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31. 发明申请

US20070173654A1 Methods for dehydration of sugars 有权
标题翻译：糖脱水方法
公开(公告)号：US20070173654A1
公开(公告)日：2007-07-26
申请号：US11341968
申请日：2006-01-26
申请人： Johnathan Holladay , Jianli Hu , Xinjie Zhang , Yong Wang
发明人： Johnathan Holladay , Jianli Hu , Xinjie Zhang , Yong Wang
IPC分类号： C07D493/02
CPC分类号： C07D493/04
摘要： The invention includes a method of dehydration of a sugar using a dehydration catalyst and a co-catalyst within a reactor. A sugar is introduced and H2 is flowed through the reactor at a pressure of less than or equal to about 300 psig to convert at least some of the sugar into an anhydrosugar product. The invention includes a process for producing isosorbide. A starting material comprising sorbitol is flowed into a reactor. H2 is counter flowed through the reactor. The starting material is exposed to a catalyst in the presence of a co-catalyst which comprises at least one metal. The exposing is conducted at a hydrogen pressure of less than or equal to 300 psig within the reactor and the hydrogen removes at least some of any water present during the exposing and inhibits formation of colored byproducts.
摘要翻译：本发明包括使用反应器内的脱水催化剂和助催化剂使糖脱水的方法。引入糖，并且H 2 O 2以小于或等于约300psig的压力流过反应器，以将至少一些糖转化为脱水糖产物。本发明包括制备异山梨醇的方法。将含有山梨醇的原料流入反应器。 H 2反向流过反应器。在包含至少一种金属的助催化剂的存在下，将原料暴露于催化剂。暴露在反应器内在小于或等于300psig的氢气压力下进行，并且氢去除暴露期间存在的任何水中的至少一些，并且抑制着色副产物的形成。

32. 发明申请

US20080103318A1 Hydroxymethyl Furfural Oxidation Methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US20080103318A1
公开(公告)日：2008-05-01
申请号：US11932436
申请日：2007-10-31
申请人： Michael Lilga , Richard Hallen , Jianli Hu , James White , Michel Gray
发明人： Michael Lilga , Richard Hallen , Jianli Hu , James White , Michel Gray
IPC分类号： C07D307/68 , B01J21/06 , B01J23/42 , C07D307/46
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O 2 2中的至少一个提供到反应器中。使起始材料与包含Pt的催化剂在载体材料上接触，其中在约50℃至约200℃的反应器温度下进行接触。一种制备氧化催化剂的方法，其中ZrO 2 / SUB>并被煅烧。将ZrO 2 2与乙酰丙酮酸铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2 2的流下被钝化。

33. 发明授权

US08957259B2 Dimethyl ether production from methanol and/or syngas 有权
标题翻译：由甲醇和/或合成气生产二甲醚
公开(公告)号：US08957259B2
公开(公告)日：2015-02-17
申请号：US11241321
申请日：2005-09-30
申请人： Robert A. Dagle , Yong Wang , Eddie G. Baker , Jianli Hu
发明人： Robert A. Dagle , Yong Wang , Eddie G. Baker , Jianli Hu
IPC分类号： C07C41/09 , C07C41/01
CPC分类号： C07C41/09 , C07C41/01 , C07C43/043
摘要： Disclosed are methods for producing dimethyl ether (DME) from methanol and for producing DME directly from syngas, such as syngas from biomass. Also disclosed are apparatus for DME production. The disclosed processes generally function at higher temperatures with lower contact times and at lower pressures than conventional processes so as to produce higher DME yields than do conventional processes. Certain embodiments of the processes are carried out in reactors providing greater surface to volume ratios than the presently used DME reactors. Certain embodiments of the processes are carried out in systems comprising multiple microchannel reactors.
摘要翻译：公开了从甲醇生产二甲醚（DME）并直接从合成气生产DME的方法，例如来自生物质的合成气。还公开了用于DME生产的装置。所公开的方法通常在比常规方法更低的接触时间和更低的压力的较高温度下起作用，以产生比常规方法更高的DME产率。该方法的某些实施方案在提供比目前使用的DME反应器更大的表面与体积比的反应器中进行。该方法的某些实施方案在包括多个微通道反应器的系统中进行。

