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31. 发明专利

JP2006321804A BENZENE DERIVATIVE AND LIQUID CRYSTAL MEDIUM 审中-公开
公开(公告)号：JP2006321804A
公开(公告)日：2006-11-30
申请号：JP2006184904
申请日：2006-07-04
申请人： MERCK PATENT GMBH
发明人： TARUMI KAZUAKI , BARTMANN EKKEHARD , REIFFENRATH VOLKER , SCHOEN SABINE , PAULUTH DETLEF , SCHULER BRIGITTE , POETSCH EIKE
IPC分类号： C07C25/18 , G02F1/13 , C07C17/26 , C07C25/24 , C07C43/225 , C07C69/76 , C07C323/01 , C09K19/08 , C09K19/12 , C09K19/30 , C09K19/34 , C09K19/42 , C09K19/44
摘要： PROBLEM TO BE SOLVED: To obtain a medium for MLC, TN or STN display and has especially high specific resistance and low threshold voltage. SOLUTION: The liquid crystal medium composed of a mixture of a polar compound having positive dielectric anisotropy as a base material comprises one or more kinds of compounds represented by general formula I. COPYRIGHT: (C)2007,JPO&INPIT

32. 发明专利

JP2003286208A Method for producing cyclic compound 有权
标题翻译：生产环化合物的方法
公开(公告)号：JP2003286208A
公开(公告)日：2003-10-10
申请号：JP2003069260
申请日：2003-03-14
申请人： Merck Patent Gmbh , メルクパテントゲゼルシャフトミットベシュレンクテルハフトング
发明人： PAULUTH DETLEF , KIRSCH PEER , BAEUERLE PETER , DEEG OLIVER
IPC分类号： C07D211/08 , C07B61/00 , C07C17/093 , C07C17/26 , C07C17/263 , C07C17/392 , C07C25/18 , C07C25/22 , C07C25/24 , C07C41/30 , C07C41/40 , C07C43/225 , C07C331/28 , C07F5/02 , C07F7/08 , C09K19/12 , C09K19/14 , C09K19/16 , C09K19/18 , C09K19/32 , C09K19/40
CPC分类号： C07C17/093 , C07C17/263 , C07C25/18 , C07C25/22 , C07C25/24 , C07C331/28 , C07F5/025 , C07F7/082 , C09K19/12 , C09K19/14 , C09K19/16 , C09K19/18 , C09K19/32 , C09K19/404 , C09K2019/124
摘要： PROBLEM TO BE SOLVED: To provide a method for synthesizing a cyclic compound with which the product can be obtained in a higher yield and a high level of conversion can be achieved in a smaller number of reactional steps than those of a conventional technique and to develop a combinatorial synthetic strategy. SOLUTION: The method for producing the cyclic compound comprises combinatorial synthesis based on the Suzuki coupling, subsequent halo- demetalation and the final Suzuki coupling. The Suzuki couplings are carried out by using boronic acid or a boronic acid ester, respectively. The corresponding cyclic compound and a new synthetic unit used therefor are provided. The cyclic compound is preferably used as a component of a liquid crystal mixture. COPYRIGHT: (C)2004,JPO
摘要翻译：待解决的问题：提供一种合成可以以比常规技术更少的数量的反应步骤来实现以更高的产率和高转化率获得产物的环状化合物的方法并制定组合合成策略。解决方案：制备环状化合物的方法包括基于Suzuki偶联，随后的卤代脱甲基和最终Suzuki偶联的组合合成。铃木耦合分别通过使用硼酸或硼酸酯进行。提供相应的环状化合物和用于其的新的合成单元。环状化合物优选用作液晶混合物的成分。版权所有（C）2004，JPO

