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31. 发明公开

EP0422202A4 OPACIFYING KAOLIN PIGMENTS AND PROCESS FOR MAKING SAME 失效
标题翻译：优选KAOLIN颜料及其制备方法
公开(公告)号：EP0422202A4
公开(公告)日：1992-09-02
申请号：EP90907663
申请日：1990-04-20
申请人： THIELE KAOLIN COMPANY
发明人： SHI, JOSEPH, C., S. , CURTIS, JERRY, L. , SALTER, TIMOTHY, L.
IPC分类号： C01B33/26 , C01B39/02 , C01B39/52 , C09C1/42 , D21H17/68 , D21H19/38 , D21H19/40 , C04B14/10
CPC分类号： C09C1/42 , C01P2006/60 , D21H17/68 , D21H19/40

32. 发明申请

WO2010037690A1 TEMPLATFREIE CLATHRASILE UND CLATHRASIL-MEMBRANEN 审中-公开
标题翻译：模板笼形硅和笼形硅滤膜
公开(公告)号：WO2010037690A1
公开(公告)日：2010-04-08
申请号：PCT/EP2009/062479
申请日：2009-09-28
申请人： BASF SE , VOSS, Hartwig , THERRE, Jörg , GIES, Hermann , MARLER, Bernd
发明人： VOSS, Hartwig , THERRE, Jörg , GIES, Hermann , MARLER, Bernd
IPC分类号： C01B37/00 , C01B37/02 , B01J29/03 , C01B39/52
CPC分类号： B01D71/027 , B01D53/047 , B01D53/228 , B01D67/0039 , B01D67/0051 , B01D69/02 , B01D71/028 , B01D2253/106 , B01D2256/24 , B01D2257/108 , B01D2257/11 , B01D2257/406 , B01D2257/80 , B01D2323/08 , B01D2323/10 , C01B37/00 , C01B37/02 , C01B39/52
摘要： Die vorliegende Erfindung betrifft templatfreie Clathrasile, deren Gerüst im Wesentlichen SiO 2 enthält, wobei die Kristalle der Clathrasile die plättchenförmige Morphologie der Schichtsilikate aufweisen. Ferner betrifft die vorliegende Erfindung ein Verfahren zur Herstellung dieser templatfreien Clathrasile, sowie deren Verwendung als Absorbens, als Seedkristalle für die Synthese von Clathrasil-Membranen des gleichen Zeolithtyps und in Form von dichten Schichten, die als molekular siebende Gastrennmembranen fungieren.
摘要翻译：本发明涉及模板笼形硅，所述主链基本上含有的SiO 2，其中所述笼形硅的晶体具有层状硅酸盐的板状形态。此外，本发明涉及一种用于制备这些模板笼形硅，以及它们作为吸收剂作为Seedkristalle对于相同沸石类型的笼形硅膜的合成，并且其中用作分子筛气体分离膜致密层的形式。

33. 发明授权

US10421666B2 Methods of controlling polymorphism in organic-free synthesis of Na-zeolites and zeolite crystals formed therefrom 有权
公开(公告)号：US10421666B2
公开(公告)日：2019-09-24
申请号：US15615969
申请日：2017-06-21
申请人： UNIVERSITY OF HOUSTON SYSTEM
发明人： Jeffrey D. Rimer , Miguel Maldonado , Matthew D. Oleksiak
IPC分类号： C01B39/46 , C01B39/52 , B01J29/70 , C01B39/02 , C01B39/50
摘要： Methods of controlling crystal polymorphism in organic-free synthesis of Na-Zeolites and the zeolite crystals formed using those methods are provided. The methods disclosed herein create certain types of zeolite crystals more efficiently than other previously known methods. The methods also create certain types of zeolite crystals in a form and concentration not previously disclosed. The methods disclosed herein generally comprise using solutions with varying ratios of silicon (Si), aluminum (Al), hydroxide (OH), and water. Some implementations of the invention disclosed include efficient methods of producing nearly pure cancrinite (CAN), methods of obtaining sodalite in solutions with a high Si/Al ratio, and a method of forming thin, platelet-like ANA crystals with a width of less than about 1 μm and a length of at least about 3 μm.

