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31. 发明专利

JP2003212670A JOINED PRODUCT OF DIFFERENT KINDS OF MATERIALS AND ITS MANUFACTURING PROCESS 审中-公开
公开(公告)号：JP2003212670A
公开(公告)日：2003-07-30
申请号：JP2002017762
申请日：2002-01-25
申请人： NGK INSULATORS LTD
发明人： SHINKAI MASAYUKI , KIDA MASAHIRO , ISHIKAWA TAKAHIRO
IPC分类号： B23K1/19 , B23K1/20 , B23K20/02 , B23K35/00 , B23K35/30 , B32B15/04 , C04B35/581 , C04B37/02 , C22C5/02
摘要： PROBLEM TO BE SOLVED: To provide a joined product of different kinds of materials which effectively inhibits the increase in hardness of Au and enables its use at high temperature ranges, by establishing a barrier layer for inhibiting the dispersion of Ni into a precoat layer made of Au brazing filler metal and performing solid-phase joining between a ceramic base and a metallic member, and its manufacturing process. SOLUTION: In the joined product of different kinds of materials, the ceramic base 1 and the metallic member 7 are solid-phase joined via a brazing filler metal 5. An active metal 4 is placed on the surface of the ceramic base 1, and the Au-based brazing filler metal 5 is placed on the active metal 4. The active metal 4 and the brazing filler metal 5 are heated to form a precoat layer 6. The metallic member 7 is placed on the surface of the precoat layer 6 via a barrier layer 8, and the precoat layer 6 and the metallic member 7 are pressurized and heated to allow their solid-phase joining. COPYRIGHT: (C)2003,JPO

32. 发明专利

JP2002294357A METHOD FOR MANUFACTURING METAL-MATRIX COMPOSITE MATERIAL 失效
公开(公告)号：JP2002294357A
公开(公告)日：2002-10-09
申请号：JP2001101266
申请日：2001-03-30
申请人： NGK INSULATORS LTD
发明人： KIDA MASAHIRO
IPC分类号： B22D19/14 , C22C1/05 , C22C1/10 , C22C49/02 , C22C49/14 , C22C101/04 , C22C101/14 , C22C101/16 , C22C101/18
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a metal-matrix composite material which is applicable even to a large-sized final product having complicated shape and by which manufacturing steps can be reduced and simplified. SOLUTION: This method is a method for manufacturing a metal-matrix composite material consisting of a reinforcement and a matrix. The reinforcement, such as Al2 O3 and AlN, and an active metal powder of Ti, Nb, Zr, Ta or Hf are mixed to prepare a powder mixture. A jig having prescribed shape is filled with the powder mixture, and the powder mixture filled into the jig is impregnated with molten metal of Ag, Cu, Ag alloy, Cu alloy, etc.

33. 发明专利

JP2001217362A LAMINATED HEAT DISSIPATING MEMBER, POWER SEMICONDUCTOR DEVICE USING IT, AND METHOD OF PRODUCTION 失效
公开(公告)号：JP2001217362A
公开(公告)日：2001-08-10
申请号：JP2000023424
申请日：2000-01-31
申请人： NGK INSULATORS LTD
发明人： KIDA MASAHIRO , ISHIKAWA TAKAHIRO , ARAKI KIYOSHI , BESSHO HIROKI , MAKINO TAKUMA
IPC分类号： H01L23/373 , C04B37/02 , H01L23/36
摘要： PROBLEM TO BE SOLVED: To provide a laminated heat dissipating member comprising a bonded body of a metal based composite material and an insulating substrate imparted with a heat sink function excellent in heat dissipation properties and heat cycle characteristics in which cracking due to difference in the coefficient of thermal expansion between the insulating substrate, i.e., a heat dissipating plate, and the metal based composite material is substantially eliminated, a power semiconductor device comprising the laminated heat dissipating member and the laminated heat dissipating member, and a method for producing a power semiconductor device comprising the laminated heat dissipating member. SOLUTION: The laminated heat dissipating member comprising the bonded body of the metal based composite material and the insulating substrate imparted with a heat sink function is produced by a method comprising a step for treating the bonding surface of the insulating substrate previously in order to ensure wettability to a soldering material or a metal, as required, a step for mounting ceramic particles previously surface treated in order to ensure wettability to the soldering material or the metal on the insulating substrate, a step for placing the soldering material on the ceramic particles, and a step for producing the metal based composite material reacted on the soldering material by thermally fusing the soldering material to make it permeate into the gap between the ceramic particles and bonding the metal based composite material to the insulating substrate.

