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31. 发明授权

US08048956B2 Functionalized polyfluorenes for use in optoelectronic devices 有权
标题翻译：用于光电器件的功能化聚芴
公开(公告)号：US08048956B2
公开(公告)日：2011-11-01
申请号：US12328797
申请日：2008-12-05
申请人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
发明人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
IPC分类号： C08G61/00 , C08L65/00 , H01L33/00
CPC分类号： C08F130/04
摘要： The present invention relates to process comprising reacting a polyfluorenes comprising at least one structural group of formula I with an iridium (III) compound of formula II The invention also relates to the polyfluorenes, which are products of the reaction, and the use of the polyfluorenes in optoelectronic devices.
摘要翻译：本发明涉及使包含至少一种式I结构基团的聚芴与式II的铱（III）化合物反应的方法。本发明还涉及作为反应产物的聚芴和聚芴的用途在光电器件中。

32. 发明申请

US20090156783A1 EMISSIVE POLYMERIC MATERIALS FOR OPTOELECTRONIC DEVICES 有权
标题翻译：用于光电器件的EMISSIVE聚合材料
公开(公告)号：US20090156783A1
公开(公告)日：2009-06-18
申请号：US11957579
申请日：2007-12-17
申请人： Joseph John Shiang , Kelly Scott Chichak , James Anthony Cella , Larry Neil Lewis , Kevin Henry Janora
发明人： Joseph John Shiang , Kelly Scott Chichak , James Anthony Cella , Larry Neil Lewis , Kevin Henry Janora
IPC分类号： C08G73/00
CPC分类号： C08G61/12 , C08G2261/142 , C08G2261/1526 , C08G2261/3142 , C08G2261/3162 , H01L51/0039 , H01L51/5012 , Y10S428/917
摘要： Polymers including at least one structural unit derived from a compound of formula I or including at least one pendant group of formula II may be used in optoelectronic devices wherein R1, R3, R4 and R6 are independently hydrogen, alkyl, alkoxy, oxaalkyl, alkylaryl, aryl, arylalkyl, heteroaryl, substituted alkyl; substituted alkoxy, substituted oxaalkyl, substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted heteroaryl; R1a is hydrogen or alkyl; R2 is alkylene, substituted alkylene, oxaalkylene, CO, or CO2; R2a is alkylene; R5 is independently at each occurrence hydrogen, alkyl, alkylaryl, aryl, arylalkyl, alkoxy, carboxy, substituted alkyl; substituted alkylaryl, substituted aryl, substituted arylalkyl, or substituted alkoxy, X is halo, triflate, —B(OR1a)2, or located at the 2, 5- or 2, 7-positions; and L is derived from phenylpyridine, tolylpyridine, benzothienylpyridine, phenylisoquinoline, dibenzoquinozaline, fluorenylpyridine, ketopyrrole, 2-(1-naphthyl)benzoxazole)), 2-phenylbenzoxazole, 2-phenylbenzothiazole, coumarin, thienylpyridine, phenylpyridine, benzothienylpyridine, 3-methoxy-2-phenylpyridine, thienylpyridine, phenylimine, vinylpyridine, pyridylnaphthalene, pyridylpyrrole, pyridylimidazole, phenylindole, derivatives thereof or combinations thereof.
摘要翻译：包括至少一种衍生自式I化合物或包含至少一个式II侧基的结构单元的聚合物可用于其中R 1，R 3，R 4和R 6独立地为氢，烷基，烷氧基，氧杂烷基，烷芳基，芳基，芳基烷基，杂芳基，取代的烷基; 取代的烷氧基，取代的氧杂烷基，取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的杂芳基; R1a是氢或烷基; R2是亚烷基，取代的亚烷基，氧杂亚烷基，CO或CO 2; R2a是亚烷基; R5各自独立地为氢，烷基，烷基芳基，芳基，芳基烷基，烷氧基，羧基，取代的烷基; 取代的烷基芳基，取代的芳基，取代的芳基烷基或取代的烷氧基，X是卤素，三氟甲磺酸酯，-B（OR1a）2，或位于2,5-或2,7-位; 苯基吡啶，苯并噻吩并吡啶，二苯并喹嗪，芴基吡啶，酮吡咯，2-（1-萘基）苯并恶唑）），2-苯基苯并恶唑，2-苯基苯并噻唑，香豆素，噻吩基吡啶，苯基吡啶，苯并噻吩基吡啶，3-甲氧基 - 2-苯基吡啶，噻吩基吡啶，苯基亚胺，乙烯基吡啶，吡啶基萘，吡啶基吡咯，吡啶基咪唑，苯基吲哚，其衍生物或其组合。

