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31. 发明授权

US07420080B2 Multistage continuous preparation of cycloaliphatic diisocyanates 有权
公开(公告)号：US07420080B2
公开(公告)日：2008-09-02
申请号：US11101428
申请日：2005-04-08
申请人： Stephan Kohlstruk , Manfred Kreczinski , Hans-Werner Michalczak
发明人： Stephan Kohlstruk , Manfred Kreczinski , Hans-Werner Michalczak
IPC分类号： C07C263/00 , C07C249/00
CPC分类号： C07C263/06 , C07C2601/14 , C07C265/14
摘要： The invention relates to a multistage process for continuous and phosgene-free preparation of cycloaliphatic diisocyanates.

32. 发明申请

US20050043562A1 Multistage continuous preparation of cycloaliphatic diisocyanates 有权
标题翻译：多级连续制备脂环族二异氰酸酯
公开(公告)号：US20050043562A1
公开(公告)日：2005-02-24
申请号：US10921934
申请日：2004-08-20
申请人： Stephan Kohlstruk , Manfred Kreczinski , Rainer Elm , Hans-Werner Michalczak
发明人： Stephan Kohlstruk , Manfred Kreczinski , Rainer Elm , Hans-Werner Michalczak
IPC分类号： C07C263/04 , C07C263/06 , C07C265/14 , C07C261/04
CPC分类号： C07C265/14 , C07C263/06 , C07C2601/14
摘要： A multistage process for continuous and phosgene-free preparation of cycloaliphatic diisocyanates.
摘要翻译：用于连续和无光气制备环脂族二异氰酸酯的多阶段方法。

33. 发明授权

US06452003B1 Process for preparing low-odor and storage-stable monomer-containing polyisocyanurates from isophorone diisocyanate 失效
标题翻译：从异佛尔酮二异氰酸酯制备低气味和储存稳定的含单体聚异氰脲酸酯的方法
公开(公告)号：US06452003B1
公开(公告)日：2002-09-17
申请号：US09899241
申请日：2001-07-06
申请人： Michael Ewald , Rainer Lomoelder , Stephan Kohlstruk
发明人： Michael Ewald , Rainer Lomoelder , Stephan Kohlstruk
IPC分类号： C07D25134
CPC分类号： C08G18/20 , C08G18/022 , C08G18/1875 , C08G18/2018
摘要： The present invention provides a process, which includes: partially trimerizing isophorone diisocyanate in the presence of a catalyst having the formula: [R—NX3]⊕Y⊖ wherein R and X are butyl groups and Y− is CH3COO−; or wherein R is a benzyl group, Y− is a carboxylate anion having from 4 to 8 carbon atoms and each X is an alkylene group having from 2 to 3 carbon atoms, wherein the three alkylene groups share a common carbon atom and, together with the N atom in the formula, form a tricyclic structure, and wherein at least one alkyene group has at least one OH group in an &agr; or &bgr; &ggr; position relative to the N atom, to obtain a monomer-containing polyisocyanurate mixture. The present invention also provides a monomer-containing polyisocyanurate mixture made from the above process.
摘要翻译：本发明提供了一种方法，其包括：在具有下式的催化剂存在下部分三聚异佛尔酮二异氰酸酯：其中R和X是丁基，Y-是CH 3 COO-; 或者R为苄基时，Y-为碳原子数为4〜8的羧酸根阴离子，X为碳原子数2〜3的亚烷基，其中，3个亚烷基具有共同的碳原子，式中的N原子形成三环结构，并且其中至少一个烷基在相对于N原子的α或βγ位置具有至少一个OH基团，以获得含单体的聚异氰脲酸酯混合物。本发明还提供由上述方法制备的含单体的聚异氰脲酸酯混合物。

34. 发明授权

US08536370B2 Low chlorine, multi-staged method for producing cycloaliphatic disocyanates 有权
标题翻译：低氯，多阶段生产脂环族二异氰酸酯的方法
公开(公告)号：US08536370B2
公开(公告)日：2013-09-17
申请号：US12922280
申请日：2009-05-18
申请人： Gerda Grund , Manfred Kreczinski , Stephan Kohlstruk , Christian Lettmann
发明人： Gerda Grund , Manfred Kreczinski , Stephan Kohlstruk , Christian Lettmann
IPC分类号： C07C263/12 , C07C263/06
CPC分类号： C07C209/78 , C07C211/50 , C07C265/14
摘要： Low chlorine, multi-staged method for producing cycloaliphatic diisocyanates. The invention relates to a multi-staged method for the continuous low-chlorine production of cycloaliphatic diisocyanates, comprising the synthesis of diaminodipheynl alkanes, the hydration thereof into the corresponding cycloaliphatic diamines and the subsequent conversion of cycloaliphatic diamines to the corresponding cycloalkylene biscarbamates and the thermal cleaving of the latter into the cycloaliphatic diisocyanates and alcohol.
摘要翻译：低氯，多阶段生产脂环族二异氰酸酯的方法。本发明涉及一种用于连续低氯生产脂环族二异氰酸酯的多阶段方法，其包括合成二氨基二炔烃，将其水合成相应的脂环族二胺，随后将脂环族二胺转化为相应的亚环烷基双氨基甲酸酯和热将后者切割成脂环族二异氰酸酯和醇。

