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31. 发明专利

JPH02199197A REMOVAL OF MERCURY FROM HYDROCARBON 失效
公开(公告)号：JPH02199197A
公开(公告)日：1990-08-07
申请号：JP1767789
申请日：1989-01-30
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , SATO KAZUO , MATSUZAWA TORU , ITO HIROFUMI
IPC分类号： B01D53/14 , B01D11/04 , C10G21/08 , C10G21/22 , C10G29/10 , C10L3/10
摘要： PURPOSE:To enable to efficiently remove mercury from a hydrocarbon by bringing a liq. or gaseous hydrocarbon contg. mercury into contact with an aq. polysulfide soln. and separating it from the aq. phase. CONSTITUTION:A liq. or gaseous hydrocarbon contg. mercury, obtd. from, e.g. a natural gas or a gas entrained by petroleum is brought into contact with an aq. soln. of a polysulfide (e.g. sodium polysulfide) and is separated from the aq. phase.

32. 发明专利

JPH0234688A METHOD FOR REMOVAL OF MERCURY 失效
公开(公告)号：JPH0234688A
公开(公告)日：1990-02-05
申请号：JP18355988
申请日：1988-07-25
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , SATO KAZUO , MATSUZAWA TORU
IPC分类号： B01D15/00 , B01J20/02 , B01J20/04 , C10L3/10
摘要： PURPOSE:To realize the removal of mercury at high efficiency by treating a liquid hydrocarbon containing mercury with a specified sulfur compound, followed by contact with an adsorbent containing a heavy metal sulfide. CONSTITUTION:1-15wt.% heavy metal sulfide (a) preferably containing 0.1-5wt.% Co or Ni is mixed, as required, with a carrier substance (b) (e.g., Al2O3) having a specific surface of 5-400m /g, molded and baked at 450-550 deg.C for 0.1-2hr in the air to give a material in which component (b) carries component (a). This material is then sulfurized with a gas mixture comprising hydrogen and 0.1-10vol.% hydrogen sulfide at 200-450 deg.C, thus giving an adsorbent. A liquid hydrocarbon containing mercury, obtained from natural gas or a gas entrained by petroleum, is treated with a sulfur compound of the formula (wherein M and M' are each H, alkali metal or ammonium) (e.g., H2S) and then brought into contact with said adsorbent.

33. 发明专利

JPH09296183A PRETREATMENT OF HEAVY OIL 失效
公开(公告)号：JPH09296183A
公开(公告)日：1997-11-18
申请号：JP10937196
申请日：1996-04-30
申请人： JGC CORP
发明人： SATO KAZUO , YAMADA MASATOSHI , KATAGIRI TSUTOMU , NOZAKI SHINJI
IPC分类号： C10G31/00 , C10G31/06 , C10G31/09
摘要： PROBLEM TO BE SOLVED: To reduce the backwashing frequency of a filter and pretreat a heavy oil so as to reduce the exchange of a changeover device of oil passage/ backwashing by carrying out the dehydrating treatment of the heavy oil before introducing the heavy oil containing solid grains and moisture into the filter and increasing the oil passage time through the filter. SOLUTION: The dehydrating treatment of a heavy oil is previously carried out by heating, vacuum and contact operations with an inert gas or combined operations thereof, etc., when introducing the heavy oil containing solid grains and moisture (e.g. an atmospheric distillation bottom oil prepared by introducing a raw material oil containing the solid grains into a distillation column and distilling the raw material oil under atmospheric pressure while blowing steam thereinto and a vacuum distillation bottom oil obtained by introducing the atmospheric distillation bottom oil into a distillation column and distilling the atmospheric distillation bottom oil under a reduced pressure while blowing steam thereinto) into a filter. Furthermore, the dehydrating treatment is preferably performed so as to provide

34. 发明专利

JPH0857302A ADSORBENT FOR MERCURY IN LIQUID HYDROCARBON 失效
公开(公告)号：JPH0857302A
公开(公告)日：1996-03-05
申请号：JP22084194
申请日：1994-08-24
申请人： JGC CORP
发明人： YAMADA MASATOSHI , SATO KAZUO , SATO KUNIO , MORII SABURO
IPC分类号： B01D15/00 , B01J20/02 , C10G25/00
摘要： PURPOSE: To provide an adsorbent suppressing the deterioration in its adsorbing performance of mercury due to the coexistence of adsorption blocking components such as mercaptan and amines. CONSTITUTION: This adsorbent contains sulfides of Mo and Cu as active components and especially adsorbs mercury as a simple substance and/or mercury compds. in liq. hydrocarbon. The proper Mo content is 5-20wt.% (expressed in terms of MoO3 ) and the proper Cu content is 0.1-5wt.%, preferably 0.1-3wt.% (expressed in terms of CuO).

