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31. 发明授权

US4841029A Diazo colors and dyeing method using the same 失效
标题翻译：重氮颜色和染色方法使用相同
公开(公告)号：US4841029A
公开(公告)日：1989-06-20
申请号：US186656
申请日：1988-04-19
申请人： Yoshiaki Kato , Toshio Hihara
发明人： Yoshiaki Kato , Toshio Hihara
IPC分类号： C09B62/513 , C07D251/70 , C09B62/44 , D06P1/38 , D06P3/82 , D06P3/84 , D06P3/85 , D06P3/872
CPC分类号： D06P1/38 , C09B62/4415
摘要： A disazo color having three triazine rings, one of which is substituted with a reactive group of --NR.sup.1 --A--SO.sub.2 C.sub.2 H.sub.4 OSO.sub.3 M, wherein R.sup.1 represents a hydrogen atom or a lower alkyl group; A represents a substituted or unsubstituted phenylene or naphthylene group; and M represents a hydrogen atom or an alkali metal. The disazo color is capable of dyeing cellulose-containing fibers under conditions conventionally employed for dyeing polyester fibers with a disperse dye, making it possible to dye mixed fibers of cellulose fiber and polyester fiber in a single-bath through one step.
摘要翻译：具有三个三嗪环的二重色，其中一个被-NR1-A-SO2C2H4OSO3M的反应性基团取代，其中R1表示氢原子或低级烷基; A表示取代或未取代的亚苯基或亚萘基; M表示氢原子或碱金属。双色调能够在通常用于用分散染料染色聚酯纤维的条件下染色含纤维素纤维，使得可以通过一步将单纤维素纤维和聚酯纤维的混合纤维染色。

32. 发明申请

US20070271710A1 Disperse Dyes for Poly(Lactic Acid) Based Fibers 审中-公开
标题翻译：分散染料用于聚（乳酸）基纤维
公开(公告)号：US20070271710A1
公开(公告)日：2007-11-29
申请号：US11630496
申请日：2005-06-17
申请人： Daisuke Hosoda , Koichi Fujisaki , Toshio Hihara
发明人： Daisuke Hosoda , Koichi Fujisaki , Toshio Hihara
IPC分类号： D06P3/54 , D06P3/82
CPC分类号： D06P3/8276 , D06P3/54
摘要： The present invention relates to the use of a yellow and/or a red and/or a blue component of disperse dyes for dyeing poly(lactic acid) fibers or poly(lactic acid) based fibers.
摘要翻译：本发明涉及分散染料的黄色和/或红色和/或蓝色成分用于染色聚（乳酸）纤维或聚（乳酸）基纤维的用途。

33. 发明授权

US4276047A Anthraquinone reactive dyes for cellulose-containing fibers 失效
标题翻译：用于含纤维素纤维的蒽醌活性染料
公开(公告)号：US4276047A
公开(公告)日：1981-06-30
申请号：US141375
申请日：1980-04-18
申请人： Seiichi Imahori , Toshio Hihara , Tomio Yomeyama , Takao Hirota
发明人： Seiichi Imahori , Toshio Hihara , Tomio Yomeyama , Takao Hirota
IPC分类号： C09B62/06 , D06P1/382 , D06P3/60 , D06P3/66 , D06P3/82
CPC分类号： D06P1/382 , C09B62/06 , D06P3/6041 , D06P3/8233 , Y10S8/918 , Y10S8/922
摘要： An anthraquinone dye for direct printing and pad dyeing of cellulose-containing fibers and of the formula: ##STR1## wherein A represents a phenylene group, Y represents a group --NH-- or --C.sub.2 H.sub.4 O--, X represents a carbamoyl group which may be substituted with a lower alkyl group or a lower alkoxy-lower alkyl group, a sulfamoyl group which may be substituted with a lower alkyl group or a lower alkoxy-lower alkyl group, a halogen atom or a cyano group, and Z represents an amino group, a mono- or di-alkylamino group having 1-6 carbon atoms in total, an anilino group, a lower alkoxy group or a group --O(R.sup.1 O).sub.n -R.sup.2 in which R.sup.1 represents an ethylene group or a propylene group, R.sup.2 represents a methyl group or an ethyl group and n is an integer of 1-5.
摘要翻译：一种用于直链印染和含纤维素纤维的垫染色的蒽醌染料，其分子式如下：其中A表示亚苯基，Y表示基团-NH-或-C2H4O-，X表示可被取代的氨基甲酰基低级烷基或低级烷氧基 - 低级烷基，可被低级烷基或低级烷氧基 - 低级烷基，卤素原子或氰基取代的氨磺酰基，Z表示氨基，总共1-6个碳原子的单 - 或二 - 烷基氨基，苯胺基，低级烷氧基或基团-O（R 1 O）n -R 2，其中R 1表示亚乙基或亚丙基，R 2表示甲基或乙基，n为1-5的整数。

