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31. 发明授权

US5952125A Batteries with electroactive nanoparticles 失效
标题翻译：电活性纳米粒子电池
公开(公告)号：US5952125A
公开(公告)日：1999-09-14
申请号：US897776
申请日：1997-07-21
申请人： Xiangxin Bi , Nobuyuki Kambe , Sujeet Kumar , James T. Gardner
发明人： Xiangxin Bi , Nobuyuki Kambe , Sujeet Kumar , James T. Gardner
IPC分类号： C01G31/02 , H01M4/131 , H01M4/48 , H01M4/485 , H01M4/62 , H01M10/0525 , H01M10/36 , H01M4/04
CPC分类号： H01M4/131 , B82Y30/00 , C01G31/02 , H01M4/485 , H01M4/622 , H01M4/623 , C01P2002/02 , C01P2002/72 , C01P2004/04 , C01P2004/62 , C01P2004/64 , C01P2006/40 , H01M10/0525
摘要： Batteries based on nanoparticles are demonstrated that achieve high energy densities. Vanadium oxide nanoparticles can have several different stoichiometries and corresponding crystal lattices. The nanoparticles preferably have average diameters less than about 500 nm and more preferably less than about 150 nm. Cathodes produced using the vanadium oxide nanoparticles and a binder can be used to construct lithium batteries or lithium ion batteries. The nanoparticles may have energy densities greater than about 900 Wh/kg.
摘要翻译：证明了基于纳米粒子的电池实现了高能量密度。氧化钒纳米颗粒可以具有几种不同的化学计量和相应的晶格。纳米颗粒优选具有小于约500nm，更优选小于约150nm的平均直径。使用氧化钒纳米粒子和粘合剂制成的阴极可用于构建锂电池或锂离子电池。纳米颗粒可具有大于约900Wh / kg的能量密度。

32. 发明授权

US6106798A Vanadium oxide nanoparticles 失效
标题翻译：氧化钒纳米粒子
公开(公告)号：US6106798A
公开(公告)日：2000-08-22
申请号：US897778
申请日：1997-07-21
申请人： Nobuyuki Kambe , Sujeet Kumar , James T. Gardner , Xiangxin Bi
发明人： Nobuyuki Kambe , Sujeet Kumar , James T. Gardner , Xiangxin Bi
IPC分类号： C01G31/02 , H01M4/02 , H01M4/48 , H01M4/485 , H01M4/58 , H01M4/62 , H01M10/0525 , H01M10/36 , C01B13/14 , B01J35/08 , C01G13/14
CPC分类号： C01G31/02 , B82Y30/00 , H01M4/485 , H01M4/622 , H01M4/623 , C01P2002/02 , C01P2002/72 , C01P2004/03 , C01P2004/32 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2006/12 , H01M10/0525 , H01M2004/021 , H01M4/02 , H01M4/5825
摘要： Vanadium oxide nanoparticles were produced with vanadium in a variety of oxidation states and with different crystalline lattice structures. These particles preferably have an average diameter of 150 nm or less with a narrow distribution of diameters. The particles manifest unique properties that result from the small particle size and correspondingly large surface area. A variety of the vanadium oxide nanoparticles can be produced by a versatile laser pyrolysis arrangement. These nanoparticles can be further processed to change the properties of the particles without destroying the nanoscale size of the particles.
摘要翻译：用各种氧化态和不同晶格结构的钒制备氧化钒纳米颗粒。这些粒子优选具有150nm以下的平均直径，直径分布窄。颗粒表现出由小颗粒尺寸和相应较大表面积产生的独特性质。可以通过多功能激光热解装置来生产各种氧化钒纳米颗粒。可以进一步处理这些纳米颗粒以改变颗粒的性质而不破坏颗粒的纳米级尺寸。