34. 发明授权

US07728156B2 Method of performing sugar dehydration and catalyst treatment 失效
标题翻译：糖脱水和催化剂处理方法
公开(公告)号：US07728156B2
公开(公告)日：2010-06-01
申请号：US11342146
申请日：2006-01-26
申请人： Jianli Hu , Johnathan E. Holladay , Xinjie Zhang , Yong Wang
发明人： Jianli Hu , Johnathan E. Holladay , Xinjie Zhang , Yong Wang
IPC分类号： C07C29/00 , C07D315/00 , C07D493/00 , C07H1/00 , C07H17/00 , C07H5/04 , C07H1/06 , C13K5/00
CPC分类号： C07H1/00
摘要： The invention includes a method of treating a solid acid catalyst. After exposing the catalyst to a mixture containing a sugar alcohol, the catalyst is washed with an organic solvent and is then exposed to a second reaction mixture. The invention includes a process for production of anhydrosugar alcohol. A solid acid catalyst is provided to convert sugar alcohol in a first sample to an anhydrosugar alcohol. The catalyst is then washed with an organic solvent and is subsequently utilized to expose a second sample. The invention includes a method for selective production of an anhydrosugar. A solid acid catalyst is provided within a reactor and anhydrosugar alcohol is formed by flowing a starting sugar alcohol into the reactor. The acid catalyst is then exposed to an organic solvent which allows a greater amount of additional anhydrosugar to be produced than would occur without exposing the acid catalyst to the organic solvent.
摘要翻译：本发明包括一种处理固体酸催化剂的方法。在将催化剂暴露于含有糖醇的混合物之后，用有机溶剂洗涤催化剂，然后暴露于第二反应混合物。本发明包括生产脱水葡萄糖醇的方法。提供固体酸催化剂以将第一样品中的糖醇转化为脱水葡萄糖醇。然后将催化剂用有机溶剂洗涤，随后用于暴露第二个样品。本发明包括选择性生产脱水糖的方法。在反应器内提供固体酸催化剂，通过将起始糖醇流入反应器而形成脱水葡萄糖醇。然后将酸催化剂暴露于有机溶剂，其允许比不会将酸催化剂暴露于有机溶剂而产生更多量的额外的脱水糖。

35. 发明授权

US07649099B2 Method of forming a dianhydrosugar alcohol 失效
标题翻译：形成二脱水糖醇的方法
公开(公告)号：US07649099B2
公开(公告)日：2010-01-19
申请号：US11341961
申请日：2006-01-26
申请人： Johnathan E. Holladay , Jianli Hu , Yong Wang , Todd A. Werpy , Xinjie Zhang
发明人： Johnathan E. Holladay , Jianli Hu , Yong Wang , Todd A. Werpy , Xinjie Zhang
IPC分类号： C07C29/00 , C07D315/00 , C07D493/00 , C07H1/00 , C07H17/00 , C07H5/04 , C07H1/06 , C13K5/00
CPC分类号： C07D307/20 , C07D493/04 , Y02P20/127
摘要： The invention includes methods of producing dianhydrosugars. A polyol is reacted in the presence of a first catalyst to form a monocyclic sugar. The monocyclic sugar is transferred to a second reactor where it is converted to a dianhydrosugar alcohol in the presence of a second catalyst. The invention includes a process of forming isosorbide. An initial reaction is conducted at a first temperature in the presence of a solid acid catalyst. The initial reaction involves reacting sorbitol to produce 1,4-sorbitan, 3,6-sorbitan, 2,5-mannitan and 2,5-iditan. Utilizing a second temperature, the 1,4-sorbitan and 3,6-sorbitan are converted to isosorbide. The invention includes a method of purifying isosorbide from a mixture containing isosorbide and at least one additional component. A first distillation removes a first portion of the isosorbide from the mixture. A second distillation is then conducted at a higher temperature to remove a second portion of isosorbide from the mixture.
摘要翻译：本发明包括生产二脱水甘油糖的方法。多元醇在第一催化剂存在下反应形成单环糖。将单环糖转移到第二反应器中，在第二反应器中，在第二催化剂的存在下将其转化为二脱水甘油醇。本发明包括形成异山梨醇的方法。在固体酸催化剂存在下，在第一温度下进行初始反应。初始反应包括使山梨醇反应生成1,4-脱水山梨糖醇，3,6-脱水山梨糖醇，2,5-甘露聚糖和2,5-己烷。利用第二温度，将1,4-脱水山梨醇和3,6-脱水山梨醇转化为异山梨醇。本发明包括从含有异山梨醇和至少一种另外的组分的混合物中纯化异山梨醇的方法。第一蒸馏从混合物中除去第一部分的异山梨醇。然后在较高温度下进行第二次蒸馏以从混合物中除去第二部分的异山梨醇。

36. 发明申请

US20090297435A1 Microcombustors, Microreformers, And Methods Involving Combusting Or Reforming Liquids 有权
标题翻译：微燃烧器，微型反应器和涉及燃烧或重整液体的方法
公开(公告)号：US20090297435A1
公开(公告)日：2009-12-03
申请号：US12538140
申请日：2009-08-09
申请人： Jamelyn D. Holladay , Yong Wang , Jianli Hu , Ya-Huei Chin , Robert A. Dagle , Guanguang Xia , Eddie G. Baker , Daniel R. Palo , Max Phelps , Heon Jung
发明人： Jamelyn D. Holladay , Yong Wang , Jianli Hu , Ya-Huei Chin , Robert A. Dagle , Guanguang Xia , Eddie G. Baker , Daniel R. Palo , Max Phelps , Heon Jung
IPC分类号： C01B3/26 , H01M8/18 , B01J8/04 , C01B3/02
CPC分类号： F23C13/00 , B01J19/0093 , B01J21/04 , B01J21/066 , B01J23/60 , B01J23/63 , B01J37/03 , B01J2219/00783 , B01J2219/00833 , B01J2219/00835 , B01J2219/00873 , B01J2219/00891 , C01B3/323 , C01B3/384 , C01B2203/00 , C01B2203/0233 , C01B2203/04 , C01B2203/0445 , C01B2203/047 , C01B2203/066 , C01B2203/0811 , C01B2203/0816 , C01B2203/0822 , C01B2203/0827 , C01B2203/1011 , C01B2203/1052 , C01B2203/1064 , C01B2203/1076 , C01B2203/1082 , C01B2203/1217 , C01B2203/1223 , C01B2203/1288 , C01B2203/1619 , F23C2900/03001 , Y02P20/128 , Y02P20/52
摘要： The invention describes combustors and steam reformers and methods of combustion and steam reforming. For example, integrated combustion reactors are described in which heat from combustion is transferred to an endothermic reaction. Thermally efficient reactors and methods of alcohol steam reforming are also described. Also described is an integrated combustor/reformer containing a methanation catalyst.
摘要翻译：本发明描述了燃烧器和蒸汽重整器以及燃烧和蒸汽重整的方法。例如，描述了将来自燃烧的热转移到吸热反应的综合燃烧反应器。还描述了热效率的反应器和醇蒸汽重整的方法。还描述了含有甲烷化催化剂的一体化燃烧器/重整器。

