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31. 发明授权

US2240275A Highly branched brominated organic acids and their esters 失效
标题翻译：高分支溴化有机酸及其酯
公开(公告)号：US2240275A
公开(公告)日：1941-04-29
申请号：US22928438
申请日：1938-09-10
申请人： MALLINCKRODT CHEMICAL WORKS
发明人： WHITMORE FRANK C , HOMEYER AUGUST H
IPC分类号： C07C51/04 , C07C51/09 , C07C51/15 , C07C51/363 , C07C51/38 , C07C51/60 , C07C51/62 , C07C53/23 , C07C55/32 , C07C57/58 , C07C59/135 , C07C59/68
CPC分类号： C07C59/68 , C07C51/04 , C07C51/09 , C07C51/15 , C07C51/363 , C07C51/38 , C07C51/60 , C07C51/62 , C07C53/23 , C07C55/32 , C07C57/58 , C07C59/135 , C07C53/19 , C07C55/02 , C07C53/126 , C07C53/42 , C07C53/46

32. 发明申请

WO2006045518A1 VERFAHREN ZUR GASTRENNUNG 审中-公开
标题翻译：工艺气体分离
公开(公告)号：WO2006045518A1
公开(公告)日：2006-05-04
申请号：PCT/EP2005/011267
申请日：2005-10-20
申请人： SOLVAY FLUOR GMBH , OLSCHIMKE, Jens , BRAUKMÜLLER, Saskia , BROSCH, Carsten
发明人： OLSCHIMKE, Jens , BRAUKMÜLLER, Saskia , BROSCH, Carsten
IPC分类号： C01B7/07 , C01B7/09 , B01D53/14 , C01B7/19 , C07C51/64 , C07D233/54
CPC分类号： C01B7/0737 , B01D53/1456 , B01D53/1493 , B01D2257/2042 , B01D2257/2045 , C01B7/0731 , C01B7/093 , C01B7/195 , C07C51/47 , C07D233/64 , C07C53/48 , C07C53/46 , C07C53/40
摘要： Gasgemische, die HF, HCI oder HBr und andere Bestandteile enthalten, insbesondere solche Gasgemische, die Carbonsäurefluoride, C(0)F 2 oder Phosphorpentafluorid sowie HCI und gegebenenfalls HF enthalten, können mittels ionischer Flüssigkeiten aufgetrennt werden.
摘要翻译：含有HF，HCl或HBr和其它成分的气体混合物，特别是含有羧酸氟化物的那些气体混合物，C（O）R _{2 或五氟化磷和HCl和任选的HF，可以通过离子液体的方法分离。}

33. 发明申请

WO1998024750A1 PRODUCTION OF CARBOXYLIC ACID FLUORIDES 审中-公开
标题翻译：生产碳素酰基氟
公开(公告)号：WO1998024750A1
公开(公告)日：1998-06-11
申请号：PCT/EP1997006647
申请日：1997-11-28
申请人： SOLVAY FLUOR UND DERIVATE GMBH , BRAUN, Max , EICHHOLZ, Kerstin , RUDOLPH, Werner
发明人： SOLVAY FLUOR UND DERIVATE GMBH
IPC分类号： C07C51/58
CPC分类号： C07C51/60 , B01J19/02 , B01J19/123 , B01J2219/00078 , B01J2219/0245 , B01J2219/0254 , B01J2219/0875 , C07C51/58 , C07C53/50 , C07C53/48 , C07C53/46
摘要： The invention relates to a method for the production of carboxylic acid fluorides of the formula RCFXC(O)F, wherein X designates F or Cl. Compounds of the formula RCFXCHFCl are reacted with oxygen by photochemical oxidation in the gaseous phase. This yields good quantities of highly selective carboxylic acid fluorides. It is preferable to work under sensitization with chlorine and light at a wavelength of lambda >/=280 nm. This makes it possible to work without the use of pressure. Glass apparatus may be covered with a protective coating so as to protect it against traces of hydrogen fluoride. To this end, for example, heat-shrinkable sleeves made of translucent hydrogen fluoride-resistant material may be used. Polytetrafluoroethylene, polyfluoropropylene or a mixture thereof are especially suitable for this purpose. This type of protection is also suited for other reactions, such as photo-induced fluoro-dediazonation in hydrogen fluoride/pyridine for the production of aromatic compounds fluorinated in the nucleus or the oxidation of CHCL2 groups for the production of carboxylic acid fluorides.
摘要翻译：公开的是用于制备式RCFXC（O）F，其中X是F或Cl的羧酸氟化物的方法。反应与氧气式RCFXCHFCl的化合物转化成在气相中的光化学氧化。形成以良好的收率和高选择性的羧酸氟化物。优选在敏化进行与波长为λ的氯和光> / = 280纳米。这是可能的，而不的工作压力。玻璃装置可被提供用于防止RF迹线以保护涂层。对于这一个就可以了，例如，热收缩使用耐HF，半透明材料制成。作为该材料聚四氟乙烯，Polyfluorpropylen或它们的混合物是特别合适的。这种保护也适用于其它反应，例如，光诱导氟dediazoniation在氟化氢/吡啶生产核氟化的芳族化合物的或CHCl 2的基团为羧酸氯化物的制剂的目的氧化的目的。