34. 发明专利

JP2001010873A METHOD FOR JOINING DIFFERENT KINDS OF MEMBERS TO EACH OTHER, AND COMPOSITE MEMBER JOINED BY THE SAME METHOD 失效
公开(公告)号：JP2001010873A
公开(公告)日：2001-01-16
申请号：JP18090299
申请日：1999-06-25
申请人： NGK INSULATORS LTD
发明人： ISHIKAWA TAKAHIRO , SHINKAI MASAYUKI , KIDA MASAHIRO
IPC分类号： B23K1/19 , B23K1/20 , B23K31/02 , B23K35/00 , B23K35/02 , B23K35/28 , B23K35/30 , B23K35/32 , B23K103/18 , C04B37/02
摘要： PROBLEM TO BE SOLVED: To provide a method for joining different kinds of members to each other to produce a composite member having a fit structure not having a space into which a prescribed amount of a hard brazing material can not be poured. SOLUTION: This method for producing a composite member which comprises different kinds of members and has a fit structure comprises uniformly spreading a particulate substance 4 on the surface of the depressed portion of a member 1 having the depressed portion, disposing a plate-like or powder-like hard brazing material 3 on the spread particulate substance 4 to cover at least its one part, and then fitting a member 2 having a projected portion, or spreading the particulate substance 4 on the depressed surface and then fitting a projected member having a layer comprising the hard brazing material formed thereon, and then heating the combination to melt and impregnate the hard brazing material into the particulate substance, thus forming the joining layer comprising the hard brazing material and the particulate material.

35. 发明专利

JP2011168472A Alumina sintered body, method for producing the same and semiconductor manufacturing apparatus member 有权
标题翻译：铝氧化物烧结体及其制造方法及半导体制造装置
公开(公告)号：JP2011168472A
公开(公告)日：2011-09-01
申请号：JP2010056466
申请日：2010-03-12
申请人： Ngk Insulators Ltd , 日本碍子株式会社
发明人： TERATANI NAOMI , HAYASE TORU , KATSUTA YUJI , KIDA MASAHIRO
IPC分类号： C04B35/111 , C04B35/645 , C04B41/88 , H01B3/12 , H01L21/683
CPC分类号： C04B35/111 , B32B18/00 , C04B35/645 , C04B2235/3206 , C04B2235/3208 , C04B2235/3217 , C04B2235/3222 , C04B2235/445 , C04B2235/5445 , C04B2235/656 , C04B2235/6567 , C04B2235/658 , C04B2235/6581 , C04B2235/77 , C04B2235/786 , C04B2235/80 , C04B2235/96 , C04B2235/963 , C04B2237/343
摘要： PROBLEM TO BE SOLVED: To sinter a molded body produced with general alumina powder at low temperature.
SOLUTION: The method for producing the alumina sintered body comprises: a step (a) molding a powdery mixture of Al
2 O
3 and MgF
2 or a powdery mixture of Al
2 O
3 , MgF
2 and MgO into a molded body with a prescribed shape; a step (b) of performing hot press-firing of the molded body in a vacuum atmosphere or a nonoxidizing atmosphere to obtain an alumina sintered body, wherein, when the amount of use of MgF
2 to 100 pts.wt. of Al
2 O
3 is X (pts.wt.) and hot press firing temperature is defined as Y(°C), the hot press firing temperature is set to satisfy the following equations (1) to (4): 1120≤Y≤1300 (1), 0.15≤X≤1.89 (2), Y≤-78.7X+1349 (3), and Y≥-200X+1212 (4).
COPYRIGHT: (C)2011,JPO&INPIT
摘要翻译：待解决的问题：在低温下烧结由一般氧化铝粉末制成的成型体。解决方案：制造氧化铝烧结体的方法包括：（a）将Al 2 SB 3 O 3 / SB 3的粉末混合物和MgF 2 / SB>或Al 2 至100重量份时 .wt。的比例为X（重量），热压烧成温度定义为Y（℃），将热压烧成温度设定为满足以下的式（1）〜（4）：1120≤Y≤1300（1），0.15≤X≤1.89（2），Y≤-78.7X + 1349（3），Y≥-200X + 1212（4）。版权所有（C）2011，JPO＆INPIT