35. 发明申请

US20110301345A1 METHOD FOR PRODUCING 1:1 ADDUCTS HAVING A LOW MONOMER CONTENT FROM HYDROXYALKYL(METH)ACRYLATES AND DIISOCYANATES 有权
标题翻译：用于生产具有低羟基甲基（甲基）丙烯酸酯和二异氰酸酯的低单体含量的1：1添加剂的方法
公开(公告)号：US20110301345A1
公开(公告)日：2011-12-08
申请号：US13201469
申请日：2010-02-08
申请人： Emmanouil Spyrou , Stephan Kohlstruk , Lars Hellkuhl , Heinz Grosse-Beck , Marita Druener
发明人： Emmanouil Spyrou , Stephan Kohlstruk , Lars Hellkuhl , Heinz Grosse-Beck , Marita Druener
IPC分类号： C07D229/00 , C07C69/00
CPC分类号： C08G18/8175 , C08G18/027 , C08G18/798 , C09D175/16
摘要： The present invention relates to the production and the use of 1:1 adducts having a low monomer content from hydroxyalkyl(meth)acrylates and diisocyanates.
摘要翻译：本发明涉及由（甲基）丙烯酸羟烷基酯和二异氰酸酯制备和使用具有低单体含量的1:1加合物。

36. 发明申请

US20110028755A1 LOW CHLORINE, MULTI-STAGED METHOD FOR PRODUCING CYCLOALIPHATIC DISOCYANATES 有权
标题翻译：低氯化物，生产环状二异氰酸酯的多阶段方法
公开(公告)号：US20110028755A1
公开(公告)日：2011-02-03
申请号：US12922280
申请日：2009-05-18
申请人： Gerda Grund , Manfred Kreczinski , Stephan Kohlstruk , Christian Lettmann
发明人： Gerda Grund , Manfred Kreczinski , Stephan Kohlstruk , Christian Lettmann
IPC分类号： C07C263/00 , C07C263/20
CPC分类号： C07C209/78 , C07C211/50 , C07C265/14
摘要： Low chlorine, multi-staged method for producing cycloaliphatic diisocyanates. The invention relates to a multi-staged method for the continuous low-chlorine production of cycloaliphatic diisocyanates, comprising the synthesis of diaminodipheynl alkanes, the hydration thereof into the corresponding cycloaliphatic diamines and the subsequent conversion of cycloaliphatic diamines to the corresponding cycloalkylene biscarbamates and the thermal cleaving of the latter into the cycloaliphatic diisocyanates and alcohol.
摘要翻译：低氯，多阶段生产脂环族二异氰酸酯的方法。本发明涉及一种用于连续低氯生产脂环族二异氰酸酯的多阶段方法，其包括合成二氨基二炔烃，将其水合成相应的脂环族二胺，随后将脂环族二胺转化为相应的亚环烷基双氨基甲酸酯和热将后者切割成脂环族二异氰酸酯和醇。

37. 发明申请

US20100036154A1 PROCESS FOR THE CONTINUOUS PREPARATION OF (CYCLO)ALIPHATIC DIISOCYANATES 有权
标题翻译：连续制备（环己烷）二异氰酸酯的方法
公开(公告)号：US20100036154A1
公开(公告)日：2010-02-11
申请号：US12519795
申请日：2007-11-05
申请人： Hans-Werner Michalczak , Stephan Kohlstruk , Manfred Kreczinski , Gerda Grund , Rainer Lomoelder
发明人： Hans-Werner Michalczak , Stephan Kohlstruk , Manfred Kreczinski , Gerda Grund , Rainer Lomoelder
IPC分类号： C07C263/06 , C07C265/14
CPC分类号： C07C263/04 , C07C269/04 , C07C2601/14 , C07C271/12 , C07C271/24 , C07C265/14
摘要： The invention relates to a multi-stage process for the continuous, phosgene-free preparation of (cyclo)aliphatic diisocyanates that comprises the conversion of (cyclo)aliphatic diamines into the corresponding (cyclo)alkylene biscarbamates and the thermal cleaving of the latter into the (cyclo)alkylene diisocyanates and alcohol. The urea used in accordance with the invention and also the urea employed for the preparation of urea equivalents (e.g. alkyl carbonates, alkyl carbamates) as a possible precursor for the synthesis of the (cyclo)aliphatic biscarbamates is unconditioned.
摘要翻译：本发明涉及用于（环）脂族二异氰酸酯的连续不光气制备的多阶段方法，其包括将（环）脂族二胺转化成相应的（环）亚烷基双氨基甲酸酯，并将后者的热裂解转化为（环）亚烷基二异氰酸酯和醇。根据本发明使用的尿素以及用于制备尿素当量（例如烷基碳酸酯，氨基甲酸烷基酯）作为合成（环）脂族双氨基甲酸酯的可能前体的尿素是无条件的。

