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31. 发明申请

US20050272920A1 Yellow disperse dye mixture which has a high level of light fastness 有权
标题翻译：具有高耐光性的黄色分散染料混合物
公开(公告)号：US20050272920A1
公开(公告)日：2005-12-08
申请号：US10523656
申请日：2003-08-02
申请人： Toshio Hihara , Hiroshi Inoue , Wataru Seto
发明人： Toshio Hihara , Hiroshi Inoue , Wataru Seto
IPC分类号： C09B67/22 , D06P1/16 , D06P1/18 , D06P1/20 , D06P3/54 , D06P3/82
CPC分类号： D06P1/18 , C09B67/0041 , D06P1/16 , D06P1/20 , D06P3/54 , Y10S8/922
摘要： The present inventions refers to a dye mixture comprising from 25 to 80% by weight with respect to the total dyestuff fraction of the yellow dyestuff represented by the structural formula [1] and from 75 to 20% by weight with respect to the total dyestuff fraction of a yellow dyestuff represented by the structural formula [2] wherein R denotes a C1 to C4 hydroxyalkyl group.
摘要翻译：本发明是指相对于由结构式[1]表示的黄色染料的总染料份数和相对于总染料份数为75〜20重量％的25〜80重量％的染料混合物的由结构式[2]表示的黄色染料，其中R表示C 1至C 4羟烷基。

32. 发明授权

US06388057B1 Crystalline modification of a water-insoluble monoazo dye 失效
标题翻译：水不溶性单偶氮染料的结晶改性
公开(公告)号：US06388057B1
公开(公告)日：2002-05-14
申请号：US09869672
申请日：2001-08-31
申请人： Toshio Hihara , Hiroshi Inoue , Yousuke Takahashi
发明人： Toshio Hihara , Hiroshi Inoue , Yousuke Takahashi
IPC分类号： C09B6748
CPC分类号： C09B67/0015 , C09B67/0029 , Y10S8/922
摘要： A water-insoluble monoazo dye represented by the following structural formula [I] having a crystal modification characterized by an X-ray diffraction pattern (CuK&agr;) showing one strong peak at a diffraction angle (2&thgr;) of 11.1±0.1° and also four intermediate peaks at 8.1±0.1°, 21.8±0.1°, 23.1±0.1° and 25.2±0.1°.
摘要翻译：具有以衍射角（2θ）为11.1±0.1°的一个强峰的X射线衍射图（CuKalpha）为特征的结晶改性的下述结构式[I]表示的水不溶性单偶氮染料，以及四个中间体峰位于8.1±0.1°，21.8±0.1°，23.1±0.1°和25.2±0.1°。

33. 发明授权

US5545236A Red reactive dyes, their compositions and dyeing method employing them 失效
标题翻译：红色活性染料，它们的组成和使用它们的染色方法
公开(公告)号：US5545236A
公开(公告)日：1996-08-13
申请号：US400934
申请日：1995-03-09
申请人： Toshio Hihara , Yousuke Takahashi
发明人： Toshio Hihara , Yousuke Takahashi
IPC分类号： C09B62/51 , D06P1/38 , C09B67/22
CPC分类号： C09B62/51
摘要： A red reactive dye having the following formula (I) in its free acid form: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --C.sub.2 H.sub.4 W (wherein W is a group splittable by alkali), A is a C.sub.2-3 alkylene group or a C.sub.2-3 alkylenoxy C.sub.2-3 alkylene group, E is a hydrogen atom, a C.sub.1-3 alkyl group or --A--SO.sub.2 X (wherein A and X are as defined above), n is 0 or 1, l is 1 or 2, m is 0 or 1, and R is a hydrogen atom, --OH, --CN, --CH.sub.3, --CF.sub.3, --SO.sub.3 H, --COOH, --CH.sub.2 SO.sub.3 H or --CH.sub.2 SO.sub.2 X (wherein X is as defined above), provided that a compound of the formula (I) wherein R is a hydrogen atom, each of m and n is 0, l is 1, and --SO.sub.2 X is --SO.sub.2 CH.dbd.CH.sub.2 which is bonded at the ortho position to the azo group, is excluded.
摘要翻译：具有游离酸形式的具有下式（I）的红色活性染料：其中X是-CH = CH 2或-C 2 H 4 W（其中W是可被碱可裂的基团），A是C2-3 亚烷基或C2-3亚烷基氧基C2-3亚烷基，E是氢原子，C1-3烷基或-A-SO2X（其中A和X如上定义），n是0或1，l是 1或2，m为0或1，R为氢原子，-OH，-CN，-CH 3，-CF 3，-SO 3 H，-COOH，-CH 2 SO 3 H或-CH 2 SO 2 X（其中X如上定义）其中R为氢原子的式（I）化合物，m和n各自为0,1或2，-SO 2 X为与偶氮基的邻位键合的-SO 2 CH = CH 2。。