33. 发明专利

JP2003096003A FLUORINATED (DIHYDRO)PHENANTHRENE DERIVATIVES, AND THEIR USE IN LIQUID-CRYSTALLINE MEDIUM 审中-公开
公开(公告)号：JP2003096003A
公开(公告)日：2003-04-03
申请号：JP2002166852
申请日：2002-06-07
申请人： MERCK PATENT GMBH
发明人： BREMER MATTHIAS , PAULUTH DETLEF , HECKMEIER MICHAEL , DUBAL HANS-ROLF DR , HORNUNG BARBARA , SCHMIDT WOLFGANG DR , WINGEN RAINER
IPC分类号： G02F1/13 , C07C13/573 , C07C15/30 , C07C17/361 , C07C25/22 , C07C25/24 , C07C43/225 , C07C45/00 , C07C255/50 , C07C255/54 , C07C331/28 , C09K19/32 , C09K19/42
摘要： PROBLEM TO BE SOLVED: To provide a medium having large positive dielectric anisotropy, broad nematic phase, relatively low double refraction factor, very high resistivi ty, good UV and thermal stability and low vapor pressure as a matrix liquid crystal display. SOLUTION: Liquid-crystalline (dihydro)phenanthrene derivatives shown by formula (I) (wherein, R is an alkyl or alkenyl group unsubstituted or substituted by CN, CF3 or a halogen; A is a 1,4-cyclohexenylene, 1,4- cyclohexylene or 1,4-phenylene group; Z is -CO-O-, -O-CO-, -CF2 O-, OCF2 -, CH2 O- or the like; Y is H, F, Cl, CN, SF5 , NCS, SCN or a halogenated alkyl, alkenyl, alkenyloxy or alkoxy group; G is -CH2 CH2 -, -CH=CF- or -CH=CH-; and L , L , L , L and L are each H or F) are provided.

34. 发明专利

JP2002069452A CRYSTAL MEDIUM 有权
公开(公告)号：JP2002069452A
公开(公告)日：2002-03-08
申请号：JP2001203241
申请日：2001-07-04
申请人： MERCK PATENT GMBH
发明人： HECKMEIER MICHAEL , SCHOEN SABINE , PAULUTH DETLEF , TARUMI KAZUAKI
IPC分类号： G02F1/13 , C09K19/30 , C09K19/34 , C09K19/42 , C09K19/44
摘要： PROBLEM TO BE SOLVED: To provide a crystal medium having high specific resistance and low threshold voltage and specifically suitable for MLC, TN or STN display. SOLUTION: This crystal medium includes as a base material a polar compound mixture having positive dielectric anisotropy and contains a compound represented by general formula I, a compound represented by general formula IIA, and/or compound represented by general formula IIB [Wherein, R is H or a 1-15C alkyl, alkoxy, alkenyl or alkenyloxy groups; R', R", R" are each 1-10C alkyl or alkoxy groups or 2-10 alkenyl group; Y is F, Cl or a 1-5C haloalkyl group; one CH2 of the haloalkyl group may be substituted with -O- or -CH=CH-; L is H or F].

35. 发明专利

JP2002020750A LIQUID CRYSTALLINE MEDIUM AND ELECTRO-OPTICAL LIQUID CRYSTAL DISPLAY CONTAINING THE SAME MEDIUM 失效
公开(公告)号：JP2002020750A
公开(公告)日：2002-01-23
申请号：JP2001156742
申请日：2001-05-25
申请人： MERCK PATENT GMBH
发明人： HECKMEIER MICHAEL , KIRSCH PEER , BREMER MATTHIAS , PAULUTH DETLEF , SCHOEN SABINE
IPC分类号： G02F1/13 , C09K19/12 , C09K19/14 , C09K19/20 , C09K19/30 , C09K19/34 , C09K19/42
摘要： PROBLEM TO BE SOLVED: To provide a liquid crystalline medium having a low crystallizing tendency at a low temperature, a low birefringence, a suitable electric resistance, in addition, a low threshold electric voltage (V10) and a low rotation viscosity (γ1) which is decisive to a response time, and a liquid crystal display by using the same medium. SOLUTION: This liquid crystalline medium having a positive dielectric anisotropy is provided by incorporating a mesogenic compound of the general formula 1 (wherein, R1 is a 1-7C alkyl or alkoxy, or a 2-7C alkenyl, alkenyloxy or alkoxyalkyl; Z1 is CF2-CF2, CF2O, CHL-CHL, trans CH=CH, trans CF=CH, trans CH=CF or trans CF=CF; and X1 is F, Cl, CF3, OCF3, OCF2H, CN or NCS).

