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31. 发明授权

US5231211A Method for preparing di(organo) esters of pyrocarbonic acid 失效
标题翻译：制备热碳酸二（有机）酯的方法
公开(公告)号：US5231211A
公开(公告)日：1993-07-27
申请号：US947211
申请日：1992-09-18
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： B01J31/02 , B01J31/06 , C07B61/00 , C07C68/02 , C07C69/96
CPC分类号： C07C68/02
摘要： Di(organo) esters of pyrocarbonic acid, e.g., dialkyl pyrocarbonates, such as diethyl pyrocarbonate, are prepared by reaction of the corresponding organohaloformate with aqueous alkali metal hydroxide, e.g., sodium hydroxide, in the substantial absence of an organic solvent and in the presence of a catalytic amount of a bis[poly(oxy(C.sub.2 -C.sub.4)alkylene)] C.sub.6 -C.sub.20 aliphatic amine, e.g., coco bis(polyoxyethylene) amine.
摘要翻译：通过相应的有机卤代甲酸酯与碱金属氢氧化物如氢氧化钠在基本上不存在有机溶剂的条件下反应制备焦碳碳酸二（有机）酯，例如焦碳酸二乙酯，催化量的双[聚（氧（C 2 -C 4）亚烷基）] C 6 -C 20脂族胺，例如椰油双（聚氧乙烯）胺。

32. 发明授权

US4742133A Poly(allyl carbonate)-functional prepolymers prepared by treatment with molecular oxygen 失效
标题翻译：通过用分子氧处理制备的聚（碳酸烯丙酯）官能预聚物
公开(公告)号：US4742133A
公开(公告)日：1988-05-03
申请号：US779400
申请日：1985-09-24
申请人： Felicia Y. Tang , Robert H. Tang
发明人： Felicia Y. Tang , Robert H. Tang
IPC分类号： C08F4/00 , C08F18/24
CPC分类号： C08F18/24
摘要： A liquid monomer composition comprising of at least one poly(allyl carbonate)-functional monomer is contacted with molecular oxygen to produce a liquid intermediate composition which is then heated to produce a polymerizable, liquid substantially gel-free composition which contains poly(allyl carbonate)-funtional prepolymer which has an allylic utilization of at least about 12 percent.
摘要翻译：包含至少一种聚（碳酸烯丙酯）官能单体的液体单体组合物与分子氧接触以产生液体中间体组合物，然后将其加热以产生可聚合的液体基本上不含凝胶的组合物，其含有聚（碳酸烯丙酯）其具有至少约12％的烯丙基利用率的自由基预聚物。

33. 发明授权

US4613656A Method for polymerizing bis(allyl carbonate) resin 失效
标题翻译：聚合双（烯丙基碳酸酯）树脂的方法
公开(公告)号：US4613656A
公开(公告)日：1986-09-23
申请号：US674115
申请日：1984-11-23
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： C08F18/24 , C08F110/00
CPC分类号： C08F18/24
摘要： Fully cured, intact, solid castings of bis(allyl carbonate) resin, e.g., diethylene glycol bis(allyl carbonate), are prepared by polymerizing the resin with between about 0.75 and about 1.50 parts, per hundred parts of resin, of a monoperoxycarbonate, e.g., tertiarybutylperoxy isopropyl carbonate. An adhesion reducing amount, e.g., between about 25 and about 75 parts, per million parts of resin, of a mold release agent is incorporated into the liquid resin monomer to avoid cracking of the casting. Use of a mold release agent is not required when the resin is prepolymerized to about 15-50 percent allylic utilization.
摘要翻译：通过将树脂与每100份树脂的单过氧碳酸酯的约0.75至约1.50份聚合制备双（烯丙基碳酸酯）树脂的完全固化，完整的固体铸件，例如二甘醇双（碳酸烯丙酯）例如叔丁基过氧化异丙基碳酸酯。将每百万份树脂的脱模剂的粘合降低量例如约25至约75份加入到液态树脂单体中以避免铸件破裂。当树脂预聚合至约15-50％的烯丙基利用时，不需要使用脱模剂。