34. 发明授权

US4500710A Quinophthalone dyes for cellulose-containing fibers 失效
标题翻译：喹诺酮染料用于含纤维素的纤维
公开(公告)号：US4500710A
公开(公告)日：1985-02-19
申请号：US505127
申请日：1983-06-16
申请人： Toshio Niwa , Toshio Hihara
发明人： Toshio Niwa , Toshio Hihara
IPC分类号： C09B62/04 , C07D401/10 , C07D401/14
CPC分类号： C09B62/046
摘要： Quinophthalone dyes for cellulose-containing fibers represented by the following general formula: ##STR1## wherein X represents a hydrogen atom, a chlorine atom or a bromine atom, --A-- represents a methylene group, an ethylene group, a propylene group or a 1,3-butylene group, n represents 0 or 1, --Y-- represents a linkage group of --O-- or --S--, R.sup.1 and R.sup.2 each represents a hydrogen atom, an alkyl or alkenyl group which may optionally be substituted with a cyano group, a hydroxy group, a lower alkoxy group or by a dialkylamino group, or R.sup.1 and R.sup.2 may be combined together with the adjacent nitrogen atom to form a 5- or 6-membered, nitrogen-containing heterocyclic ring having the total carbon atom number in R.sup.1 and R.sup.2 of up to 18.
摘要翻译：由以下通式表示的含纤维素纤维的喹诺酮染料：其中X表示氢原子，氯原子或溴原子，-A-表示亚甲基，亚乙基，亚丙基或1 ，3-亚丁基，n表示0或1，-Y-表示-O-或-S-的连接基团，R 1和R 2各自表示氢原子，可任选被氰基取代的烷基或烯基基团，羟基，低级烷氧基或二烷基氨基，或者R 1和R 2可以与相邻的氮原子一起形成含有总碳原子数的5-或6-元含氮杂环 R1和R2最多可达18个。

35. 发明授权

US4473499A Reactive disazo dyes containing an oxy fluoro triazine group for cellulose containing fibers 失效
标题翻译：含有含氟三嗪基的含有纤维素的纤维的活性双偶氮染料
公开(公告)号：US4473499A
公开(公告)日：1984-09-25
申请号：US400201
申请日：1982-07-20
申请人： Toshio Niwa , Toshio Hihara
发明人： Toshio Niwa , Toshio Hihara
IPC分类号： C09B62/09 , D06P1/382 , D06P3/60 , C09B62/03 , D06P3/66
CPC分类号： C09B62/09 , D06P1/382 , D06P3/6041
摘要： Reactive disazo dyes for dyeing cellulose-containing fibers, represented by the general formula (I): ##STR1## wherein ##STR2## is a phenyl group which may be substituted; Y.sup.1 is a phenyl group which may be substituted; Y.sup.2 is an allyl group, a benzyl group, or an alkyl group which may be substituted; ##STR3## is a phenyl group which may be substituted; and ##STR4## is a phenyl group which may be substituted, ##STR5## is a naphthylene group, or a phenylene group which may be substituted, ##STR6## is a phenylene group which may be substituted, and R.sup.1 and R.sup.2 are each a hydrogen atom, an alkyl group which may be substituted by a cyano group, a hydroxy group, a lower alkoxy group, or a dialkylamino group, or may combine together in combination with N to form a 5- or 6- membered nitrogen-containing heterocyclic ring, the total number of carbon atoms of R.sup.1 and R.sup.2 being 18 or less.
摘要翻译：用于染色含纤维素纤维的反应性双偶氮染料，由通式（I）表示：其中其中是可被取代的苯基; Y1是可被取代的苯基; Y2是烯丙基，苄基或可被取代的烷基; 是可以被取代的苯基; ＆lt; IMAGE＆gt;是可被取代的苯基，＆lt; IMAGE＆gt;是可以被取代的亚萘基或亚苯基，可以被取代的亚苯基，R 1和R 2各自为氢原子，可以被氰基，羟基，低级烷氧基或二烷基氨基取代的烷基，或者可以与N一起结合在一起形成5-或6-元含氮杂环，R1和R2的碳原子总数为18以下。

