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31. 发明申请

US20110186440A1 ELECTRODEPOSITABLE COATING COMPOSITION COMPRISING A NON-SOLUBILIZED ZINC COMPOUND 有权
标题翻译：包含非溶解锌化合物的电沉积涂料组合物
公开(公告)号：US20110186440A1
公开(公告)日：2011-08-04
申请号：US12699930
申请日：2010-02-04
申请人： Kelly L. Moore , Richard F. Karabin , Alan J. Kaylo , Michael J. Pawlik
发明人： Kelly L. Moore , Richard F. Karabin , Alan J. Kaylo , Michael J. Pawlik
IPC分类号： C25D9/02
CPC分类号： C25D9/02
摘要： The present invention is directed to an electrodepositable coating composition comprising a non-solubilized zinc compound in an amount of at least 0.61 weight % based on the total resin solids of the electrodepositable coating composition.
摘要翻译：本发明涉及一种可电沉积涂料组合物，其包含基于可电沉积涂料组合物的总树脂固体至少为0.61重量％的非溶解锌化合物。

32. 发明授权

US6093298A Electrocoating compositions containing high aspect ratio clays as crater control agents 失效
标题翻译：含有高纵横比粘土作为火山口控制剂的电涂组合物
公开(公告)号：US6093298A
公开(公告)日：2000-07-25
申请号：US255206
申请日：1999-02-22
申请人： Alan J. Kaylo , Richard F. Karabin , Tie Lan , Michael G. Sandala
发明人： Alan J. Kaylo , Richard F. Karabin , Tie Lan , Michael G. Sandala
IPC分类号： C09D201/00 , C09D5/00 , C09D5/44 , C09D7/12 , C09D175/04 , C09D201/02 , C25D13/06 , C25D13/10
CPC分类号： C09D5/4492
摘要： Provided are cationic electrodepositable compositions comprised of an acidified aqueous dispersion of (a) an ungelled cationic resin, (b) a curing agent having at least two functional groups which are reactive with (a), and (c) an exfoliated silicate derived from a layered silicate. These compositions exhibit improved crater control. Also provided is a method of electrocoating conductive substrates using such compositions.
摘要翻译：提供的是阳离子可电沉积组合物，其包含（a）未凝胶阳离子树脂的酸化水分散体，（b）具有至少两个与（a）反应的官能团的固化剂，和（c）衍生自层状硅酸盐。这些组合物表现出改善的火山口控制。还提供了使用这种组合物电导涂层导电基材的方法。