33. 发明申请

US20080027028A1 Ketopyrroles useful as ligands in organic iridium compositions 有权
标题翻译：可用作有机铱组合物中配体的酮塔吡咯
公开(公告)号：US20080027028A1
公开(公告)日：2008-01-31
申请号：US11504084
申请日：2006-08-14
申请人： Kelly Scott Chichak
发明人： Kelly Scott Chichak
IPC分类号： A61K31/695 , C07F7/02
CPC分类号： H01L51/0085 , A61K31/695 , C07F7/1804 , H01L51/0035 , H01L51/42 , H01L51/5012 , Y02E10/549
摘要： The present invention provides novel ketopyrroles having structure XXIV wherein R2 is independently at each occurrence a deuterium atom, a halogen, a nitro group, an amino group, a C3-C40 aromatic radical, a C1-C50 aliphatic radical, or a C3-C40 cyclcoaliphatic radical; “a” is an integer from 0 to 3; and X1 and X2 are independently at each occurrence a bromine atom, a hydroxy group, or the group OR10, and wherein the group R10 is independently at each occurrence a deuterium atom, a halogen, a nitro group, an amino group, a C3-C40 aromatic radical, a C1-C50 aliphatic radical, or a C3-C40 cyclcoaliphatic radical. Ketopyrroles XXIV are useful ligands for the preparation of Type (1) and Type (2) organic iridium compositions. In one aspect, the present invention provides deuterated analogs of XXIV. Organic iridium compositions are useful in the preparation optoelectronic devices, such as OLED devices and photovoltaic devices exhibiting enhanced performance characteristics.
摘要翻译：本发明提供具有结构ⅩⅩⅣ的新型酮吡咯，其中R 2 2在每次出现时独立地为氘原子，卤素，硝基，氨基，C 3 - C 40芳族基团，C 1 -C 50脂族基团或C 3 -C 30亚烷基 > 40脂环族基团; “a”是从0到3的整数; 并且X 1和X 2各自在每次出现时独立地为溴原子，羟基或OR 10，并且其中基团 R 10在每次出现时独立地为氘原子，卤素，硝基，氨基，C 3 -C 40芳族自由基，C 1 -C 50脂肪族基团或C 3 -C 40脂环族基团。酮基吡咯二酮XXIV是制备类型（1）和类型（2）有机铱组合物的有用配体。一方面，本发明提供了XXIV的氘代类似物。有机铱组合物可用于制备光电子器件，例如具有增强的性能特征的OLED器件和光伏器件。