36. 发明专利

JP2010064954A Sic/al-based composite material and method for producing the same 有权
标题翻译： SIC / AL系复合材料及其制造方法
公开(公告)号：JP2010064954A
公开(公告)日：2010-03-25
申请号：JP2009209725
申请日：2009-09-10
申请人： Ngk Insulators Ltd , 日本碍子株式会社
发明人： KIDA MASAHIRO , KATSUTA YUJI
IPC分类号： C04B35/565 , C22C1/10
摘要： PROBLEM TO BE SOLVED: To impregnate a metal in a short time even in the case of pressureless impregnation. SOLUTION: At first, a powdery mixture obtained by mixing titania (TiO 2 ) as an impregnation accelerating material and silicon carbide powder in such a manner that the grain size ratio of the impregnation accelerating material to the silicon carbide reaches ≤1/10 and the volume ratio of the impregnation accelerating material to the silicon carbide reaches ≥0.15 is produced, and the powdery mixture is formed into a preform. The preform is charged to a carbon crucible, and, in a state where an Al alloy ingot is placed on the preform, heating is performed to 1,200°C in a vacuum atmosphere, thus the Al alloy is impregnated into the preform so as to be an impregnated body. Thereafter, the impregnated body is gradually cooled so as to obtain an SiC/Al based composite material. COPYRIGHT: (C)2010,JPO&INPIT
摘要翻译：要解决的问题：即使在无压浸渍的情况下也能在短时间内浸渍金属。解决方案：首先，通过将二氧化钛（TiO 2 / SB> 2 ）作为浸渍促进材料和碳化硅粉末混合而获得的粉末混合物，使得浸渍加速材料的晶粒尺寸比碳化硅达到≤1/ 10，并且产生浸渍加速材料与碳化硅的体积比达到≥0.15，并将粉末混合物形成预成型体。将预成型体装入碳坩埚中，在将Al合金锭放置在预制件上的状态下，在真空气氛中进行1200℃的加热，将Al合金浸渍到预成型体中浸渍体。然后，将浸渍体逐渐冷却，得到SiC / Al系复合材料。版权所有（C）2010，JPO＆INPIT

37. 发明专利

JP2005023331A Method of producing composite material, and composite material 审中-公开
标题翻译：生产复合材料的方法和复合材料
公开(公告)号：JP2005023331A
公开(公告)日：2005-01-27
申请号：JP2003143946
申请日：2003-05-21
申请人： Ngk Insulators Ltd , 日本碍子株式会社
发明人： IKEMATSU TAKATOSHI , KIDA MASAHIRO , ISHIKAWA TAKAHIRO
IPC分类号： B22D19/00 , B22D19/14 , C22C1/10 , C22C21/00
摘要： PROBLEM TO BE SOLVED: To provide a method capable of producing a composite material having a high denseness at a low production cost in a short and simple process without needing high temperature or high pressure. SOLUTION: In the method of producing the composite material, aluminum molten metal is impregnated into mixed materials 2a and 2b comprising prescribed metal powder and reinforcing material, so that a composite material 5 is obtained. The mixed material 2a is filled into the internal space 1a of a reaction vessel 1 as a first compact 12 compacted so that the volume ratio of the metal powder/the reinforcing material and porosity satisfy prescribed relation. Further, the mixed material 2b is filled so as to fill a part of the internal spaces of the impregnation holes 8a in a cover body 8 as a second compact 14 compacted so that the volume ratio of the metal powder/the reinforcing material and porosity satisfy prescribed relation and also the volume ratio of the metal powder/the reinforcing material reaches the value equal to or below that in the first compact 12. Thereafter, aluminum molten metal is impregnated through the impregnation holes 8a of the cover body 8. COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：要解决的问题：提供一种能够在短而简单的工艺中以低生产成本生产具有高致密度的复合材料的方法，而不需要高温或高压。解决方案：在制造复合材料的方法中，将铝熔融金属浸渍到包含规定的金属粉末和增强材料的混合材料2a和2b中，从而获得复合材料5。将混合材料2a填充到作为压实的第一压块12的反应容器1的内部空间1a中，使得金属粉末/增强材料的体积比和孔隙率满足规定的关系。此外，填充混合材料2b，以填充作为压实的第二压块14的盖体8中的浸渍孔8a的内部空间的一部分，使得金属粉末/增强材料的体积比和孔隙率满足规定关系，并且金属粉末/增强材料的体积比达到等于或低于第一压块12中的值。此后，铝熔融金属通过盖体8的浸渍孔8a浸渍。版权所有（C）2005，JPO＆NCIPI

