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31. 发明授权

US5609682A Method for the preparation of silicon single crystal 失效
标题翻译：硅单晶的制备方法
公开(公告)号：US5609682A
公开(公告)日：1997-03-11
申请号：US498894
申请日：1995-07-06
申请人： Wataru Sato , Masahiro Sakurada , Ohta Tomohiko , Katsuhiko Kemmochi
发明人： Wataru Sato , Masahiro Sakurada , Ohta Tomohiko , Katsuhiko Kemmochi
IPC分类号： C03C3/06 , C30B15/00 , C30B15/10 , C30B35/00
CPC分类号： C30B29/06 , C03C3/06 , C30B15/10 , C30B35/002 , C03C2201/30 , C03C2201/32
摘要： An improved method is proposed for the preparation of a semiconductor silicon single crystal of N-type by the Czochralski process, which is free from the problem of occurrence of delayed OSFs as defects in the single crystal even after prolonged storage at room temperature based on the discovery that presence of a certain amount of aluminum in the melt of silicon contained in a fused silica glass crucible acts to suppress occurrence of delayed OSFs as a type of defects in the single crystal while copper as an impurity acts adversely in this regard. With a known fact that an about 30 .mu.m thick inner surface layer of the crucible is melted down into the silicon melt during the single crystal pulling-up process, namely, the invention proposes use of a crucible of which the inner surface layer of 30 .mu.m thickness contains aluminum in an average concentration of 40 to 500 ppm by weight while the content of copper is as low as possible not to exceed 0.5 ppb by weight. Alternatively, when the fused silica glass crucible is deficient in the content of aluminum, an amount of aluminum is introduced as a dopant into the melt of silicon in the crucible to supplement the content of aluminum in order to be sufficient to suppress delayed OSFs.
摘要翻译：提出了一种通过Czochralski工艺制备N型半导体硅单晶的改进方法，其即使在室温下长时间储存之后也不会出现延迟OSF作为单晶的缺陷的问题，基于发现在熔融石英玻璃坩埚中含有的硅熔体中存在一定量的铝作为抑制作为单晶中的缺陷的延迟OSF的发生，而作为杂质的铜在这方面起不利影响。在已知的事实中，在单晶提拉过程中坩埚的内表面层约30μm的内表面层熔化成硅熔体，即本发明提出使用内表面层为30的坩埚平均浓度为40〜500ppm的铝，而铜的含量尽可能低，不超过0.5ppb（重量）。或者，当熔融石英玻璃坩埚的铝含量不足时，将铝的量作为掺杂剂引入到坩埚中的硅熔体中，以补充铝的含量，以足以抑制延迟的OSF。