34. 发明申请

US20080026496A1 Method of making organic light emitting devices 有权
标题翻译：制造有机发光装置的方法
公开(公告)号：US20080026496A1
公开(公告)日：2008-01-31
申请号：US11637582
申请日：2006-12-12
申请人： Joseph John Shiang , Kevin Henry Janora , Gautam Parthasarathy , James Anthony Cella , Kelly Scott Chichak
发明人： Joseph John Shiang , Kevin Henry Janora , Gautam Parthasarathy , James Anthony Cella , Kelly Scott Chichak
IPC分类号： H01L21/00 , H01L29/08
CPC分类号： H01L51/0043 , H01L51/0003 , H01L51/0035 , H01L51/0039 , H01L51/005 , H01L51/0085 , H01L51/56 , Y10T428/31511
摘要： The present invention provides a method for the preparation of organic light-emitting devices comprising a bilayer structure made by forming a first film layer comprising an electroactive material and an INP precursor material, and exposing the first film layer to a radiation source under an inert atmosphere to generate an interpenetrating network polymer composition comprising the electroactive material. At least one additional layer is disposed on the reacted first film layer to complete the bilayer structure. The bilayer structure is comprised within an organic light-emitting device comprising standard features such as electrodes and optionally one or more additional layers serving as a bipolar emission layer, a hole injection layer, an electron injection layer, an electron transport layer, a hole transport layer, exciton-hole transporting layer, exciton-electron transporting layer, a hole transporting emission layer, or an electron transporting emission layer.
摘要翻译：本发明提供一种制备有机发光器件的方法，其包括通过形成包含电活性材料和INP前体材料的第一膜层制备的双层结构，并在惰性气氛下将第一膜层暴露于辐射源以产生包含电活性材料的互穿网络聚合物组合物。在反应的第一膜层上设置至少一个附加层以完成双层结构。双层结构包括在包括标准特征的有机发光器件中，例如电极和可选地用作双极型发射层的一个或多个附加层，空穴注入层，电子注入层，电子传输层，空穴传输层，激子 - 空穴传输层，激子 - 电子传输层，空穴传输发射层或电子传输发射层。

35. 发明授权

US08053536B2 Functionalized polyfluorenes for use in optoelectronic devices 有权
标题翻译：用于光电器件的功能化聚芴
公开(公告)号：US08053536B2
公开(公告)日：2011-11-08
申请号：US12328805
申请日：2008-12-05
申请人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
发明人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
IPC分类号： C08G61/00 , C08L65/00 , H01L33/00
CPC分类号： C08G61/02 , C08G2261/1412 , C08G2261/1424 , C08G2261/143 , C08G2261/148 , C08G2261/1526 , C08G2261/5242 , C08G2261/95 , C09K11/06 , C09K2211/185 , H01L51/0039 , H01L51/0085 , H05B33/14
摘要： The present invention relates to process comprising reacting a polyfluorenes comprising at least one structural group of formula I with an iridium (III) compound of formula II wherein R1 and R2 are independently alkyl, substituted alkyl, aryl, substituted aryl or a combination thereof; R5is H or CHO; R3 and R4 are independently hydrogen, alkyl, substituted alkyl, aryl, substituted aryl or a combination thereof; R11 and R12 taken together form a substituted or unsubstituted monocyclic or bicyclic heteroaromatic ring; R13 is independently at each occurrence halo, nitro, hydroxy, amino, alkyl, aryl, arylalkyl, alkoxy, substituted alkoxy, substituted alkyl, substituted aryl, or substituted arylalkyl; Ar is aryl, heteroaryl, substituted aryl, substituted heteroaryl, or a combination thereof; X is selected from a direct bond, alky, substituted alkyl, and combinations thereof; Y is CHO or NH2; Z is CHO or NH2 where Z does not equal Y; and p is 0, 1 or 2. The invention also relates to the polyfluorenes, which are products of the reaction, and the use of the polyfluorenes in optoelectronic devices.
摘要翻译：本发明涉及包括使包含至少一个式I结构基团的聚芴与式II的铱（III）化合物反应的方法，其中R 1和R 2独立地为烷基，取代的烷基，芳基，取代的芳基或其组合; R5is H或CHO; R3和R4独立地是氢，烷基，取代的烷基，芳基，取代的芳基或其组合; R11和R12一起形成取代或未取代的单环或双环杂芳环; R13各自独立地为卤素，硝基，羟基，氨基，烷基，芳基，芳基烷基，烷氧基，取代的烷氧基，取代的烷基，取代的芳基或取代的芳基烷基; Ar是芳基，杂芳基，取代的芳基，取代的杂芳基或其组合; X选自直接键，烷基，取代的烷基及其组合; Y为CHO或NH2; Z是CHO或NH2，其中Z不等于Y; 并且p为0,1或2.本发明还涉及作为反应产物的聚芴以及聚芴在光电器件中的应用。