38. 发明授权

US07557242B2 Multistage continuous preparation of cycloaliphatic disocyanates 失效
标题翻译：多级连续制备脂环族异氰酸酯
公开(公告)号：US07557242B2
公开(公告)日：2009-07-07
申请号：US11100603
申请日：2005-04-07
申请人： Stephan Kohlstruk , Manfred Kreczinski , Hans-Werner Michalczak
发明人： Stephan Kohlstruk , Manfred Kreczinski , Hans-Werner Michalczak
IPC分类号： C07C251/00
CPC分类号： C07C263/04 , C07C265/14
摘要： Cycloaliphatic diisocyanates can be prepared continuously and phosgene-free by reacting at least one cycloaliphatic diamine with at least one carbonic acid derivative and at least one alcohol to give a cycloaliphatic diurethane; freeing the cycloaliphatic diurethane of a low boiler, a medium boiler and mixtures thereof; thermally cleaving the cycloaliphatic diurethane in a cleavage apparatus to give a cycloaliphatic diisocyanate and a cleavage residue; continuously discharging a portion of the cleavage residue from the cleavage apparatus; removing the high boiler components from the discharge to obtain a purified discharge; reurethanizing the purified discharge with alcohol to obtain a reurethanized discharge; and recycling the reurethanized discharge into the process.
摘要翻译：环脂族二异氰酸酯可以通过使至少一种脂环族二胺与至少一种碳酸衍生物和至少一种醇反应而连续制备和无光气，得到脂环族二氨基甲酸酯; 释放低锅炉，中等锅炉及其混合物的脂环族二氨基甲酸酯; 在切割装置中热裂解脂环族二氨基甲酸酯以得到脂环族二异氰酸酯和裂解残基; 从裂解装置连续排出一部分裂解残基; 从放电中除去高锅炉组分以获得净化的排放物; 用乙醇对纯化的排出物进行氨基甲酸乙酯化，得到氨基甲酸酯化的排出物; 并将再生氨化的排放物回收到该过程中。

39. 发明申请

US20080045738A1 Method for the Production of Amines from Compounds Comprising Carbodiimide Groups, by Hydrolysis With Water 审中-公开
标题翻译：通过水解与碳二亚胺基组成的化合物生产胺的方法
公开(公告)号：US20080045738A1
公开(公告)日：2008-02-21
申请号：US10591975
申请日：2005-01-27
申请人： Matthias Orschel , Rainer Lomolder , Stephan Kohlstruk
发明人： Matthias Orschel , Rainer Lomolder , Stephan Kohlstruk
IPC分类号： C07C271/24 , C07C211/35
CPC分类号： C07C209/62 , Y02P20/127 , C07C211/00 , C07C211/35 , C07C211/36 , C07C211/50
摘要： The invention relates to a one-stage or multistage process for preparing mono-, di- and/or polyamines from compounds having carbodiimide groups and optionally also other groups of isocyanate chemistry by hydrolysis with water.
摘要翻译：本发明涉及从具有碳二亚胺基团的化合物制备单 - ，二 - 和/或多胺的单阶段或多步骤方法，并且任选地还可以通过用水解水解其它异氰酸酯化学基团。

40. 发明授权

US06924385B2 Method for synthesis of aliphatic isocyanates from aromatic isocyanates 失效
标题翻译：从芳族异氰酸酯合成脂族异氰酸酯的方法
公开(公告)号：US06924385B2
公开(公告)日：2005-08-02
申请号：US10331555
申请日：2002-12-31
申请人： Christian Lettmann , Stephan Kohlstruk , Guido Stochniol , Emmanouil Spyrou
发明人： Christian Lettmann , Stephan Kohlstruk , Guido Stochniol , Emmanouil Spyrou
IPC分类号： B01J23/46 , B01J35/04 , C07B61/00 , C07C263/04 , C07C263/16 , C07C265/10 , C07C265/14 , C07C263/02 , C07C209/10
CPC分类号： C07C263/04 , C07C265/10
摘要： The invention relates to a method for synthesis of aliphatic isocyanates from aromatic isocyanates in substantially 3 stages. In particular, the invention relates to a method for synthesis of bis{4-isocyanatocyclohexyl}methane (H12MDI) from bis{4-isocyanatophenyl}methane (MDI). More especially, the invention relates to a method for synthesis of H12MDI with a trans-trans isomer content of
摘要翻译：本发明涉及一种基本上由三个阶段合成芳族异氰酸酯的脂族异氰酸酯的方法。特别地，本发明涉及由双{4-异氰酸基苯基}甲烷（MDI）合成双{4-异氰酸根合环己基}甲烷（H 12 C 12 MDI）的方法。更具体地说，本发明涉及一种具有反式异构体含量<30％，优选<20％，特别优选5-15％的H 12 MDI的合成方法。

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