36. 发明授权

US07824451B2 Disperse dye mixtures which have a high degree of light fastness 有权
标题翻译：具有高耐光性的分散染料混合物
公开(公告)号：US07824451B2
公开(公告)日：2010-11-02
申请号：US10563198
申请日：2004-06-29
申请人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
发明人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
IPC分类号： D06P3/82
CPC分类号： C09B5/62 , C09B67/0038 , D06P3/54 , Y10S8/92 , Y10S8/922
摘要： The present invention provides a blue dye mixture which contains the pigments represented by formulae [1], [2], [3], and [4] The present invention also relates to dye mixtures in which there are compounded therewith a yellow dye mixture and/or a red dye mixture. The invention further relates to a method of dyeing polyester-based fibers and dyed polyester-based fibers and dyed polyester-based fiber materials.
摘要翻译：本发明提供了含有由式[1]，[2]，[3]和[4]表示的颜料的蓝色染料混合物。本发明还涉及其中与其混合黄色染料混合物的染料混合物， /或红色染料混合物。本发明还涉及一种染色涤纶基纤维和染色的聚酯基纤维和染色的聚酯基纤维材料的方法。

37. 发明申请

US20060230549A1 Disperse dye mixtures which have a high degree of light fastness 有权
标题翻译：具有高耐光性的分散染料混合物
公开(公告)号：US20060230549A1
公开(公告)日：2006-10-19
申请号：US10563198
申请日：2004-06-29
申请人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
发明人： Toshio Hihara , Wataru Seto , Koichi Fujisaki , Daisuke Hosoda , Hiroshi Inoue
IPC分类号： D06P3/82
CPC分类号： C09B5/62 , C09B67/0038 , D06P3/54 , Y10S8/92 , Y10S8/922
摘要： The present invention provides a blue dye mixture which contains the pigments represented by formulae [1], [2], [3], and [4] The present invention also relates to dye mixtures in which there are compounded therewith a yellow dye mixture and/or a red dye mixture. The invention further relates to a method of dyeing polyester-based fibers and dyed polyester-based fibers and dyed polyester-based fiber materials.
摘要翻译：本发明提供了含有由式[1]，[2]，[3]和[4]表示的颜料的蓝色染料混合物。本发明还涉及其中与其混合黄色染料混合物的染料混合物， /或红色染料混合物。本发明还涉及一种染色涤纶基纤维和染色的聚酯基纤维和染色的聚酯基纤维材料的方法。

38. 发明授权

US5756690A Red reactive dyes, their compositions and dyeing method employing them 失效
公开(公告)号：US5756690A
公开(公告)日：1998-05-26
申请号：US639332
申请日：1996-04-25
申请人： Toshio Hihara , Yousuke Takahashi
发明人： Toshio Hihara , Yousuke Takahashi
IPC分类号： C09B62/51 , C09B62/507
CPC分类号： C09B62/51
摘要： A red reactive dye having the following formula (I) in its free acid form: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --C.sub.2 H.sub.4 W (wherein W is a group splittable by alkali), A is a C.sub.2-3 alkylene group or a C.sub.2-3 alkylenoxy C.sub.2-3 alkylene group, E is a hydrogen atom, a C.sub.1-3 alkyl group or --A--SO.sub.2 X (wherein A and X are as defined above), n is 0 or 1, l is 1 or 2, m is 0 or 1, and R is a hydrogen atom, --OH, --CN, --CH.sub.3, --CF.sub.3, --SO.sub.3 H, --COOH, --CH.sub.2 SO.sub.3 H or --CH.sub.2 SO.sub.2 X (wherein X is as defined above), provided that a compound of the formula (I) wherein R is a hydrogen atom, each of m and n is 0, l is 1, and --SO.sub.2 X is --SO.sub.2 CH.dbd.CH.sub.2 which is bonded at the ortho position to the azo group, is excluded.