34. 发明申请

US20050272920A1 Yellow disperse dye mixture which has a high level of light fastness 有权
标题翻译：具有高耐光性的黄色分散染料混合物
公开(公告)号：US20050272920A1
公开(公告)日：2005-12-08
申请号：US10523656
申请日：2003-08-02
申请人： Toshio Hihara , Hiroshi Inoue , Wataru Seto
发明人： Toshio Hihara , Hiroshi Inoue , Wataru Seto
IPC分类号： C09B67/22 , D06P1/16 , D06P1/18 , D06P1/20 , D06P3/54 , D06P3/82
CPC分类号： D06P1/18 , C09B67/0041 , D06P1/16 , D06P1/20 , D06P3/54 , Y10S8/922
摘要： The present inventions refers to a dye mixture comprising from 25 to 80% by weight with respect to the total dyestuff fraction of the yellow dyestuff represented by the structural formula [1] and from 75 to 20% by weight with respect to the total dyestuff fraction of a yellow dyestuff represented by the structural formula [2] wherein R denotes a C1 to C4 hydroxyalkyl group.
摘要翻译：本发明是指相对于由结构式[1]表示的黄色染料的总染料份数和相对于总染料份数为75〜20重量％的25〜80重量％的染料混合物的由结构式[2]表示的黄色染料，其中R表示C 1至C 4羟烷基。

35. 发明授权

US06388057B1 Crystalline modification of a water-insoluble monoazo dye 失效
标题翻译：水不溶性单偶氮染料的结晶改性
公开(公告)号：US06388057B1
公开(公告)日：2002-05-14
申请号：US09869672
申请日：2001-08-31
申请人： Toshio Hihara , Hiroshi Inoue , Yousuke Takahashi
发明人： Toshio Hihara , Hiroshi Inoue , Yousuke Takahashi
IPC分类号： C09B6748
CPC分类号： C09B67/0015 , C09B67/0029 , Y10S8/922
摘要： A water-insoluble monoazo dye represented by the following structural formula [I] having a crystal modification characterized by an X-ray diffraction pattern (CuK&agr;) showing one strong peak at a diffraction angle (2&thgr;) of 11.1±0.1° and also four intermediate peaks at 8.1±0.1°, 21.8±0.1°, 23.1±0.1° and 25.2±0.1°.
摘要翻译：具有以衍射角（2θ）为11.1±0.1°的一个强峰的X射线衍射图（CuKalpha）为特征的结晶改性的下述结构式[I]表示的水不溶性单偶氮染料，以及四个中间体峰位于8.1±0.1°，21.8±0.1°，23.1±0.1°和25.2±0.1°。