32. 发明授权

US4414012A Fabrication methods of doped silica glass and optical fiber preform by using the doped silica glass 失效
标题翻译：通过掺杂石英玻璃制备掺杂石英玻璃和光纤预制棒的方法
公开(公告)号：US4414012A
公开(公告)日：1983-11-08
申请号：US300296
申请日：1981-09-08
申请人： Shoichi Suto , Hiroyuki Suda , Fumiaki Hanawa , Motohiro Nakahara , Nobuo Inagaki
发明人： Shoichi Suto , Hiroyuki Suda , Fumiaki Hanawa , Motohiro Nakahara , Nobuo Inagaki
IPC分类号： C03B20060101 , C03B19/10 , C03B37/014 , C03C3/06 , C03C13/04 , C03B19/06 , C03B20/00
CPC分类号： C03B19/106 , C03B19/102 , C03B37/01413 , C03B37/0142 , C03B37/01486 , C03C13/045 , C03C3/06 , C03B2203/24 , C03B2203/26 , C03B2207/06 , C03B2207/20 , C03B2207/28 , C03B2207/50 , C03B2207/64 , C03B2207/87 , C03C2201/30 , C03C2201/40 , C03C2203/40
摘要： Manufacturing method of doped silica glass suitable for optical fiber wherein quartz powder or SiO.sub.2 glass fine particles are exposed to a gas for producing the doped silica glass containing SiCl.sub.4, a gaseous additive and water vapor (H.sub.2 O) to add the dopant to the glass body, and then the resulting glass body is fused at a high temperature, thereby producing a transparent doped silica glass in which the production of the glass particles, the addition of the dopant, and the vitrification of the glass body are carried out by separate steps under respective suitable conditions. The manufacturing speed is remarkably increased because of the separate steps. The content of the dopant is not limited, but can be adjusted with any desired amount by changing the reaction time of dissolution. Dopant components like PbO.sub.2, SnO.sub.2, ZnO which were typically not added to the glass body can now be added thereto. Also, a method of manufacturing an optical fiber preform is disclosed wherein the doped silica glass is deposited and fused on a starting material which is inclined by an angle within a range of 5.degree.-90.degree. with respect to a blow-off direction of the flow of the doped silica glass to form a transparent doped silica glass body having a uniform outer diameter and a uniform boundary surface at a high synthesizing speed. This latter method aids mass production of optical fibers at low cost.
摘要翻译：适用于光纤的掺杂二氧化硅玻璃的制造方法，其中将石英粉末或SiO 2玻璃微粒暴露于用于生产含SiCl4，气态添加剂和水蒸汽（H 2 O）的掺杂石英玻璃的气体中以将掺杂剂添加到玻璃体中，然后将所得的玻璃体在高温下熔融，由此制备透明掺杂的石英玻璃，其中玻璃颗粒的产生，掺杂剂的添加和玻璃体的玻璃化在各自的步骤下通过各自的步骤进行适合条件。由于单独的步骤，制造速度显着增加。掺杂剂的含量没有限制，但可以通过改变溶解的反应时间以任何所需的量进行调节。现在可以向其中加入通常不加入到玻璃体中的掺杂剂组分如PbO 2，SnO 2，ZnO。此外，公开了一种制造光纤预制棒的方法，其中将掺杂的石英玻璃沉积并熔合在起始材料上，所述起始材料相对于所述材料的吹出方向倾斜5°-90°的范围内的角度掺杂石英玻璃的流动，以形成具有均匀外径和高合成速度的均匀边界表面的透明掺杂石英玻璃体。后一种方法有助于以低成本大量生产光纤。

33. 发明申请

US20160289861A1 METHOD FOR MANUFACTURING SINGLE CRYSTAL 有权
标题翻译：制造单晶的方法
公开(公告)号：US20160289861A1
公开(公告)日：2016-10-06
申请号：US15036095
申请日：2014-11-12
申请人： SHIN-ETSU HANDOTAI CO., LTD.
发明人： Yuuichi MIYAHARA , Shou TAKASHIMA , Yasuhiko SAWAZAKI , Atsushi IWASAKI
IPC分类号： C30B15/10 , C30B15/30 , C30B30/04 , C30B29/06
CPC分类号： C30B15/10 , C03C3/04 , C03C2201/30 , C03C2201/32 , C30B15/30 , C30B29/06 , C30B30/04
摘要： Method for manufacturing a single crystal according to a CZ method, including: pre-examining a correlation between an Al/Li ratio in a quartz raw material powder used for producing the quartz crucible, a use time of the crucible, a devitrification ratio at the use time, and occurrence or nonoccurrence of melt leakage attributable to the devitrification part; setting a range of the devitrification ratio of the quartz crucible in order not to generate the melt leakage, and determining a maximum use time of the quartz crucible according to the Al/Li ratio so as to fall within the set range of the ratio, on the basis of the correlation; and growing the single crystal by using the quartz crucible in the range of the maximum use time. This provides a manufacturing method which can efficiently use a quartz crucible to grow a single crystal while preventing occurrence of melt leakage.
摘要翻译：根据CZ方法制造单晶的方法，包括：预先检查用于制造石英坩埚的石英原料粉末中的Al / Li比与坩埚的使用时间，使用时间，以及归因于失透部分的熔体泄漏的发生或不发生; 设定石英坩埚的失透比的范围，以便不产生熔体泄漏，并且根据Al / Li比确定石英坩埚的最大使用时间，使其落入该比率的设定范围内相关的基础; 并在最大使用时间范围内使用石英坩埚生长单晶。这提供了可以有效地使用石英坩埚来生长单晶同时防止熔体泄漏的发生的制造方法。