33. 发明授权

US06680041B1 Reaction methods for producing metal oxide particles 有权
标题翻译：用于生产金属氧化物颗粒的反应方法
公开(公告)号：US06680041B1
公开(公告)日：2004-01-20
申请号：US09697697
申请日：2000-10-26
申请人： Sujeet Kumar , James T. Gardner , Xiangxin Bi , Nobuyuki Kambe
发明人： Sujeet Kumar , James T. Gardner , Xiangxin Bi , Nobuyuki Kambe
IPC分类号： C01B1314
CPC分类号： H01M4/131 , B82Y30/00 , C01G45/02 , C01P2002/02 , C01P2002/72 , C01P2002/76 , C01P2004/04 , C01P2004/51 , C01P2004/52 , C01P2004/62 , C01P2004/64 , C01P2006/40 , H01M4/485 , H01M4/50 , H01M4/505 , Y10T428/2982 , Y10T428/2991
摘要： Manganese oxide particles have been produced having an average diameter less than about 500 nm and a very narrow distribution of particle diameters. Methods are described for producing metal oxides by performing a reaction with an aerosol including a metal precursor. Heat treatments can be performed in an oxidizing environment to alter the properties of the manganese oxide particles.
摘要翻译：已经生产了具有小于约500nm的平均直径和非常窄的粒径分布的氧化锰颗粒。描述了通过与包括金属前体的气溶胶进行反应来生产金属氧化物的方法。可以在氧化环境中进行热处理以改变氧化锰颗粒的性质。

34. 发明授权

US5989514A Processing of vanadium oxide particles with heat 失效
标题翻译：氧化钒颗粒加热处理
公开(公告)号：US5989514A
公开(公告)日：1999-11-23
申请号：US897903
申请日：1997-07-21
申请人： Xiangxin Bi , James T. Gardner , Sujeet Kumar , Nobuyuki Kambe
发明人： Xiangxin Bi , James T. Gardner , Sujeet Kumar , Nobuyuki Kambe
IPC分类号： C01G31/02 , H01M4/02 , H01M4/48 , H01M4/485 , H01M4/58 , H01M4/62 , H01M10/0525 , H01M10/36 , C06B33/00 , B05B3/00 , C01B13/14 , C01G31/00
CPC分类号： C01G31/02 , B82Y30/00 , H01M4/485 , H01M4/622 , H01M4/623 , C01P2002/02 , C01P2002/72 , C01P2004/03 , C01P2004/32 , C01P2004/51 , C01P2004/62 , C01P2004/64 , C01P2006/12 , H01M10/0525 , H01M2004/021 , H01M4/02 , H01M4/5825
摘要： The stoichiometry and/or crystal structure of vanadium oxide particles are altered by heating initial particles of vanadium oxide under mild conditions. The temperature is generally at least about 300.degree. C. less than the melting point of both the initial vanadium oxide particle and the product vanadium oxide particles. Preferred initial particles are vanadium oxide nanoparticles. The heating can be performed under an oxidizing atmosphere or an inert atmosphere, depending on the particular initial particles and the desired product particles.
摘要翻译：通过在温和条件下加热钒氧化物的初始颗粒来改变氧化钒颗粒的化学计量和/或晶体结构。温度通常比初始氧化钒颗粒和产物氧化钒颗粒的熔点低至少约300℃。优选的初始颗粒是氧化钒纳米颗粒。加热可以在氧化气氛或惰性气氛下进行，这取决于特定的初始颗粒和所需的产物颗粒。