34. 发明授权

US09714174B2 Methods of controlling polymorphism in organic-free synthesis of Na-zeolites and zeolite crystals formed therefrom 有权
公开(公告)号：US09714174B2
公开(公告)日：2017-07-25
申请号：US13946919
申请日：2013-07-19
申请人： Jeffrey D. Rimer , Miguel Maldonado , Matthew D. Oleksiak
发明人： Jeffrey D. Rimer , Miguel Maldonado , Matthew D. Oleksiak
IPC分类号： C01B39/02 , C01B39/46 , C01B39/50 , C01B39/52
CPC分类号： C01B39/02 , C01B39/46 , C01B39/50 , C01B39/52 , C01P2004/20 , C01P2004/54
摘要： Methods of controlling crystal polymorphism in organic-free synthesis of Na-Zeolites and the zeolite crystals formed using those methods are provided. The methods disclosed herein create certain types of zeolite crystals more efficiently than other previously known methods. The methods also create certain types of zeolite crystals in a form and concentration not previously disclosed. The methods disclosed herein generally comprise using solutions with varying ratios of silicon (Si), aluminum (Al), hydroxide (OH), and water. Some implementations of the invention disclosed include efficient methods of producing nearly pure cancrinite (CAN), methods of obtaining sodalite in solutions with a high Si/Al ratio, and a method of forming thin, platelet-like ANA crystals with a width of less than about 1 μm and a length of at least about 3 μm.

35. 发明授权

US4938958A Antibiotic zeolite 失效
标题翻译：抗生素沸石
公开(公告)号：US4938958A
公开(公告)日：1990-07-03
申请号：US127645
申请日：1987-12-02
申请人： Reiji Niira, deceased , Tatuo Yamamoto , Masashi Uchida
发明人： Reiji Niira, deceased , Tatuo Yamamoto , Masashi Uchida
IPC分类号： C08K3/34 , A01N59/16 , A01N59/20 , A01N61/00 , C01B39/00 , C01B39/02 , C01B39/04 , C01B39/14 , C01B39/22 , C01B39/24 , C01B39/26 , C01B39/30 , C01B39/52 , C02F1/50 , C08K9/02 , C08K9/12 , C08L101/00 , C09D5/14 , D21H21/04 , D21H21/36
CPC分类号： D21H21/36 , A01N59/16 , A01N59/20 , C01B39/026 , C02F1/505 , C08K9/02 , C08K9/12 , C09D5/14 , D21H21/04
摘要： An antibiotic zeolite and an antibiotic resin composition containing thereof are provided. The antibiotic zeolite is prepared by replacing all or a part of ion-exchangeable ions in zeolite with ammonium ions and antibiotic metal ions such as silver, copper, zinc, mercury, tin, lead, bismuth, cadmium, chromium and thallium. The antibiotic resin composition comprises the antibiotic zeolite and a resin such as polyethylene, polypropylene, polyvinyl chloride and polystyrene.
摘要翻译：提供了含有抗生素沸石和抗生素树脂组合物。通过用铵离子和抗生素金属离子如银，铜，锌，汞，锡，铅，铋，镉，铬和铊替代沸石中的全部或一部分离子交换离子来制备抗生素沸石。抗生素树脂组合物包含抗生素沸石和聚乙烯，聚丙烯，聚氯乙烯和聚苯乙烯等树脂。

36. 发明授权

US4060590A Zeolite Nu-1 失效
标题翻译：沸石Nu-1
公开(公告)号：US4060590A
公开(公告)日：1977-11-29
申请号：US727773
申请日：1976-09-29
申请人： Thomas Vincent Whittam , Barry Youll
发明人： Thomas Vincent Whittam , Barry Youll
IPC分类号： C01B33/38 , B01J29/70 , C01B39/00 , C01B39/04 , C01B39/10 , C01B39/48 , C01B39/52 , C07C5/27 , C01B33/28 , B01J29/28
CPC分类号： C01B39/48 , B01J29/70 , C07C5/2737 , Y02P20/52
摘要： New zeolite "nu-1" has a silica to alumina ratio of 20 to 150 and a characteristic X-ray diffraction pattern and adsorption properties. It is made from a reaction mixture containing a methylated quaternary compound. In its hydrogen form it is highly active and selective in the isomerization of xylenes.
摘要翻译：新型沸石“nu-1”的二氧化硅与氧化铝的比例为20〜150，特征X射线衍射图和吸附性。由含有甲基化季铵化合物的反应混合物制成。在其氢形式中，其在二甲苯的异构化中是高活性和选择性的。

