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31. 发明授权

US4837000A Crystalline silicates and process for the production thereof 失效
标题翻译：结晶硅酸盐及其制备方法
公开(公告)号：US4837000A
公开(公告)日：1989-06-06
申请号：US940578
申请日：1986-12-11
申请人： Kozo Takatsu , Noboru Kawata
发明人： Kozo Takatsu , Noboru Kawata
IPC分类号： C01B39/04 , B01J29/00 , B01J29/70 , C01B39/48 , C07C1/20
CPC分类号： B01J29/70 , C01B33/2869 , C01B39/48 , C07C1/20 , C07C2529/06 , Y02P30/42 , Y10S423/36
摘要： Crystalline silicates and processes for the production thereof are described. These crystalline silicates are of new crystalline structure, which, as determined after calcination in the air at 550.degree. C., have a composition represented by the general formula (I): pM.sub.2/n O.Al.sub.2 O.sub.3.qSiO.sub.2 (the symbols are as defined in the appended claims) and give a X-ray diffraction pattern as shown in Table 2. They are superior in heat resistance and acid resistance, and can be used as catalysts for the conversion of various organic compounds, absorbents, or as catalysts for various reactions. They are produced by reacting an aqueous mixture comprising (a) a silica source, (b) an alumina source, (c) an alkali metal and/or alkaline earth metal source, and monoethanolamine at a temperature of 100.degree. to 300.degree. C. until the desired crystalline silicates are formed. Although monoethanolamine does not remain in the crystalline silicates, it plays an important role in the formation of the desired crystalline structure in the course of the production thereof.

32. 发明授权

US4657750A Process for the production of crystalline silicate ISI-4 using ethylene glycol 失效
标题翻译：使用乙二醇生产结晶硅酸盐ISI-4的方法
公开(公告)号：US4657750A
公开(公告)日：1987-04-14
申请号：US713086
申请日：1985-03-18
申请人： Kozo Takatsu , Noboru Kawata
发明人： Kozo Takatsu , Noboru Kawata
IPC分类号： C01B39/04 , B01J29/00 , B01J29/70 , C01B39/48 , C07C1/20 , C01B33/28
CPC分类号： B01J29/70 , C01B33/2869 , C01B39/48 , C07C1/20 , C07C2529/06 , Y02P30/42 , Y10S423/36
摘要： Crystalline silicates and processes for the production thereof are described. These crystalline silicates are of new crystalline structure, which, as determined after calcination in the air at 550.degree. C., have a composition represented by the general formula (I): pM.sub.2/n O.Al.sub.2 O.sub.3.qSiO.sub.2 (the symbols are as defined in the appended claims) and give a X-ray diffraction pattern as shown in Table 2. They are superior in heat resistance and acid resistance, and can be used as catalysts for the conversion of various organic compounds, absorbents, or as catalysts for various reactions. They are produced by reacting an aqueous mixture comprising (a) a silica source, (b) an alumina source, (c) an alkali metal and/or alkaline earth metal source, and (d) ethylene glycol or (e) monoethanolamine at a temperature of 100.degree. to 300.degree. C. till the desired crystalline silicates are formed. Although ethylene glycol and monoethanolamine do not remain in the crystalline silicates, they play important roles in the formation of the desired crystalline structure in the course of the production thereof.
摘要翻译：描述了结晶硅酸盐及其生产方法。这些结晶硅酸盐具有新的结晶结构，其在550℃下在空气中煅烧后测定，具有由通式（I）表示的组成：pM2 / nO.Al2O3.qSiO2（符号如所附权利要求书），得到如表2所示的X射线衍射图案。它们的耐热性和耐酸性优异，可用作各种有机化合物，吸收剂或用于各种反应的催化剂的转化催化剂。它们是通过使含有（a）二氧化硅源，（b）氧化铝源，（c）碱金属和/或碱土金属源，（d）乙二醇或（e）单乙醇胺的二氧化硅源，温度在100℃至300℃直到形成所需的结晶硅酸盐。尽管乙二醇和单乙醇胺不残留在结晶硅酸盐中，但是在制备期望的晶体结构的形成中起重要作用。

33. 发明授权

US4500419A Catalysis over activated zeolites 失效
公开(公告)号：US4500419A
公开(公告)日：1985-02-19
申请号：US552541
申请日：1983-11-16
申请人： Joseph N. Miale , Clarence D. Chang
发明人： Joseph N. Miale , Clarence D. Chang
IPC分类号： B01J29/40 , B01J29/65 , B01J29/70 , B01J37/26 , C10G11/05 , C10G11/08 , C10G45/54
CPC分类号： B01J37/26 , B01J29/40 , B01J2229/26 , B01J2229/42 , B01J29/65 , B01J29/70 , Y10S423/22 , Y10S423/23 , Y10S423/29 , Y10S423/33 , Y10S423/36
摘要： A process is provided for conducting organic compound conversion over a catalyst composition comprising a supported crystalline zeolite having a high initial silica-to-alumina mole ratio, said supported zeolite being prepared by compositing said crystalline zeolite with alumina, reacting the composite with a particular hydrogen fluoride solution in a specified way, drying the hydrogen fluoride reacted composite, treating the dried composite by hydrolysis, ammonolysis and/or by contact with an ammonium salt solution, and calcining the resulting material.