33. 发明授权

US5936012A Cationic electrocoating compositions, method of making, and use 失效
标题翻译：阳离子电涂组合物，制备方法和使用
公开(公告)号：US5936012A
公开(公告)日：1999-08-10
申请号：US167687
申请日：1998-10-07
申请人： Marvin L. Kaufman , Patrick O'Neill , Richard F. Karabin , Gregory J. McCollum
发明人： Marvin L. Kaufman , Patrick O'Neill , Richard F. Karabin , Gregory J. McCollum
IPC分类号： C08G18/58 , C08G18/64 , C09D5/44 , C09D163/00 , C09D175/04 , C09D179/02 , C08K3/20
CPC分类号： C08G18/643 , C09D5/4434 , Y10T428/31511 , Y10T428/31551
摘要： An electrodepositable composition that has: (A) an active hydrogen-containing cationic resin, electrodepositable on a cathode, having: (1) a polyepoxide; (2) an oxygen-substituted diamine compound having the following formula: ##STR1## where n is an integer from 2 to 4; and where R.sup.1 or R.sup.2 are the same or different and either one or both contain at least one oxygen and are alkyl, cycloalkyl, substituted alkyl, or substituted cycloalkyl having from 1 to 6 carbon atoms, or R.sup.1 and R.sup.2 are alkanol groups having from 2 to 6 carbon atoms, or R.sup.1, R.sup.2, and the N atom form a cyclic group which is substituted or unsubstituted such as morpholine and 1-(3-aminopropyl) imidazole; and (B) at least partially blocked isocyanate or polyisocyanate curing agent. The diamine compound of Formula I can be used alone or in conjunction with one or more secondary amines, nonhydroxy group containing amines and/or amines with ring structures. Optionally, the polyepoxide can be chain extended with active hydrogen-containing compounds other than polyoxyalkylene polyamines. Also provided is a method of producing an active hydrogen-containing cationic resin composition, electrodepositable on a cathode, comprised of (a) mixing together in a suitable reaction vessel a polyepoxide, or the precursors of the polyepoxide, a polycarboxylic acid, a blocked isocyanate curing agent; (b) adding to the mixture of (a) a base catalyst and the diamine compound of Formula I; (c) polymerizing the mixture of (b) to form a resinous composition; and (d) neutralizing the resinous composition of (c) by adding the resinous composition to a dilute mixture of acid and water to form an aqueous dispersed electrodepositable cationic resin composition.
摘要翻译：一种电沉积组合物，其具有：（A）可阴离子电解的活性含氢阳离子树脂，其具有：（1）聚环氧化物; （2）具有下式的氧取代二胺化合物：其中n是2至4的整数; 并且其中R 1或R 2相同或不同，并且一个或两者含有至少一个氧，并且是具有1至6个碳原子的烷基，环烷基，取代的烷基或取代的环烷基，或者R 1和R 2是具有2个至6个碳原子，或R 1，R 2和N原子形成取代或未取代的环状基团，例如吗啉和1-（3-氨基丙基）咪唑; 和（B）至少部分封端的异氰酸酯或多异氰酸酯固化剂。式I的二胺化合物可以单独使用或与一种或多种仲胺，含羟基的胺和/或具有环结构的胺结合使用。任选地，聚环氧化物可以用除聚氧化烯多胺以外的活性含氢化合物链延伸。还提供了一种生产可阴离子电沉积的含活性氢的阳离子树脂组合物的方法，其包括（a）在合适的反应容器中在聚环氧化物或聚环氧化物的前体，多元羧酸，封端异氰酸酯固化剂（b）向（a）碱催化剂和式I的二胺化合物的混合物中加入; （c）使（b）的混合物聚合以形成树脂组合物; 和（d）通过将树脂组合物加入酸和水的稀混合物中和（c）的树脂组合物，形成水分散的可电沉积阳离子树脂组合物。

34. 发明授权

US5582704A Cationic resin and capped polyisocyanate curing agent suitable for use in electrodeposition 失效
标题翻译：阳离子树脂和封端的多异氰酸酯固化剂适用于电沉积
公开(公告)号：US5582704A
公开(公告)日：1996-12-10
申请号：US334712
申请日：1994-11-04
申请人： Joseph T. Valko , Philippe Faucher , Richard F. Karabin , Thomas C. Moriarity , V. Eswarakrishnan , Ellor J. Van Buskirk , Gregory J. McCollum , Raphael O. Kollah
发明人： Joseph T. Valko , Philippe Faucher , Richard F. Karabin , Thomas C. Moriarity , V. Eswarakrishnan , Ellor J. Van Buskirk , Gregory J. McCollum , Raphael O. Kollah
IPC分类号： C09D163/00 , C08G18/08 , C08G18/32 , C08G18/42 , C08G18/58 , C08G18/64 , C08G18/80 , C09D5/08 , C09D5/44 , C09D175/04 , C09D175/12 , C25D13/04
CPC分类号： C08G18/3256 , C08G18/0814 , C08G18/0823 , C08G18/4294 , C08G18/581 , C08G18/584 , C08G18/6407 , C08G18/643 , C08G18/80 , C08G18/8009 , C08G18/8048 , C08G18/8064 , C09D5/4434 , C09D5/4453 , C09D5/4457
摘要： An electrodepositable composition is provided comprising:(A) a non-gelled cationic resin which is derived from a polyepoxide and which contains in the resin molecule cationic salt groups and active hydrogen groups selected from aliphatic hydroxyl and primary and secondary amino; and present as a separate component(B) a fully capped polyisocyanate curing agent containing substantially no free isocyanate groups, The electrodepositable composition contains from about 0.02 to 1.0 milliequivalents phenolic hydroxyl groups per gram of resin solids, and from about 0.1 to 2.0 milliequivalents beta-hydroxy ester groups per gram of resin solids. The composition provides excellent corrosion resistance when electrodeposited over steel substrates, and does not require lead in the formulation nor the use of a conventional chrome rinse for the steel substrate pretreatment before electrodeposition.
摘要翻译：提供了一种可电沉积的组合物，其包含：（A）衍生自聚环氧化物的非胶凝阳离子树脂，其在树脂分子中含有阳离子盐基团和选自脂族羟基和伯和仲氨基的活性氢基团; 并且作为单独的组分（B）存在基本上不含游离异氰酸酯基团的完全封端的多异氰酸酯固化剂。该可电沉积组合物每克树脂固体含有约0.02-1.0毫当量酚羟基，和约0.1-2.0毫当量β- 羟基酯基团/克树脂固体。当电沉积在钢基材上时，该组合物提供优异的耐腐蚀性，并且在电沉积之前不需要配方中的铅，也不使用常规的铬漂洗用于钢基材预处理。

