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31. 发明授权

US06303695B1 Dispersion-controlled polymers for broadband fiber optic devices 失效
标题翻译：用于宽带光纤设备的分散控制聚合物
公开(公告)号：US06303695B1
公开(公告)日：2001-10-16
申请号：US09692067
申请日：2000-10-19
申请人： Kwok Pong Chan , David G. Gascoyne , Gregory A. Wagoner
发明人： Kwok Pong Chan , David G. Gascoyne , Gregory A. Wagoner
IPC分类号： C08F800
CPC分类号： C08F8/42 , C08F2800/20 , Y10T428/24124 , C08F220/22
摘要： Novel polymer compositions for controlling or correcting dispersion mismatch between the composition and a side-fiber polished optical fiber are disclosed. The polymer compositions contain an infrared absorbing dye having an absorption maximum from about 900 to about 1200 nm and and a polar olefin copolymer containing monomers which are formed from polar olefins having an ester, benzene, or halogen substitutent attached. A method for controlling the dispersion exhibited by the novel polymer compositions is also disclosed. The method includes forming the polymer composition over an exposed surface of an optical fiber. Dispersion is controlled by controlling the amount of dye present in the polymer composition. Also disclosed is an optical device from which improvements in the uniformity of spectral response and performance are observed across a wavelength band. The optical device includes the polymer composition formed over an optical fiber. Variable optical attenuators, switches, and couplers can be designed which incorporate the polymer compositions. The invention is particularly useful in the 1500-1600 nm wavelength band.
摘要翻译：公开了用于控制或校正组合物和侧纤纤维抛光光纤之间的分散失配的新型聚合物组合物。聚合物组合物含有吸收最大约为900至约1200nm的红外线吸收染料，以及含有连接有酯，苯或卤素取代基的极性烯烃形成的单体的极性烯烃共聚物。还公开了用于控制由新型聚合物组合物表现出的分散体的方法。该方法包括在光纤的暴露表面上形成聚合物组合物。通过控制聚合物组合物中存在的染料的量来控制分散。还公开了一种光学装置，其中在波长带上观察到光谱响应和性能的均匀性的改善。光学装置包括在光纤上形成的聚合物组合物。可以设计可变光衰减器，开关和耦合器，其结合聚合物组合物。本发明在1500-1600nm波长带中特别有用。

32. 发明授权

US06288206B1 Chiral polymer compositions exhibiting nonlinear optical properties 失效
标题翻译：显示非线性光学性质的手性聚合物组合物
公开(公告)号：US06288206B1
公开(公告)日：2001-09-11
申请号：US09432312
申请日：1999-11-02
申请人： Kevin R. Stewart , Janet L. Gordon , Kwok Pong Chan , David G. Gascoyne , Feng Pan
发明人： Kevin R. Stewart , Janet L. Gordon , Kwok Pong Chan , David G. Gascoyne , Feng Pan
IPC分类号： C08G6400
CPC分类号： G02F1/3615 , C08G63/68 , C08G64/08 , C08G65/4006 , C08G65/4031 , C08G65/4068 , C08G65/48 , C08G75/23 , C08G2650/64 , G02F1/3617
摘要： Chiral organic polymers doped with or appended by nonlinear optical dyes are disclosed. The use of chiral polymers produces a more stable noncentrosymmetric environment for the dye molecules resulting in unexpectedly long relaxation times as compared with previously used organic polymers. In addition, the NLO/chiral polymer materials exhibit high electro-optical coefficients (r33), high nonlinear optical coefficients (d33), improved long-term thermal stability, and at the same time retain the processing advantages associated with organic polymers. Thus, the present NLO/chiral polymer materials are extremely well-suited for use in second-order nonlinear optical and optoelectronics devices.
摘要翻译：公开了由非线性光学染料掺杂或附加的手性有机聚合物。与以前使用的有机聚合物相比，手性聚合物的使用为染料分子产生更稳定的非中心对称环境，导致意想不到的长的松弛时间。此外，NLO /手性聚合物材料具有高的电光系数（r33），高非线性光学系数（d33），改善的长期热稳定性，同时保持与有机聚合物相关的加工优点。因此，本发明的NLO /手性聚合物材料非常适用于二阶非线性光学和光电子器件。