39. 发明授权

US4960871A Fiber-reactive halotriazine pyridine-based monoazo colorant 失效
标题翻译：纤维反应性卤代三嗪吡啶类单偶氮染料
公开(公告)号：US4960871A
公开(公告)日：1990-10-02
申请号：US313316
申请日：1989-02-17
申请人： Toshio Hihara , Yukiharu Shimizu
发明人： Toshio Hihara , Yukiharu Shimizu
IPC分类号： C09B62/085 , D06P1/382 , D06P3/66 , D06P3/82 , D06P3/85
CPC分类号： C09B62/085 , D06P1/382 , D06P3/8228
摘要： Monoazo colorants represented by the general formula (I): ##STR1## wherein: D represents ##STR2## (wherein X represents a hydrogen atom or a halogen atom, and Y represents a nitro group, a lower alkylsulfonyl group, a thiocyanic acid group or a halogen atom), or ##STR3## (wherein P represents a nitro group or a lower alkylsulfonyl group, and Q and T each represents a hydrogen atom, a halogen atom or a cyano group);R.sup.1 and R.sup.2 each represents an ethylene group or a propylene group;R.sup.3 and R.sup.4 each represents a hydrogen atom or an alkyl group which may be substituted by a lower alkoxy group or a lower alkoxyalkoxy group; andZ represents a halogen atom.This monoazo colorants include a reactive type pyridine-based monoazo dye suitable for use in dyeing of cellulose or cellulose/polyester mixed fibers in red to orange.
摘要翻译：（I）表示的单偶氮着色剂：其中：D表示（其中X表示氢原子或卤素原子，Y表示硝基，低级烷基磺酰基，硫氰酸酯酸基或卤素原子）或（其中P表示硝基或低级烷基磺酰基，Q和T各自表示氢原子，卤素原子或氰基）。 R1和R2各自表示亚乙基或亚丙基; R3和R4各自表示氢原子或可被低级烷氧基或低级烷氧基烷氧基取代的烷基; Z表示卤素原子。该单偶氮着色剂包括适用于染色红色至橙色的纤维素或纤维素/聚酯混合纤维的反应型吡啶类单偶氮染料。

40. 发明授权

US4888028A Water-soluble blue dye mixture and dyeing method: anthraquinone reactive dye and formazan reactive dye 失效
标题翻译：水溶性蓝色染料混合物和染色方法：蒽醌活性染料和甲an活性染料
公开(公告)号：US4888028A
公开(公告)日：1989-12-19
申请号：US206727
申请日：1988-06-15
申请人： Toshio Hihara , Riyouichi Sekioka
发明人： Toshio Hihara , Riyouichi Sekioka
IPC分类号： C09B67/22
CPC分类号： C09B67/004 , Y10S8/917 , Y10S8/918 , Y10S8/924
摘要： A water-soluble dye mixture comprising a blue anthraquinone reactive dye represented in its free acid form by the formula: ##STR1## wherein X is --CH.dbd.CH.sub.2 or --C.sub.2 H.sub.4 W wherein W is a group removable by action of alkali and from 0.2 to 5 times by weight to said anthraquinone reactive dye of a blue formazan reactive dye represented in its free acid form by the formula: ##STR2## wherein R is a hydrogen atom or a C.sub.1 -C.sub.4 alkyl group, Y is a halogen atom, --NHC.sub.2 H.sub.4 SO.sub.3 H or ##STR3## and X is --CH.dbd.CH.sub.2 or --C.sub.2 H.sub.4 W wherein W is a group removable by action of alkali.

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