35. 发明授权

US08865271B2 High rate deposition for the formation of high quality optical coatings 有权
标题翻译：高速沉积用于形成高质量的光学涂层
公开(公告)号：US08865271B2
公开(公告)日：2014-10-21
申请号：US10854019
申请日：2004-05-26
申请人： Xiangxin Bi , Herman A. Lopez , Prasad Narasimha , Eric Euvrard , Ronald J. Mosso
发明人： Xiangxin Bi , Herman A. Lopez , Prasad Narasimha , Eric Euvrard , Ronald J. Mosso
IPC分类号： C23C14/30 , C23C24/00 , C23C16/48 , G02B6/132 , C03B37/012 , C23C16/56 , C03B19/01 , C03B19/14 , C23C24/04 , C23C16/40 , C03B37/014 , G02B6/036
CPC分类号： G02B1/12 , B05D1/12 , B05D3/06 , C03B19/01 , C03B19/1415 , C03B37/0128 , C03B37/01294 , C03B37/01406 , C03B37/01413 , C03B37/0142 , C03B2201/10 , C03B2201/12 , C03B2201/28 , C03B2201/31 , C03B2207/34 , C23C16/401 , C23C16/482 , C23C16/483 , C23C16/56 , C23C24/00 , C23C24/04 , G02B6/036 , G02B6/132 , Y02P40/57
摘要： High rate deposition methods comprise depositing a powder coating from a product flow. The product flow results from a chemical reaction within the flow. Some of the powder coatings consolidate under appropriate conditions into an optical coating. The substrate can have a first optical coating onto which the powder coating is placed. The resulting optical coating following consolidation can have a large index-of-refraction difference with the underlying first optical coating, high thickness and index-of-refraction uniformity across the substrate and high thickness and index-of-refraction uniformity between coatings formed on different substrates under equivalent conditions. In some embodiments, the deposition can result in a powder coating of at least about 100 nm in no more than about 30 minutes with a substrate having a surface area of at least about 25 square centimeters.
摘要翻译：高速沉积方法包括从产品流中沉积粉末涂层。产物流由流动内的化学反应产生。一些粉末涂料在合适的条件下固化成光学涂层。基底可以具有第一光学涂层，其上放置粉末涂层。固结后的所得光学涂层可以具有与基底的第一光学涂层，基底上的高厚度和折射率均匀性的较大的折射率差异，以及形成在不同的涂层之间的涂层之间的高厚度和折射率均匀性在相同条件下的底物。在一些实施方案中，沉积可导致至少约100nm的粉末涂层，其表面积至少约25平方厘米，其表面积至少约为25平方厘米。

36. 发明授权

US06723435B1 Optical fiber preforms 有权
标题翻译：光纤预制棒
公开(公告)号：US06723435B1
公开(公告)日：2004-04-20
申请号：US10229937
申请日：2002-08-28
申请人： Craig R. Horne , Jesse S. Jur , Ronald J. Mosso , Eric H. Euvrard , Xiangxin Bi
发明人： Craig R. Horne , Jesse S. Jur , Ronald J. Mosso , Eric H. Euvrard , Xiangxin Bi
IPC分类号： B32B1706
CPC分类号： C03B37/018 , C03B37/0128 , C03B37/014 , C03B37/027 , C03B2205/13 , Y02P40/57
摘要： Optical fiber preforms can comprise a glass preform structure with an inner cavity. A powder can be placed within the inner cavity having an average primary particle size of less than about one micron. The powder can be in the form of an unagglomerated particles or a powder coating with a degree of agglomeration or hard fusing ranging from none to significant amounts as long as the primary particles are visible in a micrograph. Powders can be placed within a preform structure by forming a slurry with a dispersion of submicron/nanoscale particles within a cavity within the prefrom. In other embodiments, a powder coating is formed within a preform structure by depositing the powder coating directly from a reaction product stream. The formation of the powder coating can be formed within the reaction chamber or outside of the reaction chamber by flowing the product particle stream through a conduit leading to the preform structure. In additional embodiments, a powder coating is placed on an insert, e.g., a glass insert, that is subsequently placed within a preform structure.
摘要翻译：光纤预制件可以包括具有内腔的玻璃预制件结构。粉末可以放置在具有小于约一微米的平均一次粒径的内腔内。只要初级颗粒在显微照片中可见，粉末可以是非聚集颗粒或具有聚集程度或硬熔点的粉末涂层的形式，其范围从无至大量。粉末可以通过在预成型体内的空腔内形成具有亚微米/纳米级颗粒的分散体的浆料而放置在预成型体结构内。在其它实施方案中，通过直接从反应产物流沉积粉末涂料，在预成型体结构内形成粉末涂料。粉末涂层的形成可以通过使产物颗粒流通过导致预成型结构的导管而在反应室内或反应室外形成。在另外的实施例中，将粉末涂层放置在随后放置在预成型结构内的插入件上，例如玻璃插入件上。