36. 发明授权

US5545236A Red reactive dyes, their compositions and dyeing method employing them 失效
标题翻译：红色活性染料，它们的组成和使用它们的染色方法
公开(公告)号：US5545236A
公开(公告)日：1996-08-13
申请号：US400934
申请日：1995-03-09
申请人： Toshio Hihara , Yousuke Takahashi
发明人： Toshio Hihara , Yousuke Takahashi
IPC分类号： C09B62/51 , D06P1/38 , C09B67/22
CPC分类号： C09B62/51
摘要： A red reactive dye having the following formula (I) in its free acid form: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --C.sub.2 H.sub.4 W (wherein W is a group splittable by alkali), A is a C.sub.2-3 alkylene group or a C.sub.2-3 alkylenoxy C.sub.2-3 alkylene group, E is a hydrogen atom, a C.sub.1-3 alkyl group or --A--SO.sub.2 X (wherein A and X are as defined above), n is 0 or 1, l is 1 or 2, m is 0 or 1, and R is a hydrogen atom, --OH, --CN, --CH.sub.3, --CF.sub.3, --SO.sub.3 H, --COOH, --CH.sub.2 SO.sub.3 H or --CH.sub.2 SO.sub.2 X (wherein X is as defined above), provided that a compound of the formula (I) wherein R is a hydrogen atom, each of m and n is 0, l is 1, and --SO.sub.2 X is --SO.sub.2 CH.dbd.CH.sub.2 which is bonded at the ortho position to the azo group, is excluded.
摘要翻译：具有游离酸形式的具有下式（I）的红色活性染料：其中X是-CH = CH 2或-C 2 H 4 W（其中W是可被碱可裂的基团），A是C2-3 亚烷基或C2-3亚烷基氧基C2-3亚烷基，E是氢原子，C1-3烷基或-A-SO2X（其中A和X如上定义），n是0或1，l是 1或2，m为0或1，R为氢原子，-OH，-CN，-CH 3，-CF 3，-SO 3 H，-COOH，-CH 2 SO 3 H或-CH 2 SO 2 X（其中X如上定义）其中R为氢原子的式（I）化合物，m和n各自为0,1或2，-SO 2 X为与偶氮基的邻位键合的-SO 2 CH = CH 2。。

37. 发明授权

US07824451B2 Disperse dye mixtures which have a high degree of light fastness 有权
标题翻译：具有高耐光性的分散染料混合物
公开(公告)号：US07824451B2
公开(公告)日：2010-11-02
申请号：US10563198
申请日：2004-06-29
申请人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
发明人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
IPC分类号： D06P3/82
CPC分类号： C09B5/62 , C09B67/0038 , D06P3/54 , Y10S8/92 , Y10S8/922
摘要： The present invention provides a blue dye mixture which contains the pigments represented by formulae [1], [2], [3], and [4] The present invention also relates to dye mixtures in which there are compounded therewith a yellow dye mixture and/or a red dye mixture. The invention further relates to a method of dyeing polyester-based fibers and dyed polyester-based fibers and dyed polyester-based fiber materials.
摘要翻译：本发明提供了含有由式[1]，[2]，[3]和[4]表示的颜料的蓝色染料混合物。本发明还涉及其中与其混合黄色染料混合物的染料混合物， /或红色染料混合物。本发明还涉及一种染色涤纶基纤维和染色的聚酯基纤维和染色的聚酯基纤维材料的方法。

38. 发明申请

US20060230549A1 Disperse dye mixtures which have a high degree of light fastness 有权
标题翻译：具有高耐光性的分散染料混合物
公开(公告)号：US20060230549A1
公开(公告)日：2006-10-19
申请号：US10563198
申请日：2004-06-29
申请人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
发明人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
IPC分类号： D06P3/82
CPC分类号： C09B5/62 , C09B67/0038 , D06P3/54 , Y10S8/92 , Y10S8/922
摘要： The present invention provides a blue dye mixture which contains the pigments represented by formulae [1], [2], [3], and [4] The present invention also relates to dye mixtures in which there are compounded therewith a yellow dye mixture and/or a red dye mixture. The invention further relates to a method of dyeing polyester-based fibers and dyed polyester-based fibers and dyed polyester-based fiber materials.
摘要翻译：本发明提供了含有由式[1]，[2]，[3]和[4]表示的颜料的蓝色染料混合物。本发明还涉及其中与其混合黄色染料混合物的染料混合物， /或红色染料混合物。本发明还涉及一种染色涤纶基纤维和染色的聚酯基纤维和染色的聚酯基纤维材料的方法。