33. 发明授权

US5994596A Method for preparing high purity indane bisphenols 失效
标题翻译：制备高纯度茚满双酚的方法
公开(公告)号：US5994596A
公开(公告)日：1999-11-30
申请号：US52546
申请日：1998-03-31
申请人： Kwok Pong Chan , Pamela L. Cristo , Patrick M. McGrath, Jr.
发明人： Kwok Pong Chan , Pamela L. Cristo , Patrick M. McGrath, Jr.
IPC分类号： C07C37/00 , C07C39/17 , C07C39/12
CPC分类号： C07C37/11 , C07C37/84 , C07C2102/08
摘要： A process for preparing high purity indane bisphenols in high yield is disclosed. The method comprises heating a bisphenol in the presence of Montmorillonite K10 clay, which catalyzes the synthesis reaction more rapidly and effectively than other clays previously disclosed. The high purity (.gtoreq.97%) of the synthesized indane bisphenol is obtained by two successive selective recrystallizations, the first from an organic solvent, and the second from an acetic acid solution. The high purity indane bisphenols produced may be made substantially pure (>99%) by employing a purification process which includes at least one selective recrystallization from a 45%-80% by volume aqueous acetic acid solution. Alternatively, substantially pure indane bisphenol may be obtained by recrystallization from a solution of 89-93% by volume toluene and 7-11% by volume n-propanol, or by a combination of recrystallizations from toluene/n-propanol and from aqueous acetic acid. Substantially pure indane bisphenols, such as 5-hydroxy-3-(4-hydroxyphenyl)-1,1,3-trimethylindane, are suitable for conversion to high molecular weight polymers.
摘要翻译：公开了一种以高产率制备高纯度茚满双酚的方法。该方法包括在蒙脱石K10粘土存在下加热双酚，其催化合成反应比先前公开的其它粘土更快速和有效地催化合成反应。合成茚满双酚的高纯度（> / = 97％）是通过两次连续的选择性重结晶获得的，第一种是有机溶剂，第二种是由乙酸溶液获得。通过使用包含45％-80％（体积）乙酸水溶液的至少一种选择性重结晶的纯化方法，所生产的高纯度茚满二酚可以制成基本上纯的（> 99％）。或者，基本上纯的茚满双酚可以通过从89-93体积％甲苯和7-11体积％正丙醇的溶液中重结晶，或通过从甲苯/正丙醇和乙酸水溶液的重结晶。基本纯的茚满双酚，如5-羟基-3-（4-羟基苯基）-1,1,3-三甲基茚，适用于转化为高分子量聚合物。

34. 发明申请

US20120190791A1 METHODS OF PREPARING POLYMER-ORGANOCLAY COMPOSITES AND ARTICLES DERIVED THEREFROM 有权
标题翻译：制备聚合物 - 组织复合材料的方法及其衍生物
公开(公告)号：US20120190791A1
公开(公告)日：2012-07-26
申请号：US13430801
申请日：2012-03-27
申请人： Kwok Pong Chan , Sarah Elizabeth Genovese , Erik C. Hagberg , David Bruce Hall , John Lester Maxam , Tara J. Mullen , Roy Ray Odle , Albert Santo Stella , James Mitchell White
发明人： Kwok Pong Chan , Sarah Elizabeth Genovese , Erik C. Hagberg , David Bruce Hall , John Lester Maxam , Tara J. Mullen , Roy Ray Odle , Albert Santo Stella , James Mitchell White
IPC分类号： C08K9/04 , C08L79/08
CPC分类号： C08F2/44
摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.
摘要翻译：一种制备聚合物 - 有机粘土复合材料组合物的方法，包括将溶剂和未剥离的有机粘土组合以提供第一混合物，其中未剥离的有机粘土包含交替的无机硅酸盐层和有机层，并且在硅酸盐层之间具有初始间隔; 将第一混合物暴露于足够强度和持续时间的通电状态以增加无机硅酸盐层的初始间隔，以提供第二混合物; 使所述第二混合物与聚合物组合物接触，使得所述聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中所述聚合物组合物至少部分地可溶于所述溶剂中; 以及从所述第二混合物中除去至少一部分所述溶剂，其中在去除所述溶剂之后，所述无机硅酸盐层保持被所述聚合物分离。