37. 发明授权

US08529868B2 ITQ-40, new crystalline microporous material 有权
标题翻译： ITQ-40，新型结晶微孔材料
公开(公告)号：US08529868B2
公开(公告)日：2013-09-10
申请号：US12968548
申请日：2010-12-15
申请人： Karl G. Strohmaier , Avelino Corma , Maria Jose Diaz , Fernando Rey , Douglas L. Dorset , Stuart L. Soled
发明人： Karl G. Strohmaier , Avelino Corma , Maria Jose Diaz , Fernando Rey , Douglas L. Dorset , Stuart L. Soled
IPC分类号： C01B39/00 , C01B39/04 , C01B39/46 , C01B39/52 , C01B39/54 , B01J29/06 , B01J29/70 , B01J20/28
CPC分类号： C01B39/54 , B01J20/28095 , B01J29/06 , B01J29/70 , C01B37/00 , C01B37/005 , C01B39/00 , C01B39/04 , C01B39/06 , C01B39/46 , C01B39/48 , C01B39/52
摘要： ITQ-40 (INSTITUTO DE TECNOLOGÍA QUÍMICA number 40) is a new crystalline microporous material with a framework of tetrahedral atoms connected by atoms capable of bridging the tetrahedral atoms, the tetrahedral atom framework being defined by the interconnections between the tetrahedrally coordinated atoms in its framework. ITQ-40 can be prepared in silicate compositions with an organic structure directing agent. It has a unique X-ray diffraction pattern, which identifies it as a new material.
摘要翻译： ITQ-40（INSTITUTO DETECNOLOGÍAQUÍMICA40号）是一种新的结晶微孔材料，其四面体原子框架由能够桥接四面体原子的原子连接，四面体原子框架由其框架中的四面体配位原子之间的互连。 ITQ-40可以用有机结构导向剂的硅酸盐组合物制备。它具有独特的X射线衍射图，将其识别为新材料。

38. 发明授权

US5340563A Preparation of zeolites using low silica/alumina zeolites as a source of aluminum 失效
标题翻译：使用低二氧化硅/氧化铝沸石作为铝源制备沸石
公开(公告)号：US5340563A
公开(公告)日：1994-08-23
申请号：US908680
申请日：1992-06-30
申请人： Stacey I. Zones , Yumi Nakagawa
发明人： Stacey I. Zones , Yumi Nakagawa
IPC分类号： B01J29/70 , C01B39/04 , C01B39/14 , C01B39/22 , C01B39/24 , C01B39/42 , C01B39/46 , C01B39/48 , C01B39/52 , C01B33/26
CPC分类号： B01J29/7034 , B01J29/70 , B01J29/7007 , B01J29/7038 , C01B39/04 , C01B39/42 , C01B39/48
摘要： An improved method of synthesizing large pore zeolites is disclosed and claimed. The method comprises preparing a reaction mixture containing a source zeolite on alkali metal, nitrogen containing organic cation, a source of silica, and water, and having the following composition in terms of the mole ratios:______________________________________ M.sup.+ /SiO.sub.2 = 0.01-1.00 OH.sup.- /SiO.sub.2 = 0.15-0.80 H.sub.2 O/SiO.sub.2 = 20-120 Q/SiO.sub.2 = 0.10-1.00 SiO.sub.2 /Y.sub.2 O.sub.3 = Greater Than 8 ______________________________________ wherein M.sup.+ is an alkali metal not supplied by the source zeolite, Q is an organic template, and Y is a mixture of aluminum from the source zeolite, wherein said source zeolite contains soda lite substructures having tetrahedra atom densities of less than about 15 TO.sub.2 per 1000 .ANG..sup.3 ; maintaining the reaction mixture at crystallization temperature until crystals are formed; and recovering the crystals.
摘要翻译：公开并要求保护合成大孔沸石的改进方法。该方法包括制备含有碱金属源氮沸石，含氮有机阳离子，二氧化硅源和水的反应混合物，按摩尔比计算以下组成：-M + / SiO 2 = 0.01-1.00 -OH - / SiO2 = 0.15-0.80 -H2O / SiO2 = 20-120 -Q / SiO2 = 0.10-1.00 -SiO2 / Y2O3 =大于8 - 其中M +是不由源沸石供应的碱金属，Q是有机模板，Y是来自沸石的铝的混合物，其中所述源沸石含有具有小于约15 TO2 / 1000 ANGSTROM 3的四面体原子密度的苏打液晶结构; 将反应混合物保持在结晶温度直到形成晶体; 并回收晶体。

