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31. 发明授权

US08449655B2 Process for isolating N2O 有权
标题翻译： N2O分离方法
公开(公告)号：US08449655B2
公开(公告)日：2013-05-28
申请号：US12518659
申请日：2007-12-07
申请人： Dieter Baumann , Beatrice Roessler , Joaquim Henrique Teles
发明人： Dieter Baumann , Beatrice Roessler , Joaquim Henrique Teles
IPC分类号： B01D53/14
CPC分类号： C01B21/22 , B01D53/1406 , B01D53/1418 , B01D53/77 , B01D2257/402 , Y02C20/10 , Y02P20/153
摘要： The present invention relates to a process for purifying a gas mixture G-0 comprising dinitrogen monoxide, at least comprising the contacting of the gas mixture G-0 with a solvent mixture (I) at least comprising 50% by weight of water based on the overall solvent mixture (I), the pH of the solvent mixture (I) being in the range from 3.5 to 8.0, the desorption of a gas mixture G-1 from a composition (A), the contacting of the gas mixture G-1 with a solvent mixture (II) at least comprising 50% by weight of water based on the overall solvent mixture (II), the pH of the solvent mixture (II) being in the range from 2.0 to 8.0, and the desorption of a gas mixture G-2 from a composition (B), the pH being based in each case on a measurement with a glass electrode, and to the use of gas mixtures obtainable by a process according to the invention as oxidizing agents for olefins.
摘要翻译：本发明涉及一种纯化包含一氧化二氮的气体混合物G-0的方法，该方法至少包括气体混合物G-0与至少包含50重量％水的溶剂混合物（I）的接触，基于总溶剂混合物（I），溶剂混合物（I）的pH范围为3.5-8.0，气体混合物G-1从组合物（A）中的解吸，气体混合物G-1 基于总溶剂混合物（II），溶剂混合物（II）至少包含50重量％的水，溶剂混合物（II）的pH在2.0至8.0的范围内，并且气体的解吸来自组合物（B）的混合物G-2，在每种情况下，使用玻璃电极进行测量，并且使用可通过根据本发明的方法获得的气体混合物作为烯烃的氧化剂。

32. 发明授权

US08404901B2 Process for purifying dinitrogen monoxide 有权
标题翻译：纯化一氧化二氮的方法
公开(公告)号：US08404901B2
公开(公告)日：2013-03-26
申请号：US12936331
申请日：2009-03-13
申请人： Joaquim Henrique Teles , Dieter Baumann , Beatrice Röβler-Feigel
发明人： Joaquim Henrique Teles , Dieter Baumann , Beatrice Röβler-Feigel
IPC分类号： C07C45/00 , C07C43/00 , F25J3/08
CPC分类号： C01B21/22 , C01B2210/0045 , C01B2210/0062 , C07C45/28 , C07C49/607
摘要： The present invention relates to a process for purifying a gas mixture comprising dinitrogen monoxide, at least comprising the at least partial condensation of a gas mixture G-I comprising dinitrogen monoxide to obtain a liquid composition C-1 comprising dinitrogen monoxide, and the contacting of the composition C-1 with a gas mixture M-1 to obtain a composition C-2 and a gas mixture M-2.
摘要翻译：本发明涉及一种纯化包含一氧化二氮的气体混合物的方法，至少包括包含一氧化二氮的气体混合物GI的至少部分缩合，以获得包含一氧化二氮的液体组合物C-1，以及组合物 C-1与气体混合物M-1混合以获得组合物C-2和气体混合物M-2。