37. 发明授权

US07905114B1 Method for forming optical fiber preforms 有权
标题翻译：光纤预制棒的形成方法
公开(公告)号：US07905114B1
公开(公告)日：2011-03-15
申请号：US10822642
申请日：2004-04-12
申请人： Craig R. Horne , Jesse S. Jur , Ronald J. Mosso , Eric H. Euvrard , Xiangxin Bi
发明人： Craig R. Horne , Jesse S. Jur , Ronald J. Mosso , Eric H. Euvrard , Xiangxin Bi
IPC分类号： C03B37/023
CPC分类号： C03B37/018 , C03B37/0128 , C03B37/014 , C03B37/027 , C03B2205/13 , Y02P40/57
摘要： Optical fiber preforms can comprise a glass preform structure with an inner cavity. A powder can be placed within the inner cavity having an average primary particle size of less than about one micron. The powder can be in the form of an unagglomerated particles or a powder coating with a degree of agglomeration or hard fusing ranging from none to significant amounts as long as the primary particles are visible in a micrograph. Powders can be placed within a preform structure by forming a slurry with a dispersion of submicron/nanoscale particles within a cavity within the preform. In other embodiments, a powder coating is formed within a preform structure by depositing the powder coating directly from a reaction product stream. The formation of the powder coating can be formed within the reaction chamber or outside of the reaction chamber by flowing the product particle stream through a conduit leading to the preform structure. In additional embodiments, a powder coating is placed on an insert, e.g., a glass insert, that is subsequently placed within a preform structure.
摘要翻译：光纤预制件可以包括具有内腔的玻璃预制件结构。粉末可以放置在具有小于约一微米的平均一次粒径的内腔内。只要初级颗粒在显微照片中可见，粉末可以是非聚集颗粒或具有聚集程度或硬熔点的粉末涂层的形式，其范围从无至大量。可以通过在预制件内的空腔内形成具有亚微米/纳米尺寸颗粒的分散体的浆料将粉末放置在预成型结构内。在其它实施方案中，通过直接从反应产物流沉积粉末涂料，在预成型体结构内形成粉末涂料。粉末涂层的形成可以通过使产物颗粒流通过导致预成型结构的导管而在反应室内或反应室外形成。在另外的实施例中，将粉末涂层放置在随后放置在预成型结构内的插入件上，例如玻璃插入件上。

38. 发明授权

US06391494B2 Metal vanadium oxide particles 有权
标题翻译：金属氧化钒颗粒
公开(公告)号：US06391494B2
公开(公告)日：2002-05-21
申请号：US09311506
申请日：1999-05-13
申请人： Hariklia Dris Reitz , James P. Buckley , Sujeet Kumar , Yu K. Fortunak , Xiangxin Bi
发明人： Hariklia Dris Reitz , James P. Buckley , Sujeet Kumar , Yu K. Fortunak , Xiangxin Bi
IPC分类号： H01M434
CPC分类号： H01M4/131 , H01M4/1391 , H01M4/54 , H01M10/052
摘要： Laser pyrolysis can be used to produce directly metal vanadium oxide composite nanoparticles. To perform the pyrolysis a reactant stream is formed including a vanadium precursor and a second metal precursor. The pyrolysis is driven by energy absorbed from a light beam. Metal vanadium oxide nanoparticles can be incorporated into a cathode of a lithium based battery to obtain increased energy densities. Implantable defibrillators can be constructed with lithium based batteries having increased energy densities.
摘要翻译：激光热解可用于生产直接金属氧化钒复合纳米粒子。为了进行热解，形成包括钒前体和第二金属前体的反应物流。热分解是由光束吸收的能量驱动的。可以将金属氧化钒纳米颗粒掺入锂基电池的阴极中以获得增加的能量密度。可植入的除颤器可以用具有增加的能量密度的锂基电池构成。

