom, a halogen atom or a monovalent organic group unchangeable by pyrolysis reaction.

43. 发明专利

CA1337434C PROCESS FOR PRODUCING 1,1,1,2-TETRAFLUOROETHANE 未知
公开(公告)号：CA1337434C
公开(公告)日：1995-10-24
申请号：CA603343
申请日：1989-06-20
申请人： ASAHI GLASS CO LTD
发明人： MORIKAWA SHINSUKE , SAMEJIMA SHUNICHI , YOSITAKE MASARU , TATEMATSU SHIN
IPC分类号： C07C17/23 , C07C19/08
摘要： 1. A process for producing 1,1,1,2-tetrafluoroethane, which comprises reacting 2,2-dichloro-1,1,1,2-tetrafluoroethane, 2-chloro-1,1,1,2-tetrafluoroethane or a mixture thereof with hydrogen in the presence of a hydrogenation catalyst consisting essentially of a Group VIII element as the main component and at least one element selected from the group consisting of Group IB elements, lanthanum and lanthanide elements, as an additional component.

44. 发明专利

DE3869920D1 未知
公开(公告)号：DE3869920D1
公开(公告)日：1992-05-14
申请号：DE3869920
申请日：1988-11-23
申请人： ASAHI GLASS CO LTD
发明人： MORIKAWA SHINSUKE , SAMEJIMA SHUNICHI , YOSHITAKE MASARU , TATEMATSU SHIN
IPC分类号： B01J23/02 , B01J21/02 , B01J23/26 , B01J23/74 , B01J23/745 , B01J23/75 , B01J23/755 , B01J27/125 , B01J27/128 , B01J27/132 , B01J27/138 , B01J37/22 , C07B61/00 , C07C17/00 , C07C17/20 , C07C17/358 , C07C19/08 , C07C19/12 , C07C67/00 , C07C22/00
摘要： A process for producing 1,1-dichloro-1,2,2,2-tetrafluoroethane which comprises isomerizing 1,1,2-trichloro-1,2,2-trifluoroethane to form 1,1,1-trichloro-2,2,2-trifluoroethane, followed by fluorination with hydrofluoric acid.

45. 发明专利

DE60140679D1 未知
公开(公告)号：DE60140679D1
公开(公告)日：2010-01-14
申请号：DE60140679
申请日：2001-08-30
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , ITO MASAHIRO , SHIRAKAWA DAISUKE , TATEMATSU SHIN , TAKAGI HIROKAZU
IPC分类号： C07C45/54 , C07B39/00 , C07C49/167 , C07C51/09 , C07C51/58 , C07C59/135 , C07C67/14 , C07C67/287 , C07C69/708
摘要： The present invention provides a process whereby fluorinated ketones of various structures can be produced by short process steps and which is useful as an industrial production process. Namely, it is a process for producing a fluorinated ketone of the following formula (5), which comprises reacting a compound of the following formula (3) having a fluorine content of at least 30 mass%, with fluorine in a liquid phase to obtain a compound of the following formula (4), and then, subjecting the ester linkage of the compound of the formula (4) to a dissociation reaction: R COOCHR R R COOCFR R R R C=O wherein each of R and R are each a monovalent organic group such as an alkyl group, or R and R may be bonded to each other to form a bivalent organic group such as an alkylene group, R and R are a monovalent organic group such as a perfluoroalkyl group formed by fluorination of R and R , or they are bonded to each other to form a bivalent organic group such as a perfluoroalkylene group, and R and R are each a monovalent organic group such as a perfluoroalkyl group which may contain an etheric oxygen atom.

46. 发明专利

AT450493T 未知
公开(公告)号：AT450493T
公开(公告)日：2009-12-15
申请号：AT01961220
申请日：2001-08-30
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , ITO MASAHIRO , SHIRAKAWA DAISUKE , TATEMATSU SHIN , TAKAGI HIROKAZU
IPC分类号： C07C45/54 , C07B39/00 , C07C49/167 , C07C51/09 , C07C51/58 , C07C59/135 , C07C67/14 , C07C67/287 , C07C69/708
摘要： The present invention provides a process whereby fluorinated ketones of various structures can be produced by short process steps and which is useful as an industrial production process. Namely, it is a process for producing a fluorinated ketone of the following formula (5), which comprises reacting a compound of the following formula (3) having a fluorine content of at least 30 mass%, with fluorine in a liquid phase to obtain a compound of the following formula (4), and then, subjecting the ester linkage of the compound of the formula (4) to a dissociation reaction: R COOCHR R R COOCFR R R R C=O wherein each of R and R are each a monovalent organic group such as an alkyl group, or R and R may be bonded to each other to form a bivalent organic group such as an alkylene group, R and R are a monovalent organic group such as a perfluoroalkyl group formed by fluorination of R and R , or they are bonded to each other to form a bivalent organic group such as a perfluoroalkylene group, and R and R are each a monovalent organic group such as a perfluoroalkyl group which may contain an etheric oxygen atom.

47. 发明专利

AT449056T 未知
公开(公告)号：AT449056T
公开(公告)日：2009-12-15
申请号：AT08014724
申请日：2001-07-26
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , ITO MASAHIRO , SHIRAKAWA DAISUKE , TATEMATSU SHIN
IPC分类号： C07C51/58 , C07C41/24 , C07C41/48 , C07C43/303 , C07C43/313 , C07C45/43 , C07C47/14 , C07C59/135 , C07D317/42 , C08F16/24 , C08F24/00
摘要： The present invention provides a novel process for preparing a fluorinated vinyl ether.