39. 发明授权

US5071801A High density leucite based ceramics from zeolite 失效
标题翻译：来自沸石的高密度白云母基陶瓷
公开(公告)号：US5071801A
公开(公告)日：1991-12-10
申请号：US557347
申请日：1990-07-25
申请人： Robert L. Bedard , Edith M. Flanigen
发明人： Robert L. Bedard , Edith M. Flanigen
IPC分类号： B01J20/02 , B01J29/04 , C01B25/45 , C01B37/00 , C01B39/06 , C01B39/46 , C01B39/52 , C01B39/54 , C04B35/19 , C07B61/00 , C10G45/12 , C10G47/16 , C10G47/20 , C10G49/08
CPC分类号： C04B35/19
摘要： This invention relates to processes for preparing ceramic articles. One process involves taking a potassium exchanged zeolite, the zeolite characterized in that it has a SiO.sub.2 /Al.sub.2 O.sub.3 ratio of 3.5 to about 7.5, and calcining it at a temperature of about 900.degree. to about 1100.degree. C. for a time sufficient to collapse the zeolite framework and provide an amorphous powder. Next, the amorphous powder is formed into a shaped article and the article is sintered at a temperature of about 1150.degree. to about 1400.degree. C. for a time of about 0.5 to about 12 hours to give a ceramic article whose principal crystalline phase is tetragonal leucite, is substantially crack free, and has less than 5% porosity. When the zeolite is exchanged with cesium, one obtains a ceramic article whose principal crystalline phase is pollucite, when a rubidium exchanged zeolite is used one obtains a ceramic article whose principal crystalline phase is rubidium leucite, and when a potassium/cesium exchanged zeolite is used one obtains a ceramic article having as its principal crystalline phase a leucite/pollucite solid solution. The addition of pollucite to the leucite article provides a ceramic article whose thermal expansion coefficient can be varied from about 2.times.10.sup.-6 to about 27.times.10.sup.-60 C.sup.-1 as measured over the range 50.degree.-700.degree. C. This invention also relates to this leucite/pollucite ceramic article.
摘要翻译：本发明涉及制备陶瓷制品的方法。一个方法涉及获得钾交换的沸石，该沸石的特征在于其SiO 2 / Al 2 O 3比为3.5至约7.5，并在约900℃至约1100℃的温度下煅烧足够的时间，沸石骨架，并提供无定形粉末。接下来，将无定形粉末形成为成型制品，并将制品在约1150℃至约1400℃的温度下烧结约0.5至约12小时，得到其主晶相为四方晶的陶瓷制品白云母基本上无裂纹，孔隙率小于5％。当沸石与铯交换时，得到主要结晶相为铯原子的陶瓷制品，当使用铷交换的沸石时，得到主要结晶相为铷白云母的陶瓷制品，并且当使用钾/铯交换的沸石时得到具有白云母/琉璃灰固体溶液的陶瓷制品的主要结晶相。将白矾石添加到白云石制品中提供了陶瓷制品，其热膨胀系数可以在50-700℃下测量的约2×10-6至约27×10-60℃-1变化。本发明还涉及这种白云母 /琉璃陶瓷制品。

40. 发明授权

US4861739A Microporous crystalline composite compositions 失效
标题翻译：微孔结晶复合组合物
公开(公告)号：US4861739A
公开(公告)日：1989-08-29
申请号：US058259
申请日：1987-06-04
申请人： Regis J. Pellet , Peter K. Coughlin , Albert R. Springer , Richard T. Gajek
发明人： Regis J. Pellet , Peter K. Coughlin , Albert R. Springer , Richard T. Gajek
IPC分类号： C01B25/36 , B01J29/00 , B01J29/08 , B01J29/83 , B01J29/84 , B01J29/85 , C01B25/45 , C01B37/04 , C01B37/06 , C01B37/08 , C01B39/00 , C01B39/06 , C01B39/14 , C01B39/24 , C01B39/26 , C01B39/28 , C01B39/30 , C01B39/36 , C01B39/38 , C01B39/42 , C01B39/52 , C10G29/04
CPC分类号： B01J29/005 , B01J29/084 , B01J29/83 , B01J29/84 , B01J29/85 , C10G2400/10
摘要： The invention involves composite structures of multiple phases, at least two of which are inorganic crystalline compositions that are contiguous and have a common crystal framework and structure, and at least one of them contains phosphorus and aluminum atoms as part of its crystalline framework structure; and to processes for making the same. It is desired that each phase has a microporous molecular sieve structure. The process involves the growth of a crystalline structure constituting such a phase in the presence of crystals of another of such a phase. Preferably, the process involves a hydrothermal crystallization treatment of the precursors to such phase.

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