34. 发明申请

US20160145147A1 DOPED SILICA-TITANIA GLASS HAVING LOW EXPANSIVITY AND METHODS OF MAKING THE SAME 有权
标题翻译：具有低膨胀性的二氧化硅 - 钛酸钠玻璃及其制造方法
公开(公告)号：US20160145147A1
公开(公告)日：2016-05-26
申请号：US14950374
申请日：2015-11-24
申请人： CORNING INCORPORATED
发明人： Sezhian Annamalai , Carlos Alberto Duran , Kenneth Edward Hrdina , Lisa Anne Moore
IPC分类号： C03C3/112 , C03C3/076 , C03B19/02 , G03F1/22 , C03B25/02 , C03C3/06 , C03C3/089
CPC分类号： C03C3/112 , C03B5/225 , C03B19/02 , C03B25/00 , C03B25/02 , C03B2201/10 , C03B2201/12 , C03B2201/14 , C03B2201/42 , C03C3/06 , C03C3/089 , C03C3/115 , C03C21/007 , C03C23/007 , C03C2201/10 , C03C2201/12 , C03C2201/14 , C03C2201/23 , C03C2201/30 , C03C2201/42 , C03C2203/10 , C03C2203/54 , G03F1/22
摘要： A method of forming a doped silica-titania glass is provided. The method includes blending batch materials comprising silica, titania, and at least one dopant. The method also includes heating the batch materials to form a glass melt. The method further includes consolidating the glass melt to form a glass article, and annealing the glass article.
摘要翻译：提供了形成掺杂二氧化硅 - 二氧化钛玻璃的方法。该方法包括混合包含二氧化硅，二氧化钛和至少一种掺杂剂的批料。该方法还包括加热批料以形成玻璃熔体。该方法还包括固化玻璃熔体以形成玻璃制品，并对玻璃制品进行退火。

35. 发明申请

US20140053772A1 SINGLE-CRYSTAL SILICON PULLING SILICA CONTAINER AND MANUFACTURING METHOD THEREOF 有权
标题翻译：单晶硅拉丝二氧化硅容器及其制造方法
公开(公告)号：US20140053772A1
公开(公告)日：2014-02-27
申请号：US14004085
申请日：2012-10-02
申请人： Shin-Etsu Quartz Products Co., Ltd.
发明人： Shigeru Yamagata
IPC分类号： C30B15/10
CPC分类号： C30B15/10 , C03B19/095 , C03C3/06 , C03C17/004 , C03C17/02 , C03C2201/30 , C03C2203/10 , C30B15/02 , C30B29/06 , Y02P40/57 , Y10T117/1032
摘要： The present invention provides a single-crystal silicon pulling silica container including an outer layer made of opaque silica glass containing gaseous bubbles and an inner layer made of transparent silica glass that does not substantially contain the gaseous bubbles; the container also including: a bottom portion, a curved portion, and a straight body portion, wherein continuous grooves are formed on a surface of the inner layer from at least part of the bottom portion to at least part of the straight body portion through the curved portion. As a result, there are provided the single-crystal silicon pulling silica container that can reduce defects called voids or pinholes in the pulled single-crystal silicon and a method for manufacturing such a silica container.
摘要翻译：本发明提供一种单晶硅拉硅石容器，其包括由含有气泡的不透明石英玻璃制成的外层和由实质上不含有气泡的透明石英玻璃制成的内层; 所述容器还包括：底部，弯曲部分和直体部分，其中在所述内层的表面上从所述底部的至少一部分到所述直体部分的至少一部分通过所述内部部分形成连续的凹槽弯曲部分。结果，提供了可以减少拉制的单晶硅中的称为空隙或针孔的缺陷的单晶硅拉硅
石容器以及这种二氧化硅容器的制造方法。