34. 发明授权

US4427789A Activation of zeolites 失效
标题翻译：活化沸石
公开(公告)号：US4427789A
公开(公告)日：1984-01-24
申请号：US355416
申请日：1982-03-08
申请人： Joseph N. Miale , Clarence D. Chang
发明人： Joseph N. Miale , Clarence D. Chang
IPC分类号： B01J29/40 , B01J29/65 , B01J29/70 , B01J37/26 , B01J29/28
CPC分类号： B01J37/26 , B01J29/40 , B01J2229/26 , B01J2229/42 , B01J29/65 , B01J29/70 , Y10S423/22 , Y10S423/23 , Y10S423/29 , Y10S423/33 , Y10S423/36
摘要： A method for enhancing the activity of a crystalline zeolite, including a zeolite having a silica-to-alumina ratio greater than 100, is disclosed which involves compositing and extruding the zeolite with an alumina support matrix, vacuum impregnating the extrudate with an aqueous solution of an alkali metal fluoride, contacting the impregnated extrudate with a warm aqueous solution of an ammonium salt and then calcining the final product.
摘要翻译：公开了一种提高结晶沸石的活性的方法，其包括二氧化硅与氧化铝比大于100的沸石，其包括用氧化铝载体基质复合和挤出沸石，用水溶液浸渍挤出物碱金属氟化物，使浸渍的挤出物与温和的铵盐水溶液接触，然后煅烧最终产物。

36. 发明专利

JPH11511720A The method of manufacturing a zeolite having a mtt crystal structure using the small, neutral amine 失效
公开(公告)号：JPH11511720A
公开(公告)日：1999-10-12
申请号：JP52845896
申请日：1996-03-08
申请人：シェブロンユー.エス.エー.インコーポレイテッド
发明人：ナカガワ，ユミ
IPC分类号： C01B39/48
CPC分类号： C01B39/48 , Y10S423/36
摘要： (57)【要約】本発明は、ゼオライトを形成することができる小さい中性アミンを用いる、例えばゼオライトＳＳＺ−３２及びＺＳＭ-２３のようなＭＴＴ結晶構造を有するゼオライトの製造方法であって、前記アミンが（ａ）炭素、窒素及び水素原子のみを含有し、（ｂ）１個の第１級、第２級又は第３級の、第４級ではないアミノ基を含有し、（ｃ）第３級窒素原子、少なくとも１個の第３級炭素原子、又は少なくとも１個の第２級炭素原子に直接結合した窒素原子を含有するアミン（例えば、イソブチルアミン、ジイソブチルアミン、ジイソプロピルアミン又はトリメチルアミン）であり、第４級アンモニウム化合物の不存在下でおこなわれる方法に関する。

37. 发明授权

KR101285526B1 질소-함유 유기 화합물을 이용한 ＭＴＴ 제올라이트의제조방법 有权
标题翻译：使用含有有机化合物的含氮有机化合物制备MTT沸石的方法
公开(公告)号：KR101285526B1
公开(公告)日：2013-07-17
申请号：KR1020087007471
申请日：2006-08-15
申请人： 셰브런 유.에스.에이.인크.
发明人： 버튼알렌더블유쥬니어 , 존스스테이시아이
IPC分类号： C01B39/48 , C01B39/00
CPC分类号： C01B39/48 , C01B39/12 , Y10S423/36
摘要： 본 발명은 특정 질소-함유 유기 화합물을 이용하여 제올라이트 SSZ-32 및 ZSM-23과 같은 제올라이트에 존재하는 사면체 원자들의 연결지수로 정의되는 MTT 구조 위상을 갖는 제올라이트를 제조하는 방법에 관한 것이다.
제올라이트, 사면체, 원자, 구조 위상, 질소함유 유기화합물

38. 发明授权

EP1928786B1 PROCESSES FOR PREPARING MTT ZEOLITES USING NITROGEN-CONTAINING ORGANIC COMPOUNDS 有权转让
标题翻译：于制备MTT沸石使用含氮有机化合物
公开(公告)号：EP1928786B1
公开(公告)日：2016-12-28
申请号：EP06801642.7
申请日：2006-08-15
申请人： Chevron U.S.A. Inc.
发明人： BURTON, Allen, W., Jr. , ZONES, Stacey, I.
IPC分类号： C01B39/48 , C01B39/12
CPC分类号： C01B39/48 , C01B39/12 , Y10S423/36

39. 发明公开

EP1928786A1 PROCESSES FOR PREPARING MTT ZEOLITES USING NITROGEN-CONTAINING ORGANIC COMPOUNDS 有权转让
标题翻译：于制备MTT沸石使用含氮有机化合物
公开(公告)号：EP1928786A1
公开(公告)日：2008-06-11
申请号：EP06801642.7
申请日：2006-08-15
申请人： Chevron U.S.A., Inc.
发明人： BURTON, Allen, W., Jr. , ZONES, Stacey, I.
IPC分类号： C01B39/48
CPC分类号： C01B39/48 , C01B39/12 , Y10S423/36
摘要： The present invention relates to a process for preparing zeolites having the MTT framework topology defined by the connectivity of the tetrahedral atoms in the zeolite, such as zeolites SSZ-32 and ZSM-23, using certain nitrogen-containing organic compounds.

40. 发明授权

EP1088791B1 Procédé de preparation de zeolithes de type structural MTT utilisant des precurseurs specifiques du structurant 有权
标题翻译：一种用于通过所述结构化剂的具体前体的方法制备的MTT型沸石的过程
公开(公告)号：EP1088791B1
公开(公告)日：2003-11-26
申请号：EP00402598.7
申请日：2000-09-20
申请人： Institut Français du Pétrole
发明人： Rouleau, Loic , Kolenda, Frédéric , Benazzi, Eric
IPC分类号： C01B39/48 , B01J20/18 , B01J29/04 , C10G45/64
CPC分类号： B01J20/18 , B01J29/04 , C01B39/48 , C10G45/64 , Y10S423/36

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