39. 发明授权

US07423512B1 Zinc oxide particles 有权
标题翻译：氧化锌颗粒
公开(公告)号：US07423512B1
公开(公告)日：2008-09-09
申请号：US09266202
申请日：1999-03-10
申请人： Hariklia Dris Reitz , Sujeet Kumar , Xiangxin Bi , Nobuyuki Kambe
发明人： Hariklia Dris Reitz , Sujeet Kumar , Xiangxin Bi , Nobuyuki Kambe
IPC分类号： H01C7/10
CPC分类号： C09K11/54 , B82Y30/00 , C01G9/03 , C01P2002/72 , C01P2004/04 , C01P2004/51 , C01P2004/54 , C01P2004/62 , C01P2004/64 , C09K11/671 , C09K11/7701 , H01C7/112 , Y10T428/2982
摘要： A collection of zinc oxide nanoparticles have been produced by laser pyrolysis. The zinc oxide nanoparticles have average particle diameters of less than about 95 nm and a very narrow particle size distribution. The laser pyrolysis process is characterized by the production of a reactant stream within the reaction chamber, where the reactant stream includes a zinc precursor and other reactants. The zinc precursor can be delivered as an aerosol.
摘要翻译：通过激光热解制备了氧化锌纳米颗粒的集合体。氧化锌纳米颗粒具有小于约95nm的平均粒径和非常窄的粒度分布。激光热解过程的特征在于在反应室内产生反应物流，其中反应物流包括锌前体和其它反应物。锌前体可以作为气溶胶递送。

40. 发明申请

US20050118411A1 Optical materials and optical devices 有权
公开(公告)号：US20050118411A1
公开(公告)日：2005-06-02
申请号：US10977608
申请日：2004-10-29
申请人： Craig Horne , Pierre DeMascarel , Christian Honeker , Benjamin Chaloner-Gill , Herman Lopez , Xiangxin Bi , Ronald Mosso , William McGovern , James Gardner , Sujeet Kumar , James Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chinuvolu , Jesse Jur
发明人： Craig Horne , Pierre DeMascarel , Christian Honeker , Benjamin Chaloner-Gill , Herman Lopez , Xiangxin Bi , Ronald Mosso , William McGovern , James Gardner , Sujeet Kumar , James Gilliam , Vince Pham , Eric Euvrard , Shivkumar Chinuvolu , Jesse Jur
IPC分类号： G02B6/12 , C01B13/20 , C01B19/00 , C01F17/00 , C01G1/00 , C01G17/00 , C01G23/00 , C03B8/00 , C03B19/10 , C03B19/14 , C03C3/068 , C03C3/095 , C03C3/15 , C03C4/12 , C03C12/00 , C23C16/42 , G02B1/00 , B32B5/16
CPC分类号： B82Y30/00 , C01B13/20 , C01B19/004 , C01F17/0043 , C01G1/00 , C01G17/00 , C01G23/00 , C01P2002/02 , C01P2002/50 , C01P2004/50 , C01P2004/62 , C01P2004/64 , C01P2004/84 , C01P2006/60 , C01P2006/80 , C03B19/106 , C03B19/1415 , C03B2207/34 , C03C3/062 , C03C3/078 , C03C3/095 , C03C3/097 , C03C3/122 , C03C3/17 , C03C3/253 , C03C12/00 , C09K11/7706 , Y02P40/57 , Y10T428/25 , Y10T428/256 , Y10T428/2949 , Y10T428/2982 , Y10T428/2991 , Y10T428/31609
摘要： Nanoscale particles, particle coatings/particle arrays and corresponding consolidated materials are described based on an ability to vary the composition involving a wide range of metal and/or metalloid elements and corresponding compositions. In particular, metalloid oxides and metal-metalloid compositions are described in the form of improved nanoscale particles and coatings formed from the nanoscale particles. Compositions comprising rare earth metals and dopants/additives with rare earth metals are described. Complex compositions with a range of host compositions and dopants/additives can be formed using the approaches described herein. The particle coating can take the form of particle arrays that range from collections of disbursable primary particles to fused networks of primary particles forming channels that reflect the nanoscale of the primary particles. Suitable materials for optical applications are described along with some optical devices of interest.

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