36. 发明申请

WO2012069133A8 COMPOUNDS FOR A LIQUID CRYSTAL MEDIUM, AND THE USE THEREOF FOR HIGH-FREQUENCY COMPONENTS 审中-公开
标题翻译：液晶介质的化合物及其用于高频成分的研究
公开(公告)号：WO2012069133A8
公开(公告)日：2012-08-23
申请号：PCT/EP2011005502
申请日：2011-10-31
申请人： MERCK PATENT GMBH , JASPER CHRISTIAN , MANABE ATSUTAKA , PAULUTH DETLEF , REIFFENRATH VOLKER
发明人： JASPER CHRISTIAN , MANABE ATSUTAKA , PAULUTH DETLEF , REIFFENRATH VOLKER
IPC分类号： C09K19/18 , C09K19/34 , C09K19/42
CPC分类号： C09K19/18 , C09K19/3405 , C09K19/3455 , C09K19/3458 , C09K19/3491 , C09K19/42 , C09K2019/0459 , C09K2019/3009 , C09K2019/301 , C09K2019/3021 , C09K2019/3037 , C09K2219/11
摘要： The invention relates to compounds with at least one fluorinated C-C double bond between two rings, to the use thereof for high-frequency components, to liquid crystal media containing the compounds, and to high-frequency components containing said media, in particular antennas, especially for the gigahertz range. The liquid crystal media are used for example for phase-shifting microwaves for tunable phased-array antennas.
摘要翻译：本发明涉及一种具有两个环之间含有该化合物的液晶介质含有高频率成分，特别是天线，特别是对千兆赫范围这些介质的至少一种氟化的C-C双键，其对高频分量的使用，和化合物。液晶介质例如用于可调谐“相控阵”天线的相移微波。

37. 发明申请

WO2011066905A8 COMPONENTS FOR HIGH FREQUENCY TECHNOLOGY, LIQUID CRYSTAL MEDIA AND COMPOUNDS 审中-公开
标题翻译：高频技术，液晶介质和连接的组件
公开(公告)号：WO2011066905A8
公开(公告)日：2011-08-04
申请号：PCT/EP2010006961
申请日：2010-11-16
申请人： MERCK PATENT GMBH , MANABE ATSUTATA , JASPER CHRISTIAN , REIFFENRATH VOLKER , MONTENEGRO ELVIRA , PAULUTH DETLEF
发明人： MANABE ATSUTATA , JASPER CHRISTIAN , REIFFENRATH VOLKER , MONTENEGRO ELVIRA , PAULUTH DETLEF
IPC分类号： C09K19/12
CPC分类号： C09K19/52 , C07C1/321 , C07C15/14 , C07C2531/24 , C09K19/12 , C09K2019/523 , C09K2219/11 , H01Q19/02
摘要： The invention relates to a component for high frequency technology, or for the microwave range and millimetre wave range of the electromagnetic spectrum, characterised in that it contains a liquid crystal medium, which consists of one or more compounds containing 6 to 15 five-, six- or seven-membered rings, preferably 1,4-linked phenylene rings, or in that it contains a liquid crystal medium which itself contains a component A, which in turn consists of one or more of said compounds containing 6 to 15 five-, six- or seven-membered rings, preferably 1,4-linked phenylene rings. The present invention also relates to compounds of formula (I), wherein the parameters have the meanings given in the text, and also to the corresponding novel liquid crystal media, to the use and production thereof, and also to the production and use of the components. The components according to the invention are suitable in particular as phase shifters in the microwave and millimetre wave range, for microwave and millimetre wave array antennas and most particularly for so-called tunable "reflectarrays".
摘要翻译：本发明涉及一种用于高频技术的组件，或用于微波范围内，和在电磁谱的毫米波范围内，其特征在于它含有由一种或多种化合物，其是一种或多种化合物，的6〜15的五元的液晶介质中，六元或七元环，优选1,4-连接的亚苯基环含有，或者它包含一个液晶介质，其又包含的分量的，这反过来又由一个或多个的所述含有含6至一种或多种化合物的化合物存在15个五元，六元或七元环，优选含有1,4-连接的亚苯基环。本发明还涉及式（I）的化合物，其中参数具有本文给出的含义，以及相应的新型液晶介质，它们的用途和制备以及组分的制备和用途。根据本发明的组件特别适用于微波和毫米波范围内的移相器，微波和毫米波阵列天线以及非常特别适用于所谓的可调谐反射阵列。

38. 发明申请

WO02081418A2 2,4'-SUBSTITUTED 6-CYCLOHEXYL-TRANS-DECALINES 审中-公开
标题翻译： 2,4'-取代的6-环己基TRANS-DEKA LINE
公开(公告)号：WO02081418A2
公开(公告)日：2002-10-17
申请号：PCT/EP0203228
申请日：2002-03-22
申请人： MERCK PATENT GMBH , BREMER MATTHIAS , PAULUTH DETLEF , LUESSEM GEORG
发明人： BREMER MATTHIAS , PAULUTH DETLEF , LUESSEM GEORG
IPC分类号： G02F1/13 , C07C17/00 , C07C17/35 , C07C17/354 , C07C22/00 , C07C22/08 , C07C43/192 , C07C45/51 , C07C47/347 , C09K19/32 , C09K19/42
CPC分类号： C09K19/322 , C07C17/00 , C07C17/35 , C07C17/354 , C07C22/08 , C07C45/515 , C07C47/347 , C09K2019/326 , Y10T428/10
摘要： The invention relates to 2,4'-substituted 6-cyclohexyl-trans-decalines of general formula (I) wherein R1, R2 and Z have the designations cited in claim 1. The invention also relates to the use of the same as constituents of liquid crystal media, and a liquid crystal and electro-optical display element.
摘要翻译：本发明涉及2,4'-二取代的通式（I）其中R1，R2和Z具有权利要求1中给出的含义，6-环己基 - 反式 - 十氢化萘和它们作为液晶介质的组分和液晶和电光学显示元件中使用，