33. 发明申请

US20120108780A1 METHOD FOR PRODUCING POLYOLS ON THE BASIS OF RENEWABLE RESOURCES 审中-公开
标题翻译：基于可再生资源生产多元醇的方法
公开(公告)号：US20120108780A1
公开(公告)日：2012-05-03
申请号：US13382991
申请日：2010-07-09
申请人： Andreas Kunst , Michael Schelper , Joaquim Henrique Teles , Berend Eling , Jenny Reuber , Gerd-Dieter Tebben
发明人： Andreas Kunst , Michael Schelper , Joaquim Henrique Teles , Berend Eling , Jenny Reuber , Gerd-Dieter Tebben
IPC分类号： C08G18/28 , C07C43/11 , C07C41/03
CPC分类号： C08G18/4866 , C08G18/4891 , C08G65/2609 , C08G65/2615 , C08G65/2663 , C08G2101/0008 , C08G2101/0025 , C08G2190/00 , C08G2410/00
摘要： A method for producing a polyol, the method including:(a) reacting at least one selected from the group consisting of an unsaturated natural fat, an unsaturated natural fatty acid, and a fatty acid ester with dinitrogen monoxide, to obtain a first intermediate;(b) reacting the first intermediate with a hydrogenation reagent, to obtain a second intermediate;(c) reacting the second intermediate with at least one alkylene oxide, to obtain a polyol.
摘要翻译：一种制备多元醇的方法，该方法包括：（a）使选自不饱和天然脂肪，不饱和天然脂肪酸和脂肪酸酯与一氧化二氮的至少一种反应，得到第一中间体; （b）使第一中间体与氢化试剂反应，得到第二中间体; （c）使第二中间体与至少一种烯化氧反应，得到多元醇。

34. 发明授权

US08119550B2 Process for epoxidation and catalyst to be used therein 有权
标题翻译：环氧化方法和催化剂用于其中
公开(公告)号：US08119550B2
公开(公告)日：2012-02-21
申请号：US10526939
申请日：2003-09-16
申请人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Goebbel , Peter Rudolf , Joaquim Henrique Teles
发明人： Ulrich Mueller , Georg Krug , Peter Bassler , Hans-Georg Goebbel , Peter Rudolf , Joaquim Henrique Teles
IPC分类号： B01J29/06 , C07D301/19
CPC分类号： C07D301/19 , B01J29/89 , B01J37/10 , B01J2229/36 , B01J2229/40 , C07D301/12 , Y02P20/125
摘要： The present invention relates to a process for treating a solid material containing at least one zeolite and being at least partly crystalline or treating a shaped body obtained from said solid material wherein said solid material or shaped body is brought in contact with a composition containing water after at least one of the following steps of an integrated process for producing a solid material or a shaped body containing at least one zeolite: (i) after step (II) of separating the at least partly crystalline solid material from its mother liquor or (ii) after step (S) of shaping said solid material into a shaped body or (iii) after a step (C) of calcining said solid material or said shaped body. The present invention furthermore relates to the solid material obtainable by the inventive process and the shaped body obtainable by the inventive process. The present invention also relates to the use of the solid material or the shaped body as mentioned above as a catalyst in chemical reactions, in particular in reactions of compounds containing at least one C-C double bond with at least one hydroperoxide.
摘要翻译：本发明涉及一种用于处理含有至少一种沸石并且至少部分结晶的固体材料或处理由所述固体材料获得的成形体的方法，其中所述固体材料或成形体与含有水的组合物接触用于生产固体材料或含有至少一种沸石的成形体的整合方法中的至少一个步骤：（i）在从母液中分离出至少部分结晶固体材料的步骤（II）之后，或（ii ）在将所述固体材料成形为成形体的步骤（S）之后或（iii）在煅烧所述固体材料或所述成形体的步骤（C）之后。本发明还涉及可通过本发明方法获得的固体材料和通过本发明方法获得的成形体。本发明还涉及如上所述的固体材料或成形体作为化学反应中的催化剂，特别是在含有至少一个C-C双键的化合物与至少一种氢过氧化物的反应中的用途。