36. 发明申请

US20100156278A1 ORGANIC METAL COMPLEXES FOR USE IN OPTOELECTRONIC DEVICES 审中-公开
标题翻译：用于光电器件的有机金属复合物
公开(公告)号：US20100156278A1
公开(公告)日：2010-06-24
申请号：US12342604
申请日：2008-12-23
申请人： Kelly Scott Chichak , Brian Christopher Bales , Kyle Erik Litz
发明人： Kelly Scott Chichak , Brian Christopher Bales , Kyle Erik Litz
IPC分类号： H01J1/63 , C07F15/00 , C09K11/06
CPC分类号： C07F15/0033 , C07F15/0073 , C07F15/0086
摘要： The invention provides an organic metal complex represented by the formula (I), wherein M is a metal selected from Rh, Ir, or Pt; Y represents N or O; R1 represents a hydrogen, a halogen, a nitro group, an amino group, a hydroxyl group, a C3-C40 aromatic radical, a C1-C50 aliphatic radical, and a C3-C50 cycloaliphatic radical; R2 represents a hydrogen, C3-C20 aromatic radical, C1-C50 aliphatic radical, or a C3-C50 cycloaliphatic radical; or R1 and R2, together with the adjacent Y, may form a ring, preferably a 5- or 6-membered ring; n1 has a value of from 0 to 3; and n2 has a value of 0 to 2; m1 has a value of at least 1; and m2 has a value of at least 1 provided that m1+m2 is 3.
摘要翻译：本发明提供由式（I）表示的有机金属络合物，其中M为选自Rh，Ir或Pt的金属; Y表示N或O; R1表示氢，卤素，硝基，氨基，羟基，C3-C40芳族基，C1-C50脂族基和C3-C50脂环族基; R 2表示氢，C 3 -C 20芳族基，C 1 -C 50脂族基或C 3 -C 50脂环族基; 或R 1和R 2与相邻的Y一起可以形成环，优选5-或6-元环; n1的值为0〜3; n2的值为0〜2; m1的值至少为1; 如果m1 + m2为3，则m2的值至少为1。

37. 发明授权

US07608677B2 Method for preparing polymeric organic iridium compositions 有权
标题翻译：聚合有机铱组合物的制备方法
公开(公告)号：US07608677B2
公开(公告)日：2009-10-27
申请号：US11599972
申请日：2006-11-15
申请人： James Anthony Cella , Kelly Scott Chichak
发明人： James Anthony Cella , Kelly Scott Chichak
IPC分类号： C08G64/00 , C08G63/02
CPC分类号： C07F15/0033 , C07B2200/11 , H01L51/0035 , H01L51/0085 , H01L51/5012 , Y10S428/917
摘要： The present invention provides a method for the preparation of polymeric organic iridium complexes useful in electronic devices such as OLEDs. The method provides polymeric organic iridium compositions comprising at least one cyclometallated ligand and at least one ketopyrrole ligand. The polymeric organic iridium compositions provided are referred to as Type (2) organic iridium compositions and are constituted such that at least one ligand of the polymeric organic iridium compound has a number average molecular weight of 2,000 grams per mole or greater (as measured by gel permeation chromatography). Type (2) organic iridium compositions are referred to herein as comprising “polymeric organic iridium complexes”. In one embodiment, the method comprises providing a non-polymeric organic iridium complex comprising one or more reactive functional groups and carrying out a polymerization step to provide the polymeric organic iridium complex comprising at least one cyclometallated ligand and at least one ketopyrrole ligand.
摘要翻译：本发明提供了制备用于诸如OLED的电子器件中的聚合有机铱络合物的方法。该方法提供包含至少一种环金属配体和至少一种酮吡咯配体的聚合有机铱组合物。提供的聚合有机铱组合物称为类型（2）有机铱组合物，并且构成为使得至少一种高分子有机铱化合物的配位体的数均分子量为每摩尔或更大2000克（通过凝胶测量）渗透色谱）。类型（2）有机铱组合物在本文中被称为包含“聚合有机铱络合物”。在一个实施方案中，该方法包括提供包含一个或多个反应性官能团的非聚合有机铱络合物，并进行聚合步骤以提供包含至少一种环金属配体和至少一种酮吡咯配体的聚合有机铱络合物。