36. 发明申请

US20120107589A1 COMPOSITE SHAPED BODY AND SILICA GLASS, AND METHOD FOR PRODUCING THE SAME 审中-公开
标题翻译：复合形状体和二氧化硅玻璃及其制造方法
公开(公告)号：US20120107589A1
公开(公告)日：2012-05-03
申请号：US13382005
申请日：2010-07-07
申请人： Shigeru Fujino , Hiroshi Ikeda , Seiji Inaba , Toshihisa Kajiwara
发明人： Shigeru Fujino , Hiroshi Ikeda , Seiji Inaba , Toshihisa Kajiwara
IPC分类号： B32B3/00 , H01B1/08 , H01B1/12 , B82Y30/00
CPC分类号： C03B20/00 , B82Y30/00 , C03B19/066 , C03B19/12 , C03B2201/30 , C03B2201/32 , C03C1/006 , C03C3/06 , C03C2201/30 , C03C2201/32 , C03C2203/30 , C03C2203/36 , C08J5/005 , C08J5/02
摘要： The present invention provides a composite shaped body comprising silica nanoparticles and an organic polymer, wherein the silica nanoparticles and the organic polymer form a three-dimensional network; thereby provides: a composite shaped body which exhibits excellent formability and fabricability and which is also suited for use, for example, in producing a silica glass provided with an electrical conductivity; and a silica glass (especially, an electrically conductive silica glass) obtained by firing the composite shaped body.
摘要翻译：本发明提供了一种包含二氧化硅纳米颗粒和有机聚合物的复合成形体，其中二氧化硅纳米颗粒和有机聚合物形成三维网络; 从而提供：复合成形体，其具有优异的成形性和可制造性，并且也适用于例如制备具有导电性的石英玻璃; 以及通过烧结复合成形体得到的石英玻璃（特别是导电性石英玻璃）。

37. 发明申请

US20110158595A1 RARE-EARTH-DOPED FIBER OPTIC WAVEGUIDE AND OPTICAL DEVICE COMPRISING IT 审中-公开
标题翻译：稀土光纤波导和包含IT的光学器件
公开(公告)号：US20110158595A1
公开(公告)日：2011-06-30
申请号：US12735569
申请日：2009-01-27
申请人： Ekaterina Burov , Alain Pastouret , Christian Simonneau , Laurent Gasca , Christine Collet
发明人： Ekaterina Burov , Alain Pastouret , Christian Simonneau , Laurent Gasca , Christine Collet
IPC分类号： G02B6/02 , H01S3/067 , B82Y20/00
CPC分类号： G02B6/0229 , B82Y20/00 , B82Y30/00 , C03B37/01838 , C03B2201/34 , C03B2201/36 , C03B2201/58 , C03C3/06 , C03C4/0071 , C03C4/10 , C03C4/12 , C03C13/045 , C03C14/004 , C03C14/006 , C03C2201/30 , C03C2201/34 , C03C2201/3476 , C03C2201/36 , C03C2203/40 , H01S3/06716 , H01S3/06754 , H01S3/0933 , H01S3/094003 , H01S3/1608 , H01S3/169
摘要： The invention relates to an optical waveguide, in particular an optical fibre comprising a core, formed from a material based on rare-earth-ion-doped silica, covered by an optical cladding. Nanoparticles, at least some of which are metal nanoparticles, are dispersed in the material of the core. The optical devices, such as especially optical amplifiers, comprise an optical fibre having a core formed, from a material based on rare-earth-ion-doped silica covered with an optical cladding, nanoparticles, at least some of which are metal nanoparticles, being dispersed in the material of the core, and a pumping source delivering electromagnetic excitation radiation, which propagates in the core.
摘要翻译：本发明涉及光波导，特别是包括由由光电覆层覆盖的基于稀土离子掺杂的二氧化硅的材料形成的芯的光纤。其中至少一些是金属纳米颗粒的纳米颗粒分散在芯的材料中。诸如特别是光学放大器的光学器件包括具有由基于覆盖有光学包层的稀土离子掺杂的二氧化硅的材料形成的芯的光纤，纳米颗粒中的至少一些是金属纳米颗粒，分散在芯的材料中，以及泵送源，其输送在芯中传播的电磁激发辐射。