48. 发明专利

CA2381351C PROCESS FOR PRODUCING A VIC-DICHLORO ACID FLUORIDE 未知
公开(公告)号：CA2381351C
公开(公告)日：2009-11-17
申请号：CA2381351
申请日：2000-08-30
申请人： ASAHI GLASS CO LTD
发明人： ITO MASAHIRO , WATANABE KUNIO , OKAZOE TAKASHI , TATEMATSU SHIN , SHIRAKAWA DAISUKE
IPC分类号： C07C51/58 , C07C43/16 , C07C43/17 , C07C43/178 , C07C51/09 , C07C51/60 , C07C53/50 , C07C59/135 , C07C59/315 , C07C62/08 , C07C67/08 , C07C67/14 , C07C67/287 , C07C67/307 , C07C69/003 , C07C69/63 , C07C69/708 , C08G73/24
摘要： The process for producing a vic-dichloro acid fluoride compound in a short process and in good yield from the starting material which is inexpensive and readily available is provided. (R H1-E H1-)CR H2R H3CH2-OCOR HB (I) is fluorinated in a liquid phase to form (CF2C1CFC1-E F1-) CR F2R F3CF2-OCOR FB(II), and then, a n ester bond of the compound (II) is dessociated to form (CF2C1CFC1-E F1-)CR F2R F3COF (III) or the compound (III) and FCOR FB (IV).

49. 发明专利

CA2418118C PROCESSES FOR THE PREPARATION OF FLUORINATED ACYL FLUORIDES AND FLUORINATED VINYL ETHERS 未知
公开(公告)号：CA2418118C
公开(公告)日：2009-09-29
申请号：CA2418118
申请日：2001-07-26
申请人： ASAHI GLASS CO LTD
发明人： ITO MASAHIRO , TATEMATSU SHIN , SHIRAKAWA DAISUKE , OKAZOE TAKASHI , WATANABE KUNIO
IPC分类号： C07C51/58 , C07C41/24 , C07C41/48 , C07C43/303 , C07C43/313 , C07C45/43 , C07C47/14 , C07C59/135 , C07D317/42 , C08F16/24 , C08F24/00
摘要： The present invention provides novel processes for preparing a fluorinated acyl fluoride and a fluorinated vinyl ether. Namely, it provides a process for preparing a fluorinated acyl fluoride (3), which comprises reacting a compound (1) having a fluorine content of 30 mass% or above with fluorine in a liquid phase to form a compound (2) and then dissociating the ester bond in the compound (2), and a process for preparing a fluorinated vinyl ether (10), which comprises pyrolyzing the fluorinated acyl fluoride: (see formula 1) (see formula 2) (see formula 3) (see formula 10) wherein R A and R B are alkyl groups or the like, or the combination R A and R B is an ethereal oxygen-containing alkylene group or the like, R C and R D are perfluoro(ethereal oxygen-containing alkyl) groups or the like, or the combination of R C and R D is a perfluoro(ethereal oxygen-containing alkylene) group or the like, X1, X2, X3, X4, X5 and X6 are hydrogen atoms, fluorine atoms or the like, R AF, R BF, R CF and R DF are groups derived respectively from R A, R B, R C and R D by replacing substantially all of the hydrogen atoms by fluorine atoms.

50. 发明专利

CA2415620C METHOD FOR PRODUCING FLUORINE-CONTAINING COMPOUND 未知
公开(公告)号：CA2415620C
公开(公告)日：2009-09-08
申请号：CA2415620
申请日：2001-07-11
申请人： ASAHI GLASS CO LTD
发明人： OKAZOE TAKASHI , WATANABE KUNIO , OKAMOTO HIDEKAZU , SHIRAKAWA DAISUKE , ITO MASAHIRO , TATEMATSU SHIN , IWAYA MASAO
IPC分类号： C07C69/708 , C07C45/54 , C07C49/175 , C07C51/58 , C07C55/40 , C07C59/135 , C07C67/287 , C07C67/307 , C07C69/63
摘要： The present invention provides a method for obtaining a compound useful as a raw material for various fluororesins in high yield by a short process by using a starting material which is inexpensive and readily available. Namely, the present invention is characterized by reacting the following compound (1) with the following compound (2) to produce the following compound (3) having a fluorine content of at least 30 mass%, fluorinating the compound (3) in a liquid phase to produce the following compound (4), followed by a cleavage reaction of E F of the compound (4) to obtain a compound (5) and/or a compound (6): E1-R A-E1 (1) E2-R B (2) R B-E-R A-E-R B (3) R BF-E F-R AF-E F-R BF (4) E F1-R AF-E F1 (5) R BF-E F2 (6) wherein R A is a fluorine-containing bivalent organic group which is the same as R AF, or a bivalent organic group which will be converted to R AF by a fluorination reaction, and R B is a monovalent organic group which is the same as R BF, or a monovalent organic group which will be converted to R BF by a fluorination reaction, R AF is a fluorine-containing bivalent organic group which is the same as or different from R A, and when different, it is a group having R A fluorinated, R BF is a fluorine-containing monovalent organic group which is the same as or different from R B, and when different, it is a group having R B fluorinated, E1 and E2 are reactive groups which will react to each other to form a bivalent connecting group (E), E is a bivalent connecting group formed by the reaction of E1 and E2, E F is a group which is the same as E, or a group having E fluorinated, provided that at least one selected from R AF, R BF and E F, is a group formed by a fluorination reaction, and each of E F1 and E F2 which are independent from each other, is a group formed by cleavage of E F.

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