34. 发明申请

WO2019113435A1 PROCESS FOR THE PREPARATION OF A 1,3-DISUBSTITUTED PYRAZOLE COMPOUND 审中-公开
公开(公告)号：WO2019113435A1
公开(公告)日：2019-06-13
申请号：PCT/US2018/064460
申请日：2018-12-07
申请人： VERTEX PHARMACEUTICALS INCORPORATED
发明人： BLIGH, Cavan, McKeon , COURT, John, J. , LIANG, Jianglin , O'DOWD, Hardwin , ROEPER, Stefanie , RYAN, Michael, P.
IPC分类号： C07D401/04 , C07C231/02 , C07C53/46
CPC分类号： C07D401/04 , B01D9/005 , C07C53/44 , C07C53/46
摘要： The disclosure provides a process for preparing a compound of formula (I) or a pharmaceutically acceptable salt thereof.

35. 发明申请

WO2009013198A1 PROCESS FOR OBTAINING A PURIFIED HYDROFLUOROALKANE 审中-公开
标题翻译：获得纯化氢氟烷的方法
公开(公告)号：WO2009013198A1
公开(公告)日：2009-01-29
申请号：PCT/EP2008/059285
申请日：2008-07-16
申请人： SOLVAY FLUOR GmbH , UENVEREN, Ercan , HAUSMANN, Eckhard , EICHER, Johannes , EICHHOLZ, Kerstin
发明人： UENVEREN, Ercan , HAUSMANN, Eckhard , EICHER, Johannes , EICHHOLZ, Kerstin
IPC分类号： C07C17/395 , C07C19/08 , C07C51/58 , C07C53/48
CPC分类号： C07C17/395 , C07C51/58 , C07C19/08 , C07C53/46 , C07C53/48
摘要： The invention consequently relates, in one aspect, to a process for obtaining a hydrofluoroalkane comprising at least two carbon atoms, which is purified of unsaturated organic impurities, according to which the hydrofluoroalkane containing organic impurities including (chloro)fluoro olefins is subjected to at least one purification treatment with bromine or BrCl, preferably in the presence of an initiator. The process is suitable, for example, to purify 1,1,1,2-tetrafluoroethane. A further aspect concerns the application of LEDs or OLEDs to support chemical reactions of the gas-gas, liquid-liquid or gas-liquid type, and a respective reactor.
摘要翻译：因此，本发明在一方面涉及一种获得含有至少两个碳原子的氢氟烷烃的方法，该方法是不饱和有机杂质的纯化，根据该方法，含有（氯）氟烯烃的有机杂质的含氟氟烷烃至少经受用溴或BrCl进行一次净化处理，优选在引发剂存在下进行。该方法例如用于纯化1,1,1,2-四氟乙烷是合适的。另一方面涉及LED或OLED的应用以支持气体，液体或气液型以及相应的反应器的化学反应。