38. 发明授权

US07245424B2 Amplification device utilizing thulium doped modified silicate optical fiber 失效
标题翻译：利用掺doped改性硅酸盐光纤的放大器件
公开(公告)号：US07245424B2
公开(公告)日：2007-07-17
申请号：US11151176
申请日：2005-06-09
申请人： Michael Dennis , Brian Cole
发明人： Michael Dennis , Brian Cole
IPC分类号： H01S3/00 , H01S3/30 , C03B37/075
CPC分类号： H01S3/06716 , C03C3/06 , C03C3/095 , C03C13/046 , C03C2201/30 , C03C2201/3411 , C03C2201/347 , C03C2201/3482 , C03C2201/40 , H01S3/06754 , H01S3/06775 , H01S3/1603 , H01S3/161 , H01S3/1616 , H01S3/1698 , H01S3/17
摘要： A device amplifies light at wavelengths in the vicinity of 1420-1530 nm, using thulium doped silica-based optical fiber. This wavelength band is of interest as it falls in the low-loss optical fiber telecommunications window, and is somewhat shorter in wavelength than the currently standard erbium doped silica fiber amplifier. The device thus extends the band of wavelengths which can be supported for long-distance telecommunications. The additional wavelength band allows the data transmission rate to be substantially increased via wavelength division multiplexing (WDM), with minimal modification to the standard equipment currently used for WDM systems. The host glass is directly compatible with standard silica-based telecommunications fiber. The invention also enables modified silicate based amplifiers and lasers on a variety of alternative transitions. Specifically, an S-band thulium doped fiber amplifier (TDFA) using a true silicate fiber host is described.
摘要翻译：器件利用ium掺杂的二氧化硅基光纤放大1420-1530nm附近波长的光。该波长带在低损耗光纤通信窗口中是有意义的，并且其波长比当前标准的掺铒二氧化硅光纤放大器稍短。因此，该装置延长了可被长距离通信支持的波长带。附加波长带允许通过波分复用（WDM）大幅增加数据传输速率，对目前用于WDM系统的标准设备进行最小修改。主机玻璃与标准的二氧化硅电信光纤直接兼容。本发明还使得能够在各种替代转变上改性硅酸盐基放大器和激光器。具体来说，描述了使用真硅酸盐纤维主体的S波段ium掺杂光纤放大器（TDFA）。