38. 发明专利

JP2004346368A Method for manufacturing composite material, and composite material 审中-公开
标题翻译：制备复合材料的方法和复合材料
公开(公告)号：JP2004346368A
公开(公告)日：2004-12-09
申请号：JP2003144081
申请日：2003-05-21
申请人： Ngk Insulators Ltd , 日本碍子株式会社
发明人： KIDA MASAHIRO , IKEMATSU TAKATOSHI , ISHIKAWA TAKAHIRO
IPC分类号： B22D19/00 , B22D19/14 , B22D21/02 , B22D21/06 , C22C1/10 , C22C21/00
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a composite material by which a composite material having high denseness and heat resistance (high-temperature strength) can be manufactured at a low cost and low energy by a shortened and simplified manufacturing process while dispensing with high-temperature/high-pressure conditions .
SOLUTION: In the method for manufacturing the composite material, a mixed material 2 containing prescribed metal powder 3 and reinforcement 15 is impregnated with molten aluminum to obtain the composite material 5. An internal space 1a of a reaction vessel 1 is filled with the mixed material 2 in the form of a compact prepared by performing compaction so that a volume ratio (X) between the metal powder and the reinforcement and a porosity (ε) satisfy a prescribed relation. Then the molten aluminum is impregnated via an impregnation hole 8a of a cover body 8.
COPYRIGHT: (C)2005,JPO&NCIPI
摘要翻译：解决的问题：提供一种复合材料的制造方法，通过该复合材料的制造，可以通过缩短和简化的制造以低成本和低能量制造具有高致密度和耐热性（高温强度）的复合材料同时分配高温/高压条件。解决方案：在复合材料的制造方法中，将含有规定金属粉末3和增强材料15的混合材料2浸渍有熔融铝，得到复合材料5.反应容器1的内部空间1a填充有通过进行压实制备的压块形式的混合材料2使得金属粉末和增强材料之间的体积比（X）和孔隙率（ε）满足规定的关系。然后，通过盖体8的浸渍孔8a浸渍熔融铝。版权所有（C）2005，JPO＆NCIPI

39. 发明专利

JP2004332056A Composite material, and its production method 审中-公开
公开(公告)号：JP2004332056A
公开(公告)日：2004-11-25
申请号：JP2003130676
申请日：2003-05-08
申请人： Ngk Insulators Ltd , 日本碍子株式会社
发明人： KIDA MASAHIRO , ISHIKAWA TAKAHIRO , IKEMATSU TAKATOSHI
IPC分类号： C22C1/10 , C22C47/08 , C22C49/12 , C22C101/04 , C22C101/14
摘要： PROBLEM TO BE SOLVED: To provide a composite material having a dense microstructure in spite of its large/complicated shape, and provided with excellent physical properties such as high fracture toughness and easiness in working. SOLUTION: The composite material 5 contains a composite structure in which a dispersion material is dispersed into a matrix comprising an aluminide intermetallic compound as a constituent. A first composite structure 12 (first structure 13) in which a first dispersion material 37 is dispersed into a first matrix 36 comprising a first aluminide intermetallic compound, and a structure (second structure 14) of the material same as or different from that of the first composite structure 12 composed of at least one kind selected from the group consisting of a second composite structure 15 in which a second dispersion material is dispersed into a second matrix comprising a second aluminide intermetallic compound, a metallic structure 16 and a ceramic structure 17 are coexistent in a state of being mutually partitioned/held in each existing region. COPYRIGHT: (C)2005,JPO&NCIPI

40. 发明专利

JP2004156058A Method for manufacturing composite material, and composite material manufactured by the method 有权
公开(公告)号：JP2004156058A
公开(公告)日：2004-06-03
申请号：JP2002319787
申请日：2002-11-01
申请人： Naoyuki Kanetake , Makoto Kobashi , Ngk Insulators Ltd , 眞小橋 , 日本碍子株式会社 , 直幸金武
发明人： KANETAKE NAOYUKI , KOBASHI MAKOTO , ISHIKAWA TAKAHIRO , KIDA MASAHIRO
IPC分类号： B22D19/00 , C22C1/10 , C22C29/16 , C22C32/00
摘要： PROBLEM TO BE SOLVED: To provide a method for manufacturing a composite material, which can easily adjust the percentage of each material content, particularly a metallic aluminum content, in an obtaining composite material, without needing a special external heating means and device, at a lower energy expenditure as well as being industrially easy and inexpensive, and to provide the composite material manufactured by the method.
SOLUTION: The method for manufacturing the composite material comprises filling a predetermined vessel with a mixed powder obtained by mixing a nitride powder with a boron nitride powder to form a green compact having a porous structure, and impregnating the green compact with an Al molten metal to form a composite material including metal boride and having a matrix consisting of aluminum nitride, wherein the green compact is formed by compacting the mixed powder having a mixed ratio of the nitride powder with the boron nitride powder in a range of 1 to 1.8 to 1 to 2.2 (by mole ratio) so that the porosity of the green compact can be 35 to 70%.
COPYRIGHT: (C)2004,JPO

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