35. 发明授权

US08492542B2 Method for producing bicyclic guanidines by use of a cyclic thiourea 有权
标题翻译：通过使用环状硫脲制备双环胍的方法
公开(公告)号：US08492542B2
公开(公告)日：2013-07-23
申请号：US12120725
申请日：2008-05-15
申请人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Thomas R. Hockswender , Gregory J. McCollum
发明人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Thomas R. Hockswender , Gregory J. McCollum
IPC分类号： C07D487/04 , C07D239/10 , C07D235/02 , C07D233/44
CPC分类号： C07D487/04
摘要： The present invention is directed to a method producing bicyclic guanidine comprising heating a cyclic thiourea to a temperature ranging from ≧140° C. in a substantially non-hydrocarbon solvent to form the bicyclic guanidine.
摘要翻译：本发明涉及一种产生双环胍的方法，其包括在基本上非烃溶剂中加热环状硫脲至> 140℃的温度以形成双环胍。

36. 发明授权

US08389651B2 Electrodepositable coating composition comprising a non-solubilized zinc compound 有权
标题翻译：包含未溶解的锌化合物的电沉积涂料组合物
公开(公告)号：US08389651B2
公开(公告)日：2013-03-05
申请号：US12699930
申请日：2010-02-04
申请人： Kelly L. Moore , Richard F. Karabin , Alan J. Kaylo , Michael J. Pawlik
发明人： Kelly L. Moore , Richard F. Karabin , Alan J. Kaylo , Michael J. Pawlik
IPC分类号： C08G59/14
CPC分类号： C25D9/02
摘要： The present invention is directed to an electrodepositable coating composition comprising a non-solubilized zinc compound in an amount of at least 0.61 weight % based on the total resin solids of the electrodepositable coating composition.
摘要翻译：本发明涉及一种可电沉积涂料组合物，其包含基于可电沉积涂料组合物的总树脂固体至少为0.61重量％的非溶解锌化合物。

37. 发明授权

US08039618B2 Method for producing bicyclic guanidines by use of a cyclic urea 有权
标题翻译：通过使用环状脲制备双环胍的方法
公开(公告)号：US08039618B2
公开(公告)日：2011-10-18
申请号：US12118082
申请日：2008-05-09
申请人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Gregory J. McCollum
发明人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Gregory J. McCollum
IPC分类号： C07D471/04
CPC分类号： C07D487/04
摘要： The present invention is directed to a method for producing bicyclic guanidines comprising heating a cyclic urea to a temperature >200° C. to form the bicyclic guanidines.
摘要翻译：本发明涉及一种制备双环胍的方法，包括将环状脲加热到> 200℃的温度以形成双环胍。