35. 发明申请

US20080044639A1 POLYIMIDE SOLVENT CAST FILMS HAVING A LOW COEFFICIENT OF THERMAL EXPANSION AND METHOD OF MANUFACTURE THEREOF 审中-公开
标题翻译：具有低热膨胀系数的聚酰亚胺溶剂型薄膜及其制造方法
公开(公告)号：US20080044639A1
公开(公告)日：2008-02-21
申请号：US11758782
申请日：2007-06-06
申请人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
发明人： Kwok Pong Chan , Erik Hagberg , Tara J. Mullen , Roy Ray Odle
IPC分类号： C08G69/26 , B32B5/00 , C08K3/34
CPC分类号： H05K1/0346 , B82Y30/00 , C08G73/1007 , C08J5/005 , C08J5/18 , C08J2379/08 , H05K1/0373 , H05K2201/0154 , H05K2201/0209 , H05K2201/0257 , H05K2201/068
摘要： A solvent cast film comprises a polyimide comprising structural units derived from polymerization of a dianhydride component comprising a dianhydride selected from the group consisting of 3,4′-oxydiphthalic dianhydride, 3,3′-oxydiphthalic dianhydride, 4,4′-oxydiphthalic dianhydride, and combinations thereof, with a diamine component wherein the polyimide has a glass transition temperature of at least 190° C.; wherein the film has a coefficient of thermal expansion of less than 60 ppm/° C., a thickness from 0.1 to 250 micrometers, and less than 5% residual solvent by weight; wherein the polyimide has less than 15 molar % of structural units derived from a member selected from the group consisting of biphenyltetracarboxylic acid, a dianhydride of biphenyltetracarboxylic acid, an ester of biphenyltetracarboxylic acid, and a combination thereof.
摘要翻译：溶剂流延膜包括聚酰亚胺，其包含衍生自二酐组分的聚合的结构单元，所述二酐组分包含二酐，其选自3,4'-氧二邻苯二甲酸二酐，3,3'-氧联二邻苯二甲酸二酐，4,4'-氧联二邻苯二甲酸二酐，和其组合与二胺组分，其中聚酰亚胺的玻璃化转变温度至少为190℃; 其中所述膜具有小于60ppm /℃的热膨胀系数，0.1至250微米的厚度和小于5重量％的残留溶剂; 其中所述聚酰亚胺具有少于15摩尔％的衍生自选自联苯四羧酸，联苯四羧酸的二酐，联苯四羧酸的酯及其组合的成员的结构单元。

36. 发明授权

US06611649B2 Variable optical attenuator with polarization maintaining fiber 失效
公开(公告)号：US06611649B2
公开(公告)日：2003-08-26
申请号：US09811913
申请日：2001-03-19
申请人： Kwok Pong Chan , Kim Roger LaBarge
发明人： Kwok Pong Chan , Kim Roger LaBarge
IPC分类号： G02B600
CPC分类号： G02B6/266 , G02B6/105 , G02F1/0118 , G02F1/0147 , G02F2203/48
摘要： An electrically controllable, variable optical attenuator (VOA) is disclosed, in which polarization maintaining fiber is employed. The fiber is modified to expose the evanescent field of optical energy transmitted therein, by removing material therefrom in a direction parallel to either the fast or slow axis of the fiber, while preserving the polarization maintaining property of the fiber. A controllable material is formed over the modified portion, to remove optical energy in response to a changeable stimulus applied, which changes the refractive index of the material. Related packaging, material composition and system aspects of the attenuator are also disclosed.

