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31. 发明申请

US20060167312A1 Process for producing 5-iodo-2-methylbenzoic acid 失效
标题翻译： 5-碘-2-甲基苯甲酸的制备方法
公开(公告)号：US20060167312A1
公开(公告)日：2006-07-27
申请号：US10563088
申请日：2004-07-01
申请人： Takafumi Yoshimura , Toshio Hidaka , Yoshifumi Sato , Norio Fushimi , Kazuhiro Yamada
发明人： Takafumi Yoshimura , Toshio Hidaka , Yoshifumi Sato , Norio Fushimi , Kazuhiro Yamada
IPC分类号： C07C63/04
CPC分类号： C07C51/363 , C07C63/70
摘要： The present invention provides a process for producing 5-iodo-2-methylbenzoic acid through iodination of 2-methylbenzoic acid, the process including, as essential steps, a reaction step of iodinating 2-methylbenzoic acid in the presence of a microporous compound, iodine, an oxidizing agent, and acetic anhydride, and a purification step including sublimation, distillation, crystallization, or a combination of two or more of these. According to the present invention, 5-iodo-2-methylbenzoic acid, which is useful for producing functional chemicals such as drugs, can be produced at high purity and high yield in a simple manner. Since the production process includes a simple reaction step and a simple separation/purification step, the load of purification is mitigated. In addition, the microporous compound such as a zeolite catalyst which has been separated and recovered from the reaction mixture can be repeatedly employed after performing of a simple treatment. Thus, the production process ensures a long service life of catalysts and high efficiency.
摘要翻译：本发明提供了通过2-甲基苯甲酸碘化生产5-碘-2-甲基苯甲酸的方法，该方法包括作为必要步骤的步骤，在微孔化合物存在下碘化2-甲基苯甲酸，碘，氧化剂和乙酸酐，以及包括升华，蒸馏，结晶或这些中的两种或更多种的组合的纯化步骤。根据本发明，可以以高纯度和高产率以简单的方式制备可用于制备功能性化学物质如药物的5-碘-2-甲基苯甲酸。由于生产过程包括简单的反应步骤和简单的分离/纯化步骤，减轻了纯化负荷。此外，在进行简单处理之后，可以重复使用从反应混合物中分离回收的微孔化合物如沸石催化剂。因此，生产过程确保催化剂的使用寿命长，效率高。

32. 发明授权

US06590124B1 Catalysts for producing methylamines and method for manufacturing the same 有权
公开(公告)号：US06590124B1
公开(公告)日：2003-07-08
申请号：US10303697
申请日：2002-11-26
申请人： Toshio Hidaka , Katsumi Higuchi , Takeshi Kawai
发明人： Toshio Hidaka , Katsumi Higuchi , Takeshi Kawai
IPC分类号： C07C20916
CPC分类号： C07C209/16 , B01J29/85 , B01J35/023 , B01J2229/42 , C01B37/08 , C07C211/04
摘要： Catalysts useful for producing methylamines and having practical catalyst life and large selectivity for dimethylamine comprise crystalline silicoaluminophosphate molecular sieves which have a molar ratio of silicon atom to aluminum atom in the range of 0.01-0.30.

33. 发明授权

US06495724B1 Catalysts for producing methylamines and method for manufacturing the same 失效
标题翻译：用于生产甲胺的催化剂及其制造方法
公开(公告)号：US06495724B1
公开(公告)日：2002-12-17
申请号：US09559751
申请日：2000-04-27
申请人： Toshio Hidaka , Katsumi Higuchi , Takeshi Kawai
发明人： Toshio Hidaka , Katsumi Higuchi , Takeshi Kawai
IPC分类号： C07C20964
CPC分类号： C07C209/16 , B01J29/85 , B01J35/023 , B01J2229/42 , C01B37/08 , C07C211/04
摘要： Catalysts useful for producing methylamines and having practical catalyst life and large selectivity for dimethylamine comprise crystalline silicoaluminophosphate molecular sieves which have a molar ratio of silicon atom to aluminum atom in the range of 0.01-0.30.
摘要翻译：可用于生产甲胺并具有实用的催化剂寿命和对二甲胺的大选择性的催化剂包括硅原子与铝原子的摩尔比在0.01-0.30范围内的结晶硅铝磷酸盐分子筛。

34. 发明授权

US5250101A Process for the production of fine powder 失效
标题翻译：生产细粉的工艺
公开(公告)号：US5250101A
公开(公告)日：1993-10-05
申请号：US862218
申请日：1992-04-02
申请人： Toshio Hidaka , Takamasa Kawakami , Satoru Makinose
发明人： Toshio Hidaka , Takamasa Kawakami , Satoru Makinose
IPC分类号： B22F9/30 , C01B13/18 , B22F9/24
CPC分类号： C01B13/18 , B22F9/30 , C01P2004/03 , C01P2004/50 , C01P2004/61 , C01P2004/62 , C01P2006/12
摘要： A process for the production of a fine powder suitable for use in the fields of electronic materials, catalysts, powder metallurgy, pigments and adsorbens. The powder has a primary particle diameter of not more than 0.5 .mu.m, an average secondary aggregate particle diameter of not more than 10 .mu.m and a secondary aggregate particle specific surface area of 2 to 250 m.sup.2 /g, and is produced by a process comprising heating an organic acid metal salt in the presence of palladium, which lowers the thermal decomposition temperature of the salt, at a temperature elevation rate of 0.5.degree. to 20.degree.C./minute and thermally decomposing the organic acid metal salt in the presence of the palladium in the temperature range of not higher than 400.degree.C.

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