36. 发明申请

US20100181186A1 Process for obtaining a purified hydrofluoroalkane 审中-公开
标题翻译：获得纯化氢氟烷烃的方法
公开(公告)号：US20100181186A1
公开(公告)日：2010-07-22
申请号：US12668779
申请日：2008-07-16
申请人： Ercan Uenveren , Eckhard Hausmann , Johannes Eicher , Kerstin Eichholz
发明人： Ercan Uenveren , Eckhard Hausmann , Johannes Eicher , Kerstin Eichholz
IPC分类号： C01B7/01 , C07C17/38 , C07C17/00 , B01J19/08
CPC分类号： C07C17/395 , C07C51/58 , C07C19/08 , C07C53/46 , C07C53/48
摘要： The invention consequently relates, in one aspect, to a process for obtaining a hydrofluoroalkane comprising at least two carbon atoms, which is purified of unsaturated organic impurities, according to which the hydrofluoroalkane containing organic impurities including (chloro)fluoro olefins is subjected to at least one purification treatment with bromine or BrCl, preferably in the presence of, an initiator. The process is suitable, for example, to purify 1,1,1,2-tetrafluoroethane. A further aspect concerns the application of LEDs or OLEDs to support chemical reactions of the gas-gas, liquid-liquid or gas-liquid type, and a respective reactor.
摘要翻译：因此，本发明在一方面涉及一种获得含有至少两个碳原子的氢氟烷烃的方法，该方法是不饱和有机杂质的纯化，根据该方法，含有（氯）氟烯烃的有机杂质的含氟氟烷烃至少经受用溴或BrCl进行一次净化处理，优选在引发剂存在下进行。该方法例如用于纯化1,1,1,2-四氟乙烷是合适的。另一方面涉及LED或OLED的应用以支持气体，液体或气液型以及相应的反应器的化学反应。

37. 发明授权

US07161025B2 Method for producing a fluorinated ester compound 有权
标题翻译：氟化酯化合物的制造方法
公开(公告)号：US07161025B2
公开(公告)日：2007-01-09
申请号：US11105518
申请日：2005-04-14
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Koichi Yanase , Yasuhiro Suzuki , Daisuke Shirakawa
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Koichi Yanase , Yasuhiro Suzuki , Daisuke Shirakawa
IPC分类号： C07C69/63
CPC分类号： C07C67/287 , C07C41/06 , C07C51/60 , C07C67/14 , C07C67/297 , C07C53/50 , C07C53/46 , C07C59/135 , C07C69/708 , C07C69/63 , C07C43/178
摘要： The present invention provides a method for producing industrially useful fluorine-containing compounds such as a fluorinated ester compound and an acid fluoride compound.Namely, the present invention resides in a method for producing a fluorinated ester compound, which comprises fluorinating an ester compound which is an ester of a compound having hydroxyl group(s) with a compound having acyl fluoride group(s) and which has a structure which can be fluorinated, in a liquid phase to produce a fluorinated ester compound, wherein the fluorination is carried out in the form of a liquid mixture of the ester compound and the compound having acyl fluoride group(s).
摘要翻译：本发明提供了一种制造工业上有用的含氟化合物如氟化酯化合物和酰氟化合物的方法。即，本发明涉及氟化酯化合物的制造方法，其特征在于，将具有羟基的化合物的酯化合物与具有酰氟基的化合物氟化，并且具有结构其可以在液相中被氟化以产生氟化酯化合物，其中氟化是以酯化合物和具有酰氟基团的化合物的液体混合物的形式进行的。

38. 发明授权

US07053238B2 Process for producing fluorinated polyvalent carbonyl compound 失效
公开(公告)号：US07053238B2
公开(公告)日：2006-05-30
申请号：US10891155
申请日：2004-07-15
申请人： Takashi Okazoe , Kunio Watanabe , Daisuke Shirakawa , Masahiro Ito , Shin Tatematsu
发明人： Takashi Okazoe , Kunio Watanabe , Daisuke Shirakawa , Masahiro Ito , Shin Tatematsu
IPC分类号： C07C69/63
CPC分类号： C07C67/14 , C07C45/54 , C07C51/60 , C07C67/287 , C07C67/29 , C07C67/297 , C07C67/307 , C07C59/21 , C07C53/46 , C07C69/63
摘要： A fluorinated polyvalent carbonyl compound is produced by an economically advantageous method from inexpensive materials without requiring a complicated synthetic process step. Namely, the present invention comprises reacting a polyvalent alcohol having at least two kinds of alcohol skeletons selected among a primary alcohol, a secondary alcohol and a tertiary alcohol, with an acid halide to obtain a polyvalent ester compound, fluorinating it in a liquid phase to obtain a perfluorinated polyvalent ester compound, and cleaving the ester bonds derived from primary and secondary alcohols in the perfluoropolyvalent ester compound to obtain a fluorinated polyvalent carbonyl compound.