37. 发明授权

US06489399B1 Dye-appended polymers for broadband fiber optic devices 失效
标题翻译：用于宽带光纤设备的染料附着聚合物
公开(公告)号：US06489399B1
公开(公告)日：2002-12-03
申请号：US09628887
申请日：2000-07-31
申请人： Kwok Pong Chan , David G. Gascoyne , Janet L. Krahn , Gregory A. Wagoner
发明人： Kwok Pong Chan , David G. Gascoyne , Janet L. Krahn , Gregory A. Wagoner
IPC分类号： C08F800
CPC分类号： G02F1/0118 , C08F8/42 , C08F2800/20 , C08F2810/40 , G02B6/266 , G02B6/2835 , G02F1/0147 , G02F2202/022 , Y10T428/24124 , C08F220/14
摘要： Novel dye/polymer compositions are disclosed, which when used in connection with fiber optic devices, provide a uniform spectral response across a broadband wavelength region. The dye/polymer compositions contain an infrared absorbing dye having an absorption maximum from about 900 to about 1300 nm. One or more polar olefin copolymers containing monomers derived from polar olefins having an ester, benzene, or halogen substitutent attached, is/are chemically bonded to the dye. Optionally, a detached polar olefin copolymer may be blended with the dye-appended copolymer. Also disclosed is a broadband optical device comprising the novel dye/polymer compositions formed over an optical fiber. Improvements in the uniformity of spectral response and performance are observed across a wavelength band. Variable optical attenuators, switches, shutters, and couplers can be designed which incorporate the dye/polymer compositions. The invention is particularly useful in the 1500-1700 nm wavelength band.
摘要翻译：公开了新的染料/聚合物组合物，其在与光纤器件结合使用时，在宽带波长区域提供均匀的光谱响应。染料/聚合物组合物含有吸收最大约为900至约1300nm的红外吸收染料。含有衍生自具有连接有酯，苯或卤素取代基的极性烯烃的单体的一种或多种极性烯烃共聚物与染料化学键合。任选地，分离的极性烯烃共聚物可以与染料附着的共聚物共混。还公开了一种宽带光学装置，其包括在光纤上形成的新型染料/聚合物组合物。在波长带上观察到光谱响应和性能的均匀性的改善。可以设计可变光衰减器，开关，百叶窗和耦合器，其结合染料/聚合物组合物。本发明在1500-1700nm波长带中特别有用。

38. 发明授权

US06466729B1 Controllable fiber optic attenuators employing tapered and/or etched fiber sections 失效
标题翻译：采用锥形和/或蚀刻光纤段的可控光纤衰减器
公开(公告)号：US06466729B1
公开(公告)日：2002-10-15
申请号：US09539469
申请日：2000-03-30
申请人： Gregory A. Wagoner , Kevin J. McCallion , Walter Johnstone , Kwok Pong Chan , David G. Gascoyne
发明人： Gregory A. Wagoner , Kevin J. McCallion , Walter Johnstone , Kwok Pong Chan , David G. Gascoyne
IPC分类号： G02B600
CPC分类号： G02B6/2552 , G02B6/266 , G02B6/2835 , G02F1/0115 , G02F1/0147
摘要： Controllable fiber optic attenuators and attenuation systems are disclosed for controllably extracting optical energy from a fiber optic, and therefore attenuating the optical signal being transmitted through the fiber optic. A portion of the fiber optic is etched or tapered, thereby providing a side surface through which optical energy can be extracted. The portion of the fiber is suspended between two support points, and a controllable material is formed over the surface for controllably extracting optical energy according to a changeable stimulus applied thereto, which affects the refractive index thereof. In one embodiment, the changeable stimulus is temperature, and a controllable heating/cooling source can be provided in the attenuator for control of the attenuation. The limited amount of thermal contact between the suspended portion of the fiber optic and the controllable material to surrounding structures offers a more predictable response, and improved response time. The controllable material, in one embodiment, may be a dispersion controlled (e.g., matched) polymer, offering uniform spectral characteristics of attenuation across a wavelength band of interest.
摘要翻译：公开了可控光纤衰减器和衰减系统，用于可控地从光纤提取光能，并因此衰减通过光纤传输的光信号。光纤的一部分被蚀刻或渐缩，从而提供可以提取光能的侧表面。纤维的一部分悬挂在两个支撑点之间，并且在表面上形成可控材料，用于根据影响其折射率的可变刺激来可控地提取光能。在一个实施例中，可变的刺激是温度，并且可以在衰减器中提供可控制的加热/冷却源以控制衰减。光纤的悬挂部分和可控材料与周围结构之间的热接触的有限量提供了更可预测的响应，并且改善了响应时间。在一个实施方案中，可控材料可以是分散体控制（例如，匹配的）聚合物，其在所关注的波长带上提供均匀的衰减光谱特性。