35. 发明申请

US20110218323A1 PROCESS FOR PREPARING CYCLIC DIAMINES 失效
标题翻译：制备循环泵的方法
公开(公告)号：US20110218323A1
公开(公告)日：2011-09-08
申请号：US13128508
申请日：2009-11-06
申请人： Kirsten Dahmen , Martin Ernst , Michael Limbach , Johann-Peter Melder , Beatrice Rössler-Feigel , Joaquim Henrique Teles
发明人： Kirsten Dahmen , Martin Ernst , Michael Limbach , Johann-Peter Melder , Beatrice Rössler-Feigel , Joaquim Henrique Teles
IPC分类号： C08G69/00 , C07C209/48 , C07C211/35 , C08G71/04
CPC分类号： C07C209/48 , C07C209/16 , C07C209/26 , C07C253/30 , C07C2601/14 , C07C211/36 , C07C255/46
摘要： The present invention relates to a process for preparing a cyclic diamine, comprising the reaction of at least one cyclic alkene with a gas mixture (G) comprising dinitrogen the subsequent conversion of monoxide to give at least one cyclic ketone and then converting the at least one cyclic ketone to a cyclic diamine. The invention also relates to the use of a cyclic diamine with primary and secondary amine functions thus obtained to prepare polyamides and polyurethanes.
摘要翻译：本发明涉及一种制备环状二胺的方法，其包括使至少一种环烯与包含二氮的气体混合物（G）的反应，随后将一氧化碳转化成至少一种环酮，然后将至少一种环酮到环状二胺。本发明还涉及具有如此获得的伯胺和仲胺官能团的环状二胺的用途，以制备聚酰胺和聚氨酯。

36. 发明授权

US07973183B2 Process for the preparation of an olefin oxide 有权
标题翻译：制备烯烃氧化物的方法
公开(公告)号：US07973183B2
公开(公告)日：2011-07-05
申请号：US12599395
申请日：2008-04-24
申请人： Hans-Georg Goebbel , Peter Bassler , Joaquim Henrique Teles , Peter Rudolf , Ulrich Mueller , Anna Forlin , Malte Schulz , Meinolf Weidenbach
发明人： Hans-Georg Goebbel , Peter Bassler , Joaquim Henrique Teles , Peter Rudolf , Ulrich Mueller , Anna Forlin , Malte Schulz , Meinolf Weidenbach
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/584
摘要： The present invention relates to a continuous process for the preparation of an olefin oxide wherein an olefin is reacted with a hydroperoxidein the presence of a catalyst, and wherein the reaction which is carried out in at least three reactors operated in parallel is controlled by specifically adjusting the catalyst loads in the reactors.
摘要翻译：本发明涉及一种用于制备烯烃氧化物的连续方法，其中烯烃在催化剂存在下与氢过氧化物反应，并且其中在至少三个并联操作的反应器中进行的反应通过特别调节来控制反应器中的催化剂负载。

37. 发明授权

US07608728B2 Method for producing propylene oxide 有权
标题翻译：生产环氧丙烷的方法
公开(公告)号：US07608728B2
公开(公告)日：2009-10-27
申请号：US10555961
申请日：2004-05-10
申请人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
发明人： Ulrich Mueller , Georg Krug , Peter Rudolf , Joaquim Henrique Teles , Hans-Georg Goebbel , Peter Bassler
IPC分类号： C07D301/12
CPC分类号： C07D301/12 , Y02P20/52
摘要： Process for preparing propylene oxide, which comprises at least the steps (i) and (ii): (i) providing a catalyst comprising at least one porous oxidic material; (ii) reacting propene with a hydroperoxide in at least one nitrile as solvent or in a solvent mixture comprising at least one nitrile in the presence of the catalyst of (i), wherein the at least one porous oxidic material is a zeolite which is assigned X-ray-crystallographically to the MWW type.
摘要翻译：制备环氧丙烷的方法，其至少包括步骤（i）和（ii）：（i）提供包含至少一种多孔氧化物质的催化剂; （ii）使丙烯与至少一种腈作为溶剂中的氢过氧化物反应或在包含至少一种腈的溶剂混合物中，在（i）的催化剂存在下反应，其中所述至少一种多孔氧化物质是被分配的沸石 X射线晶体学到MWW型。