39. 发明申请

US20050155388A1 Substantially dry, silica-containing soot, fused silica and optical fiber soot preforms, apparatus, methods and burners for manufacturing same 有权
公开(公告)号：US20050155388A1
公开(公告)日：2005-07-21
申请号：US11034359
申请日：2005-01-10
申请人： Gerald Burke , Steven Dawes , V. Srikant , Pushkar Tandon
发明人： Gerald Burke , Steven Dawes , V. Srikant , Pushkar Tandon
IPC分类号： C03B37/018 , C03B19/14 , C03B37/012 , C03B37/014 , C03C3/06 , F23D14/22 , F23D14/32 , G03F1/00 , G03F7/20
CPC分类号： G03F7/70216 , C03B19/1407 , C03B19/1415 , C03B19/1423 , C03B19/1453 , C03B37/01202 , C03B37/01406 , C03B37/01413 , C03B37/0142 , C03B37/0146 , C03B2201/12 , C03B2203/22 , C03B2207/02 , C03B2207/06 , C03B2207/08 , C03B2207/14 , C03B2207/20 , C03B2207/30 , C03B2207/38 , C03B2207/40 , C03B2207/42 , C03B2207/46 , C03B2207/54 , C03B2207/70 , C03B2207/81 , C03C3/06 , C03C2201/12 , C03C2201/20 , C03C2201/23 , C03C2201/30 , C03C2201/32 , F23D14/22 , F23D14/32 , G03F1/60 , G03F7/70958
摘要： Methods, apparatus and precursors for producing substantially water-free silica soot, preforms and glass. The methods and apparatus make substantially water-free fused silica preforms or glass by removing water as a reaction product, removing water from the atmosphere, removing water from the transport process, or combinations thereof. In a first embodiment, substantially water-free soot, preforms or glass are achieved by using a hydrogen-free fuel, such as carbon monoxide, in the deposition process. In another embodiment, a soot producing burner has parameters that enable operation on a substantially hydrogen-free fuel. End burners, which minimize water production, are also described. Such water-free methods are useful in depositing fluorine-doped soot because of the low water present and the efficiency in which fluorine is incorporated. In another embodiment, glassy barrier layer methods and apparatus are described for minimizing dopant migration, especially fluorine. Laser and induction methods and apparatus for forming the barrier layer are depicted. A chlorine, fluorine and silica precursor, such as chlorofluorosilane, may be utilized to form fluorinated soot. Other methods and apparatus are directed to combinations of conventional and substantially water-free processes. One embodiment is directed to combustion enhancing additives for addition to the substantially hydrogen-free fuels. The methods and apparatus in accordance with the invention are particularly useful for producing photomask substrates and optical fiber preforms.

40. 发明授权

US06342460B1 Infrared absorbing glass, and it's fabrication method 有权
标题翻译：红外吸收玻璃，它的制作方法
公开(公告)号：US06342460B1
公开(公告)日：2002-01-29
申请号：US09336678
申请日：1999-06-21
申请人： Yoshinobu Akimoto , Hiroaki Kinoshita
发明人： Yoshinobu Akimoto , Hiroaki Kinoshita
IPC分类号： C03C304
CPC分类号： C03C1/006 , C03B19/12 , C03B2201/40 , C03B2201/50 , C03C3/06 , C03C3/078 , C03C4/082 , C03C13/046 , C03C2201/30 , C03C2201/40 , C03C2201/50 , C03C2203/20 , Y10S501/905
摘要： The invention relates to a glass excellent in infrared absorption capability and corrosion resistance, and its fabrication process. A compound of divalent copper and a compound of a metal species for a network modifier oxide are introduced in a wet gel. Then, the wet gel is dipped in a dipping solution having a low solubility with respect to the compound of divalent copper and the compound of a metal species for a network modifier oxide for the precipitation in the wet gel of the divalent-t copper compound and the compound of a metal species for a network modifier oxide, followed by drying and firing. Thus, an infrared absorbing glass comprising 70 to 98 mol % of SiO2, 1 to 12 mol % of CuO and 1 to 18 mol % of a network modifier oxide other than CuO is fabricated.
摘要翻译：本发明涉及一种红外吸收能力和耐腐蚀性优异的玻璃及其制造工艺。将二价铜的化合物和用于网络改性剂氧化物的金属物质的化合物引入湿凝胶中。然后，将湿凝胶浸入相对于二价铜化合物的低溶解度的浸渍溶液和用于网络改性剂氧化物的金属物质的化合物，用于在二价铜化合物的湿凝胶中沉淀，以及用于网络改性剂氧化物的金属物质的化合物，随后进行干燥和烧制。因此，制造包含70〜98摩尔％的SiO 2，1〜12摩尔％的CuO和1〜18摩尔％的CuO以外的网络改性剂氧化物的红外线吸收玻璃。

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