37. 发明申请

US20100152470A1 Hydroxymethyl Furfural Oxidation Methods 有权
公开(公告)号：US20100152470A1
公开(公告)日：2010-06-17
申请号：US12712100
申请日：2010-02-24
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/46
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.

38. 发明申请

US20090113787A1 Palladium Catalyzed Hydrogenation of Bio-Oils and Organic Compounds 有权
标题翻译：钯催化生物油和有机化合物的氢化
公开(公告)号：US20090113787A1
公开(公告)日：2009-05-07
申请号：US12140929
申请日：2008-06-17
申请人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
发明人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
IPC分类号： C10L1/18
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果已经显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

39. 发明授权

US07425657B1 Palladium catalyzed hydrogenation of bio-oils and organic compounds 有权
标题翻译：钯催化氢化生物油和有机化合物
公开(公告)号：US07425657B1
公开(公告)日：2008-09-16
申请号：US11759075
申请日：2007-06-06
申请人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
发明人： Douglas C. Elliott , Jianli Hu , Todd R. Hart , Gary G. Neuenschwander
IPC分类号： C07C41/48 , C07C41/50 , C07C33/03 , C07C31/18
CPC分类号： C07C29/172 , B01J21/18 , B01J23/44 , B01J23/462 , B01J37/0201 , C07C29/149 , C07C2601/08 , C07C2601/14 , C07D307/06 , C10G1/00 , C10G1/06 , C10G1/086 , C10G3/47 , C10G3/48 , C10G3/50 , C10G2300/1014 , C10G2300/4018 , Y02E50/14 , Y02E50/32 , Y02P20/52 , Y02P30/20 , C07C35/14 , C07C35/08 , C07C31/04 , C07C31/08 , C07C31/20 , C07C31/125 , C07C35/06
摘要： The invention provides palladium-catalyzed hydrogenations of bio-oils and certain organic compounds. Experimental results have shown unexpected and superior results for palladium-catalyzed hydrogenations of organic compounds typically found in bio-oils.
摘要翻译：本发明提供钯催化的生物油和某些有机化合物的氢化。实验结果已经显示出对于通常在生物油中发现的有机化合物的钯催化氢化的意想不到的和优异的结果。

40. 发明授权

US07700788B2 Hydroxymethyl furfural oxidation methods 有权
标题翻译：羟甲基糠醛氧化法
公开(公告)号：US07700788B2
公开(公告)日：2010-04-20
申请号：US11932436
申请日：2007-10-31
申请人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
发明人： Michael A. Lilga , Richard T. Hallen , Jianli Hu , James F. White , Michel J. Gray
IPC分类号： C07D307/44
CPC分类号： C07D307/48 , C07D307/44
摘要： A method of oxidizing hydroxymethylfurfural (HMF) includes providing a starting material which includes HMF in a solvent comprising water into a reactor. At least one of air and O2 is provided into the reactor. The starting material is contacted with the catalyst comprising Pt on a support material where the contacting is conducted at a reactor temperature of from about 50° C. to about 200° C. A method of producing an oxidation catalyst where ZrO2 is provided and is calcined. The ZrO2 is mixed with platinum (II) acetylacetonate to form a mixture. The mixture is subjected to rotary evaporation to form a product. The product is calcined and reduced under hydrogen to form an activated product. The activated product is passivated under a flow of 2% O2.
摘要翻译：氧化羟甲基糠醛（HMF）的方法包括在包含水的溶剂中将包含HMF的原料提供到反应器中。将空气和O2中的至少一个提供到反应器中。起始材料与包含Pt的催化剂在载体材料上接触，其中接触在约50℃至约200℃的反应器温度下进行。制备其中提供ZrO 2并被煅烧的氧化催化剂的方法。将ZrO 2与乙酰丙酮化铂（II）混合以形成混合物。将混合物进行旋转蒸发以形成产物。将产物在氢气下煅烧和还原以形成活化产物。活化产物在2％O 2的流量下钝化。

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