34. 发明授权

US4552682A Peroxide composition containing phenolic antioxidant 失效
标题翻译：含有酚类抗氧化剂的过氧化物成分
公开(公告)号：US4552682A
公开(公告)日：1985-11-12
申请号：US430058
申请日：1982-09-30
申请人： Donald J. Black , Robert H. Tang
发明人： Donald J. Black , Robert H. Tang
IPC分类号： C07C409/00 , C09K15/08 , C01B13/00 , C01B15/00 , C09K3/00
CPC分类号： C09K15/08
摘要： Phenolic antioxidant compounds are added to aqueous dispersions of organic peroxide to reduce the rate of self induced homolytic decomposition of the peroxide at temperatures of from above -5.degree. C. to +20.degree. C. From about 0.1 to about 2 mole percent, basis the organic peroxide, of phenolic antioxidant is preferentially used. Among the organic peroxides described are the dialkylperoxydicarbonates. Among the phenolic antioxidants described are hindered phenols such as 2,6-di-tertiarybutyl-4-methylphenol.
摘要翻译：将酚类抗氧化剂加入到有机过氧化物的水性分散体中以降低过氧化氢在-5℃至+ 20℃的温度下自身均分解的速率。约0.1至约2摩尔％，基于优选使用酚类抗氧化剂的有机过氧化物。所描述的有机过氧化物是二烷基过氧化二碳酸酯。所述的酚类抗氧化剂中的受阻酚如2,6-二叔丁基-4-甲基苯酚。

35. 发明授权

US4522991A Method for polymerizing ethylenically unsaturated monomer with novel organic percarbonates 失效
标题翻译：用新型有机过碳酸酯聚合烯属不饱和单体的方法
公开(公告)号：US4522991A
公开(公告)日：1985-06-11
申请号：US642304
申请日：1984-08-20
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： C07C409/40 , C08F2/08 , C08F14/06 , C08F214/06 , C08F299/04 , C08F4/32
CPC分类号： C07C255/00 , C08F299/0457
摘要： Organic peroxydicarbonates represented by the following graphic formula are described. ##STR1## In the formula, R and R' are each selected from an alkyl group containing from 1 to 4 carbon atoms, a cycloalkyl group of from 5 to 7 carbon atoms, a C.sub.1 -C.sub.4 alkyl substituted cycloalkyl group, or participate in a cycloalkyl group having from 5 to 7 carbon atoms, provided that when one of R and R' is cycloalkyl, the other is alkyl. The peroxydicarbonates are useful as initiators for the polymerization or copolymerization of ethylenically unsaturated monomers or the cross-linking of unsaturated polyester resins. The organic peroxydicarbonates can be used in combination with commercially available peroxydicarbonates, particularly those having a shorter half-life.
摘要翻译：描述由以下图形公式表示的有机过氧化二碳酸酯。在该式中，R和R'各自选自含有1至4个碳原子的烷基，5至7个碳原子的环烷基，C 1 -C 4烷基取代的环烷基，或者参与具有5至7个碳原子的环烷基，条件是当R和R'中的一个是环烷基时，另一个是烷基。过氧二碳酸酯可用作烯属不饱和单体的聚合或共聚的引发剂或不饱和聚酯树脂的交联。有机过氧碳酸氢盐可以与市售的过氧化二碳酸酯组合使用，特别是半衰期较短的那些。

36. 发明授权

US4515929A Peroxide composition 失效
标题翻译：过氧化物组成
公开(公告)号：US4515929A
公开(公告)日：1985-05-07
申请号：US518162
申请日：1983-07-28
申请人： Robert H. Tang
发明人： Robert H. Tang
IPC分类号： C07C409/00 , C08F4/32 , C08F4/38 , C01B13/00 , C01B15/00 , C09K3/00
CPC分类号： C08F4/38 , C07C407/006
摘要： Dispersions of organic peroxide, e.g., organic peroxydicarbonates, in an aqueous medium are stabilized against homolytic peroxide decomposition at temperatures of from about -5.degree. C. to 20.degree. C. by incorporating into the dispersion, e.g., into the organic peroxide phase, from about 0.05 to about 1 mole percent, basis the organic peroxide, of diphenyl peroxydicarbonate or di(alkyl substituted) phenyl peroxydicarbonate.
摘要翻译：有机过氧化物，例如有机过氧化二碳酸酯在水性介质中的分散体，在约-5℃至20℃的温度下，通过将分散体（例如，从有机过氧化物相中）约0.05至约1摩尔％，基于有机过氧化物，过氧化二碳酸二苯酯或二（烷基取代的）苯基过氧化二碳酸酯。

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