39. 发明申请

US20050192456A1 Method for producing a fluorinated ester compound 有权
标题翻译：氟化酯化合物的制造方法
公开(公告)号：US20050192456A1
公开(公告)日：2005-09-01
申请号：US11105518
申请日：2005-04-14
申请人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Koichi Yanase , Yasuhiro Suzuki , Daisuke Shirakawa
发明人： Takashi Okazoe , Kunio Watanabe , Shin Tatematsu , Koichi Yanase , Yasuhiro Suzuki , Daisuke Shirakawa
IPC分类号： C07C41/06 , C07C43/178 , C07C51/60 , C07C67/14 , C07C67/287 , C07C67/297 , C07C69/63
CPC分类号： C07C67/287 , C07C41/06 , C07C51/60 , C07C67/14 , C07C67/297 , C07C53/50 , C07C53/46 , C07C59/135 , C07C69/708 , C07C69/63 , C07C43/178
摘要： The present invention provides a method for producing industrially useful fluorine-containing compounds such as a fluorinated ester compound and an acid fluoride compound. Namely, the present invention resides in a method for producing a fluorinated ester compound, which comprises fluorinating an ester compound which is an ester of a compound having hydroxyl group(s) with a compound having acyl fluoride group(s) and which has a structure which can be fluorinated, in a liquid phase to produce a fluorinated ester compound, wherein the fluorination is carried out in the form of a liquid mixture of the ester compound and the compound having acyl fluoride group(s).
摘要翻译：本发明提供了一种制造工业上有用的含氟化合物如氟化酯化合物和酰氟化合物的方法。即，本发明涉及氟化酯化合物的制造方法，其特征在于，将具有羟基的化合物的酯化合物与具有酰氟基的化合物氟化，并且具有结构其可以在液相中被氟化以产生氟化酯化合物，其中氟化是以酯化合物和具有酰氟基团的化合物的液体混合物的形式进行的。

40. 发明授权

US3905800A Quinazolinones as novel herbicides 失效
标题翻译：喹唑啉酮作为新型除草剂
公开(公告)号：US3905800A
公开(公告)日：1975-09-16
申请号：US42297073
申请日：1973-12-07
申请人： PFIZER
发明人： DOMINY BERYL WILLIAM , HESS HANS-JURGEN ERNST , KOCH RICHARD CARL
IPC分类号： C07C53/21 , C07C53/46 , A01N9/22
CPC分类号： C07C53/21 , C07C53/46
摘要： Substituted 4(3H)-quinazolinones of the formulae

AND THE ALKALI METAL AND ALKYLAMINE SALTS THEREOF, WHEREIN R is Cl, CH3O, CH3 or carbamyl or mono- or dialkylcarbamyl wherein each alkyl contains from 1 to 3 carbon atoms; R1 is H, F, Cl, perfluoroalkyl of 2 to 4 carbon atoms or -CXYZ wherein X, Y and Z are each H, F or Cl; R2 is H, F. Cl, Br, I, CH3 or CF3; and R3 is H, NO2, F, Cl or Br, and their use as novel herbicides.
摘要翻译：取代的下式的4（3H） - 喹唑啉酮及其碱金属和碱金属盐，其中R是Cl，CH 3 O，CH 3或氨基甲酰基或单或二烷基氨基甲酰基，其中每个烷基含有1至3个碳原子; R1是H，F，Cl，2至4个碳原子的全氟烷基或-CXYZ，其中X，Y和Z各自为H，F或Cl; R2是H，F.Cl，Br，I，CH3或CF3; 和R3是H，NO2，F，Cl或Br，以及它们作为新型除草剂的用途。

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