38. 发明申请

US20090281313A1 METHOD FOR PRODUCING BICYCLIC GUANIDINES BY USE OF A CYCLIC UREA 有权
标题翻译：通过使用循环尿素生产双环类药物的方法
公开(公告)号：US20090281313A1
公开(公告)日：2009-11-12
申请号：US12118082
申请日：2008-05-09
申请人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Gregory J. McCollum
发明人： Britt A. Minch , Charles R. Hickenboth , Richard F. Karabin , Steven R. Zawacky , Gregory J. McCollum
IPC分类号： C07D471/04
CPC分类号： C07D487/04
摘要： The present invention is directed to a method for producing bicyclic guanidines comprising heating a cyclic urea to a temperature >200° C. to form the bicyclic guanidines.
摘要翻译：本发明涉及一种制备双环胍的方法，包括将环状脲加热到> 200℃的温度以形成双环胍。

39. 发明授权

US06190525B1 Electrodeposition baths containing yttrium 有权
标题翻译：含有钇的电沉积浴
公开(公告)号：US06190525B1
公开(公告)日：2001-02-20
申请号：US09298104
申请日：1999-04-22
申请人： Richard F. Karabin , Alan J. Kaylo
发明人： Richard F. Karabin , Alan J. Kaylo
IPC分类号： C25D1310
CPC分类号： C09D5/4492 , C09D5/448 , Y10S524/901
摘要： Disclosed are improved electrodeposition bath compositions comprising a resinous phase dispersed in an aqueous medium, the resinous phase being comprised of an active hydrogen containing ionic electrodepositable resin and a curing agent, where the improvement comprises the addition to an electrodeposition bath of at least one source of yttrium in an amount of about 10 to 10,000 parts per million of total yttrium based on electrodeposition bath weight. The electrodeposition bath compositions are preferably cationic and provide for excellent corrosion resistance over a variety of metal substrates including untreated steel. Also disclosed is a method of electrocoating a conductive substrate using the improved electrodeposition bath compositions of the invention. Metallic substrates which are coated using the method of the invention are also disclosed.
摘要翻译：公开了改进的电沉积浴组合物，其包含分散在水性介质中的树脂相，所述树脂相由含活性氢的离子可电沉积树脂和固化剂组成，其中改进包括添加至少一种源的电沉积浴基于电沉积浴重量，钇的总钇的量为约10至10,000份。电沉积浴组合物优选是阳离子的，并且在包括未处理的钢的各种金属基材上提供优异的耐腐蚀性。还公开了使用本发明的改进的电沉积浴组合物电导涂层的方法。还公开了使用本发明的方法涂覆的金属基底。

40. 发明授权

US6107387A Acidified aqueous dispersions of high aspect ratio clays 失效
标题翻译：酸化的高纵横比粘土的水性分散体
公开(公告)号：US6107387A
公开(公告)日：2000-08-22
申请号：US255205
申请日：1999-02-22
申请人： Alan J. Kaylo , Richard F. Karabin , Tie Lan , Michael G. Sandala
发明人： Alan J. Kaylo , Richard F. Karabin , Tie Lan , Michael G. Sandala
IPC分类号： C01B33/44 , C08K3/36
CPC分类号： C01B33/44
摘要： Provided are acidified aqueous stable dispersions of an exfoliated silicate derived from a silicate having a layer lattice structure in which the silicate layer units have a thickness of 5 to 25 Angstroms, wherein the exchange capacity ranges from 30 to 200 millequivalents per gram of silicate having a layer lattice structure, and wherein the silicate materials have been exfoliated with a cationic group-containing polymer or polymer having functional groups which can be post-reacted to form cationic groups. These silicate dispersions are useful in coating compositions, particularly in electrodepositable coating compositions, where they impart improved crater control.
摘要翻译：提供衍生自具有层状晶格结构的硅酸盐的剥离的硅酸盐的酸化水性稳定分散体，其中硅酸盐层单元的厚度为5至25埃，其中交换容量为每克硅酸盐具有30至200立方米，具有层状晶格结构，并且其中硅酸盐材料已经被含阳离子基团的聚合物或具有可以后反应形成阳离子基团的官能团的聚合物剥离。这些硅酸盐分散体可用于涂料组合物，特别是在可电沉积涂料组合物中，其中它们赋予改进的凹坑控制。

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