39. 发明授权

US5756690A Red reactive dyes, their compositions and dyeing method employing them 失效
公开(公告)号：US5756690A
公开(公告)日：1998-05-26
申请号：US639332
申请日：1996-04-25
申请人： Toshio Hihara , Yousuke Takahashi
发明人： Toshio Hihara , Yousuke Takahashi
IPC分类号： C09B62/51 , C09B62/507
CPC分类号： C09B62/51
摘要： A red reactive dye having the following formula (I) in its free acid form: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --C.sub.2 H.sub.4 W (wherein W is a group splittable by alkali), A is a C.sub.2-3 alkylene group or a C.sub.2-3 alkylenoxy C.sub.2-3 alkylene group, E is a hydrogen atom, a C.sub.1-3 alkyl group or --A--SO.sub.2 X (wherein A and X are as defined above), n is 0 or 1, l is 1 or 2, m is 0 or 1, and R is a hydrogen atom, --OH, --CN, --CH.sub.3, --CF.sub.3, --SO.sub.3 H, --COOH, --CH.sub.2 SO.sub.3 H or --CH.sub.2 SO.sub.2 X (wherein X is as defined above), provided that a compound of the formula (I) wherein R is a hydrogen atom, each of m and n is 0, l is 1, and --SO.sub.2 X is --SO.sub.2 CH.dbd.CH.sub.2 which is bonded at the ortho position to the azo group, is excluded.

40. 发明授权

US4960871A Fiber-reactive halotriazine pyridine-based monoazo colorant 失效
标题翻译：纤维反应性卤代三嗪吡啶类单偶氮染料
公开(公告)号：US4960871A
公开(公告)日：1990-10-02
申请号：US313316
申请日：1989-02-17
申请人： Toshio Hihara , Yukiharu Shimizu
发明人： Toshio Hihara , Yukiharu Shimizu
IPC分类号： C09B62/085 , D06P1/382 , D06P3/66 , D06P3/82 , D06P3/85
CPC分类号： C09B62/085 , D06P1/382 , D06P3/8228
摘要： Monoazo colorants represented by the general formula (I): ##STR1## wherein: D represents ##STR2## (wherein X represents a hydrogen atom or a halogen atom, and Y represents a nitro group, a lower alkylsulfonyl group, a thiocyanic acid group or a halogen atom), or ##STR3## (wherein P represents a nitro group or a lower alkylsulfonyl group, and Q and T each represents a hydrogen atom, a halogen atom or a cyano group);R.sup.1 and R.sup.2 each represents an ethylene group or a propylene group;R.sup.3 and R.sup.4 each represents a hydrogen atom or an alkyl group which may be substituted by a lower alkoxy group or a lower alkoxyalkoxy group; andZ represents a halogen atom.This monoazo colorants include a reactive type pyridine-based monoazo dye suitable for use in dyeing of cellulose or cellulose/polyester mixed fibers in red to orange.
摘要翻译：（I）表示的单偶氮着色剂：其中：D表示（其中X表示氢原子或卤素原子，Y表示硝基，低级烷基磺酰基，硫氰酸酯酸基或卤素原子）或（其中P表示硝基或低级烷基磺酰基，Q和T各自表示氢原子，卤素原子或氰基）。 R1和R2各自表示亚乙基或亚丙基; R3和R4各自表示氢原子或可被低级烷氧基或低级烷氧基烷氧基取代的烷基; Z表示卤素原子。该单偶氮着色剂包括适用于染色红色至橙色的纤维素或纤维素/聚酯混合纤维的反应型吡啶类单偶氮染料。

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