38. 发明授权

US09711748B2 OLED devices with internal outcoupling 有权
公开(公告)号：US09711748B2
公开(公告)日：2017-07-18
申请号：US13599477
申请日：2012-08-30
申请人： Kelly Scott Chichak , Jie Jerry Liu , Joseph John Shiang , Arunkumar Natarajan , Christian Maria Anton Heller
发明人： Kelly Scott Chichak , Jie Jerry Liu , Joseph John Shiang , Arunkumar Natarajan , Christian Maria Anton Heller
IPC分类号： H01L51/54 , C07D401/14 , H01L51/50 , H01L51/52 , H01L51/00
CPC分类号： H01L51/5072 , H01L51/0067 , H01L51/5088 , H01L51/5268 , H01L2251/5369
摘要： Optoelectronic devices with enhanced internal outcoupling include a substrate, an anode, a cathode, an electroluminescent layer, and electron transporting layer comprising a fluoro compound of formula I (Ar2)n—Ar1—(Ar2)n I wherein Ar1 is C5-C40 aryl, C5-C40 substituted aryl, C5-C40 heteroaryl, or C5-C40 substituted heteroaryl; Ar2 is, independently at each occurrence, fluoro- or fluoroalkyl-substituted C5-40 heteroaryl; and n is 1, 2, or 3.

39. 发明申请

US20140061591A1 OLED DEVICES WITH INTERNAL OUTCOUPLING 有权
标题翻译：具有内部输出的OLED器件
公开(公告)号：US20140061591A1
公开(公告)日：2014-03-06
申请号：US13599477
申请日：2012-08-30
申请人： Kelly Scott Chichak , Jie Jerry Liu , Joseph John Shiang , Arunkumar Natarajan , Christian Maria Anton Heller
发明人： Kelly Scott Chichak , Jie Jerry Liu , Joseph John Shiang , Arunkumar Natarajan , Christian Maria Anton Heller
IPC分类号： H01L51/54 , C07D401/14
CPC分类号： H01L51/5072 , H01L51/0067 , H01L51/5088 , H01L51/5268 , H01L2251/5369
摘要： Optoelectronic devices with enhanced internal outcoupling include a substrate, an anode, a cathode, an electroluminescent layer, and electron transporting layer comprising a fluoro compound of formula I (Ar2)n—Ar1—(Ar2)n I wherein Ar1 is C5-C40 aryl, C5-C40 substituted aryl, C5-C40 heteroaryl, or C5-C40 substituted heteroaryl; Ar2 is, independently at each occurrence, fluoro- or fluoroalkyl-substituted C5-40 heteroaryl; and n is 1, 2, or 3.
摘要翻译：具有增强的内部输出耦合的光电子器件包括基底，阳极，阴极，电致发光层和包含式I（Ar2）n -Ar1-（Ar2）nI的氟化合物的电子传输层，其中Ar 1是C 5 -C 40芳基， C5-C40取代的芳基，C5-C40杂芳基或C5-C40取代的杂芳基; Ar2在每次出现时独立地为氟代或氟烷基取代的C 5-40杂芳基; 且n为1,2或3。

40. 发明申请

US20100144992A1 FUNCTIONALIZED POLYFLUORENES FOR USE IN OPTOELECTRONIC DEVICES 有权
标题翻译：用于光电器件的功能化聚偏氟乙烯
公开(公告)号：US20100144992A1
公开(公告)日：2010-06-10
申请号：US12328797
申请日：2008-12-05
申请人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
发明人： Kelly Scott Chichak , Larry Neil Lewis , James Anthony Cella , Joseph John Shiang
IPC分类号： C08F130/04
CPC分类号： C08F130/04
摘要： The present invention relates to process comprising reacting a polyfluorenes comprising at least one structural group of formula I with an iridium (III) compound of formula II The invention also relates to the polyfluorenes, which are products of the reaction, and the use of the polyfluorenes in optoelectronic devices.
摘要翻译：本发明涉及使包含至少一种式I结构基团的聚芴与式II的铱（III）化合物反应的方法。本发明还涉及作为反应产物的聚芴和聚芴的用途在光电器件中。

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