39. 发明申请

WO2015024635A8 ALKINYL-TOLANES, LIQUID-CRYSTAL MIXTURES CONTAINING THEM AND COMPONENTS FOR HIGH-FREQUENCY TECHNOLOGY 审中-公开
标题翻译：炔基二苯乙炔，包含高频技术液晶化合物和组分
公开(公告)号：WO2015024635A8
公开(公告)日：2016-03-17
申请号：PCT/EP2014002194
申请日：2014-08-11
申请人： MERCK PATENT GMBH
发明人： JASPER CHRISTIAN , BROCKE CONSTANZE , PAULUTH DETLEF , REIFFENRATH VOLKER , MANABE ATSUTAKA
IPC分类号： C09K19/18 , C09K19/32 , C09K19/34
CPC分类号： C09K19/3059 , C07C15/18 , C07C15/24 , C07C25/24 , C09K19/18 , C09K19/32 , C09K19/322 , C09K19/3405 , C09K19/3491 , C09K2019/181 , C09K2219/11
摘要： The present invention relates to the compounds of formula I, wherein the parameters have the respective meanings given in the description, to the use thereof for high-frequency components, liquid-crystal media containing the compounds, and high-frequency components containing said media, in particular antennas, specifically for the gigahertz range. The liquid-crystal media are used for example to shift the phase of microwaves for tunable phased-array antennas.
摘要翻译：本发明涉及式I的化合物，其中所述参数具有各自的，在说明书中给出，其对高频分量的使用，含有这些化合物和含有高频率成分，特别是天线，特别是对千兆赫范围这些介质的液晶介质。该液晶介质被用于例如微波的可调谐“相控阵天线的相移。

40. 发明申请

WO2011035863A8 COMPONENTS FOR HIGH-FREQUENCY TECHNOLOGY AND LIQUID CRYSTAL MEDIA 审中-公开
标题翻译：组件高频技术和液晶MEDIA
公开(公告)号：WO2011035863A8
公开(公告)日：2011-06-03
申请号：PCT/EP2010005640
申请日：2010-09-14
申请人： MERCK PATENT GMBH , MANABE ATSUTAKA , GOEBEL MARK , KLASS DAGMAR , MONTENEGRO ELVIRA , PAULUTH DETLEF
发明人： MANABE ATSUTAKA , GOEBEL MARK , KLASS DAGMAR , MONTENEGRO ELVIRA , PAULUTH DETLEF
IPC分类号： C09K19/18 , C09K19/30
CPC分类号： C09K19/18 , C09K19/30 , C09K19/3001 , C09K2019/186 , C09K2019/188 , C09K2219/11 , G02B27/0087 , G02F1/292
摘要： The present invention relates to a component for high-frequency technology or for the microwave range and millimeter wave range of the electromagnetic spectrum, characterized in that the component contains a liquid crystal compound of the formula I, wherein the parameters have the respective meanings given in the claims or in the text, or a liquid crystal medium, which in turn contains one or more compounds of said formula I, and the corresponding, novel liquid crystal media, the use and the production thereof, and the production and the use of the components. The components according to the invention are suitable in particular as phase shifters in the microwave range and in the millimeter wave range, for microwave and millimeter wave array antennas, and especially for so-called adaptable "reflectarrays".
摘要翻译：本发明涉及一种用于高频技术的组件，或用于微波范围内，和在电磁谱的毫米波范围内，其特征在于它是下式的液晶化合物，其中所述参数已经在权利要求中或在文本相应的含义给出，或液晶介质包括，反过来，包含此式I的一种或多种化合物，以及对应的新的液晶介质，其用途和制造，以及制备和使用该组件的。本发明的组分特别适合作为微波和毫米波的移相器，用于微波和毫米波阵列天线，特别是用于所谓的可调谐“反射阵列”。

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