38. 发明授权

US07544818B2 Continuous recirculation of the olefin which has not been reacted in the oxidation of olefins by hydroperoxides, by means of solvent scrubbing 失效
标题翻译：通过溶剂洗涤，通过氢过氧化物在烯烃的氧化中未反应的烯烃的连续再循环
公开(公告)号：US07544818B2
公开(公告)日：2009-06-09
申请号：US10531868
申请日：2003-10-23
申请人： Peter Bassler , Hans-Georg Goebbel , Joaquim Henrique Teles , Peter Rudolf
发明人： Peter Bassler , Hans-Georg Goebbel , Joaquim Henrique Teles , Peter Rudolf
IPC分类号： C07D301/06 , C07D301/12 , C07D301/19
CPC分类号： C07D301/12 , B01D53/1487 , B01D53/1493 , B01D2257/702 , C07D301/32
摘要： Process for the continuous recirculation of the olefin which has not been reacted in the oxidation of olefins by means of hydroperoxide to give oxiranes and is present in the offgas stream formed during the oxidation, which comprises the steps (i) to (iii) (i) separating the olefin from the offgas stream by absorption in a hydrocarbon, (ii) desorbing the olefin from the hydrocarbon, (iii) recirculating the olefin obtained in step (ii) to the oxidation process.
摘要翻译：通过氢过氧化物在烯烃氧化中未反应的烯烃的连续再循环以产生环氧乙烷并存在于氧化期间形成的废气流中的方法，其包括步骤（i）至（iii）（i ）通过在烃中的吸收从废气流中分离烯烃，（ii）从烃解链烯烃，（iii）将步骤（ii）中获得的烯烃再循环到氧化过程中。

39. 发明授权

US07449606B2 Method for producing a ketone 有权
标题翻译：酮的制造方法
公开(公告)号：US07449606B2
公开(公告)日：2008-11-11
申请号：US10573326
申请日：2004-09-23
申请人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Thomas Genger , Thomas Preiss
发明人： Joaquim Henrique Teles , Beatrice Röβler , Rolf Pinkos , Thomas Genger , Thomas Preiss
IPC分类号： C07C45/28
CPC分类号： C07C45/28 , C07C45/62 , C07C2601/20 , C07C49/607 , C07C49/413
摘要： A process for preparing a ketone, in particular cyclododecanone, by reacting cyclododecatriene with dinitrogen monoxide to obtain cyclododecadienone and hydrogenating the resulting cyclododecadienone, in particular to give cyclododecanone.
摘要翻译：通过使环十二碳三烯与一氧化二氮反应制备酮，特别是环十二酮的方法，得到环十二二烯酮，并使所得环十二己烯酮氢化，特别是得到环十二烷酮。

40. 发明授权

US07084310B2 Method for the continuous production of propylene glycol 失效
标题翻译：连续生产丙二醇的方法
公开(公告)号：US07084310B2
公开(公告)日：2006-08-01
申请号：US10521467
申请日：2003-07-22
申请人： Peter Bassler , Hans-Georg Goebbel , Joaquim Henrique Teles , Peter Rudolf
发明人： Peter Bassler , Hans-Georg Goebbel , Joaquim Henrique Teles , Peter Rudolf
IPC分类号： C07C29/03 , C07C29/04 , C07C29/10 , C07C29/80 , C07C29/84
CPC分类号： B01D3/141 , B01D3/143 , C07C29/106 , C07D301/12 , C07C31/205
摘要： Process for the continuous preparation of propylene glycols, which comprises the steps (i) to (ii): (i) reacting propylene with hydrogen peroxide to form propylene oxide and give propylene glycols as by-products, (ii) reacting the propylene oxide obtained in step (i) with water to give propylene glycols, (iii) separating off the propylene glycols obtained in steps (i) and (ii).
摘要翻译：用于连续制备丙二醇的方法，其包括步骤（i）至（ii）：（i）使丙烯与过氧化氢反应以形成环氧丙烷并产生作为副产物的丙二醇，（ii）使获得的环氧丙烷在步骤（i）中用水进行丙二醇，（iii）分离步骤（i）和（ii）中获得的丙二醇。

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