35. 发明专利

JPH0633070A METHOD FOR REMOVING MERCURY IN LIQUID HYDROCARBON 失效
公开(公告)号：JPH0633070A
公开(公告)日：1994-02-08
申请号：JP10019892
申请日：1992-03-27
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , YAMADA MASATOSHI , MATSUZAWA TORU , SATO KAZUO
IPC分类号： B01D15/00 , B01J20/02 , B01J21/18 , C10G25/00 , C10G29/00 , C10G29/10
摘要： PURPOSE:To remove all the mercury contained in a liquid hydrocarbon. CONSTITUTION:A natural gas condensate (with 400mug/l total mercury content), produced in Southeast Asia and containing 390mug/l ogranomercury as mercury is passed through a reactional tube, having 14mm inside diameter, filled with 20ml gamma-alumina supporting 15.9wt.% carbon under conditions of 200 deg.C temperature, 30kg/cm G pressure and 52ml/hr flow rate and then passed over a sulfide adsorbent containing 6.9wt.% Mo, 0.9wt.% cobalt and 0.4wt.% nickel expressed in terms of an unsulfided composition on alumina to afford the objective product with

36. 发明专利

JPH0569887B2 失效
公开(公告)号：JPH0569887B2
公开(公告)日：1993-10-04
申请号：JP14417989
申请日：1989-06-08
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , SATO KAZUO
IPC分类号： C22B43/00

37. 发明专利

JPH04214794A REMOVAL OF MERCURY IN LIQUID HYDROCARBON 失效
公开(公告)号：JPH04214794A
公开(公告)日：1992-08-05
申请号：JP40989690
申请日：1990-12-12
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , YAMADA MASATOSHI , SATO KAZUO
IPC分类号： B01D53/02 , B01J20/08 , B01J20/20 , C01G13/00 , C07C7/12 , C10G25/00 , C10G29/02 , C10L1/00 , C10L3/10
摘要： PURPOSE:This invention relates to a method for highly efficiently removing mercury from a liquid hydrocarbon containing mercury with an adsorbent. CONSTITUTION:The method of the invention for removing mercury in a liquid hydrocarbon is characterized in that the liquid hydrocarbon is brought into contact with an adsorbent comprising an alkali metal sulfide-carrying alumina or active carbon or with a mixture of the adsorbent and an adsorbent containing a heavy metal sulfide. Since ionic mercury can be removed only by a fixed bed style adsorbing process, the area of an installation can highly reduced in comparison with extraction methods using absorbing solutions. The liquid hydrocarbon can be treated at the ordinary temperature under the atmospheric pressure.

38. 发明专利

JPH0428040B2 失效
公开(公告)号：JPH0428040B2
公开(公告)日：1992-05-13
申请号：JP18355988
申请日：1988-07-25
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , SATO KAZUO , MATSUZAWA TOORU
IPC分类号： B01D15/00 , B01J20/02 , B01J20/04 , C10L3/10

39. 发明专利

JPH03250092A METHOD FOR REMOVING MERCURY FROM LIQUID HYDROCARBON 失效
公开(公告)号：JPH03250092A
公开(公告)日：1991-11-07
申请号：JP4546990
申请日：1990-02-28
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , SATO KAZUO , ISHIKAWA SAKAE
IPC分类号： C10L1/12 , C10G29/10 , C10G29/28 , C10L1/24 , C10L3/10
摘要： PURPOSE:To realize the removal of even a hardly reactive organomercury compound at a high rate of removal by treating a liquid hydrocarbon containing a mercury compound with an aqueous solution of a water-soluble SH-containing organic compound and then with an aqueous solution of a specified sulfur compound to remove the mercury compound through extraction into the aqueous phase. CONSTITUTION:A liquid hydrocarbon (e.g. natural gas condensate) containing a mercury compound is treated with an aqueous solution of a water-soluble SH-containing organic compound (e.g. cysteine) and then with an aqueous solution of a sulfur compound of the formula MM'Sx (wherein M is an alkali metal or ammonium; M' is H or M; (x) is 1 to 6) (e.g. Na2S4) to remove the mercury compound through extraction into the aqueous phase.

40. 发明专利

JPH0310033A METHOD FOR RECOVERING MERCURY FROM SPENT MERCURY ADSORBENT 失效
公开(公告)号：JPH0310033A
公开(公告)日：1991-01-17
申请号：JP14417989
申请日：1989-06-08
申请人： JGC CORP
发明人： FURUTA AKIO , SATO KUNIO , SATO KAZUO
IPC分类号： C22B43/00
摘要： PURPOSE:To recover mercury from a spent mercury adsorbent and to make the adsorbent harmless by treating the adsorbent in a reducing stage of being brought into contact with a hydrogen gas and then in a hydrogen gas washing stage with the water soln. of polysulfide. CONSTITUTION:A spent adsorbent such as Co.Mo-S/Al2O3 adsorbing mercury in the shape of sulfide is brought into contact with a hydrogen gas at a temp. higher than the b.p. of mercury and reduction with hydrogen is executed to evaporate the reduced single mercury into the hydrogen gas. Next, the hydrogen gas contg. the obtd. single mercury is washed by the water soln. of polysulfide such as sodium polysulfide to recover mercury from the above adsorbent. If required, after the above stage, an acid is added to the water soln. of polysulfide contg. mercury obtd. by the above method and the pH of the soln. is regulated to about

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