39. 发明申请

US20090263612A1 System and Method for Photobleaching of Optical Media 审中-公开
标题翻译：光学媒体漂白的系统和方法
公开(公告)号：US20090263612A1
公开(公告)日：2009-10-22
申请号：US12105821
申请日：2008-04-18
申请人： David Gilles Gascoyne , Kwok Pong Chan , Daniel Olson , Marc Brian Wisnudel , Kasiraman Krishnan
发明人： David Gilles Gascoyne , Kwok Pong Chan , Daniel Olson , Marc Brian Wisnudel , Kasiraman Krishnan
IPC分类号： G11B7/24 , C08L31/00
CPC分类号： G11B7/252
摘要： A photobleachable ink composition having: at least one light-sensitive optical-state change material; at least one bleaching accelerant; at least one solvent; and at least one binder material; wherein the ink composition has a viscosity between about 0.1 centipoise and about 10,000 centipoise, and a maximum optical absorbance in a range from about 200 nanometers to about 800 nanometers; and wherein the ink composition is capable of change from a first optical state to a second optical state upon exposure to light. The composition may also include a plasticizer.
摘要翻译：一种可光漂白油墨组合物，其具有：至少一种光敏光学变化材料; 至少一种漂白促进剂; 至少一种溶剂; 和至少一种粘合剂材料; 其中所述油墨组合物的粘度在约0.1厘泊至约10,000厘泊之间，最大光吸收率在约200纳米至约800纳米的范围内; 并且其中所述油墨组合物在暴露于光时能够从第一光学状态变为第二光学状态。组合物还可以包含增塑剂。

40. 发明授权

US08278383B2 Methods of preparing polymer-organoclay composites and articles derived therefrom 有权
标题翻译：制备聚合物 - 有机粘土复合材料及其衍生物的方法
公开(公告)号：US08278383B2
公开(公告)日：2012-10-02
申请号：US13430801
申请日：2012-03-27
申请人： Kwok Pong Chan , Sarah Elizabeth Genovese , Erik C. Hagberg , David Bruce Hall , John Lester Maxam , Tara J. Mullen , Roy Ray Odle , Albert Santo Stella , James Mitchell White
发明人： Kwok Pong Chan , Sarah Elizabeth Genovese , Erik C. Hagberg , David Bruce Hall , John Lester Maxam , Tara J. Mullen , Roy Ray Odle , Albert Santo Stella , James Mitchell White
IPC分类号： C08K9/04 , C08K3/34
CPC分类号： C08F2/44
摘要： A method for preparing a polymer-organoclay composite composition comprises combining a solvent and an unexfoliated organoclay to provide a first mixture, wherein the unexfoliated organoclay comprises alternating inorganic silicate layers and organic layers, and has an initial spacing between the silicate layers; exposing the first mixture to an energized condition of a sufficient intensity and duration to increase the initial spacing of the inorganic silicate layers, to provide a second mixture; contacting the second mixture with a polymer composition so that the polymer composition fills at least one region located between at least one pair of silicate layers, wherein the polymer composition is at least partially soluble in the solvent; and removing at least a portion of the solvent from the second mixture, wherein the inorganic silicate layers remain separated by the polymer after removal of the solvent.
摘要翻译：一种制备聚合物 - 有机粘土复合材料组合物的方法，包括将溶剂和未剥离的有机粘土组合以提供第一混合物，其中未剥离的有机粘土包含交替的无机硅酸盐层和有机层，并且在硅酸盐层之间具有初始间隔; 将第一混合物暴露于足够强度和持续时间的通电状态以增加无机硅酸盐层的初始间隔，以提供第二混合物; 使所述第二混合物与聚合物组合物接触，使得所述聚合物组合物填充位于至少一对硅酸盐层之间的至少一个区域，其中所述聚合物组合物至少部分地可溶于所述溶剂中; 以及从所述第二混合物中除去至少一部分所述溶剂，其中在去除所述溶剂之后，所述无机硅酸盐层保持被所述聚合物分离。

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