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31. 发明申请

US20080242885A1 Method for Hydrocyanation 有权
标题翻译：氢化方法
公开(公告)号：US20080242885A1
公开(公告)日：2008-10-02
申请号：US10587027
申请日：2005-01-26
申请人： Tim Jungkamp , Hans-Martin Polka , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Hans-Martin Polka , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C253/10
CPC分类号： C07C253/34 , C07C255/07 , C07C255/04
摘要： A process is described for removing hydrogen cyanide from mixtures comprising pentenenitrile, wherein the removal is effected by an azeotropic distillation of hydrogen cyanide with 1,3-butadiene.
摘要翻译：描述了从包含戊烯腈的混合物中除去氰化氢的方法，其中通过氰化氢与1,3-丁二烯的共沸蒸馏来进行除去。

32. 发明申请

US20080221351A1 Method for the Production of Adipodinitrile by Hydrocyanation of 1,3-Butadiene 有权
标题翻译：通过1,3-丁二烯氢化生产阿ip啶腈的方法
公开(公告)号：US20080221351A1
公开(公告)日：2008-09-11
申请号：US10586450
申请日：2005-01-26
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Migeul Angel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Migeul Angel Flores , Tim Jungkamp , Hermann Luyken , Jens Scheidel , Wolfgang Siegel
IPC分类号： C07C253/08
CPC分类号： C07C253/10 , C07C255/09
摘要： A process is described for preparing adiponitrile by hydrocyanating 1,3-butadiene over a catalyst, by, in a first process step, hydrocyanating 1,3-butadiene to 3-pentenenitrile over at least one nickel(0) catalyst, and, in a second process step, hydrocyanating 3-pentenenitrile to adiponitrile over at least one nickel(0) catalyst with addition of at least one Lewis acid, wherein at least one of the at least one nickel(0) catalysts used in the particular process steps is transferred into the other process step.
摘要翻译：描述了通过在催化剂上氢化1,3-丁二烯来制备己二腈的方法，通过在第一工艺步骤中，在至少一种镍（O）催化剂上氢化1,3-丁二烯至3-戊烯腈，并且在在至少一种镍（O）催化剂中加入至少一种路易斯酸，将3-戊烯腈氢化成己二腈，其中在特定工艺步骤中使用的至少一种镍（0）催化剂中的至少一种被转移进入其他流程步骤。

33. 发明申请

US20070155980A1 Homogeneous isomerization of cis-2-pentene nitrile to form 3-pentene nitrile 失效
标题翻译：顺式-2-戊烯腈的均相异构化形成3-戊烯腈
公开(公告)号：US20070155980A1
公开(公告)日：2007-07-05
申请号：US10586481
申请日：2005-01-27
申请人： Jens Scheidel , Christian Miller , Robert Baumann , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Wolfgang Siegel , Peter Bassler
发明人： Jens Scheidel , Christian Miller , Robert Baumann , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Wolfgang Siegel , Peter Bassler
IPC分类号： C07C253/12
CPC分类号： C07C253/30 , Y02P20/127 , C07C255/07
摘要： A process is described for isomerizing pentenenitrile in a reactant stream, wherein the isomerization is effected over a homogeneously dissolved catalyst.
摘要翻译：描述了在反应物流中异构化戊烯腈的方法，其中异构化在均匀溶解的催化剂上进行。

34. 发明申请

US20070155978A1 Method for producing dinitriles 有权
公开(公告)号：US20070155978A1
公开(公告)日：2007-07-05
申请号：US10586500
申请日：2005-01-27
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C253/10
CPC分类号： C07C253/10 , C07C255/04
摘要： A process is described for preparing adiponitrile and methylglutaronitrile, characterized by the following process steps: (a) reacting a reactant stream comprising pentenenitriles with hydrogen cyanide in the presence of at least one catalyst and of at least one promoter to obtain a reaction stream which comprises pentenenitriles, the at least one catalyst, catalyst degradation products, the at least one promoter, adiponitrile and methylglutaronitrile, (b) distilling the reaction stream to obtain a stream 3 which is depleted in pentenenitriles and comprises the at least one catalyst, catalyst degradation products, the at least one promoter, adiponitrile and methylglutaronitrile as the bottom product and a stream 4 enriched in pentenenitriles as the top product, (c) extracting the stream 3 using an extractant present in stream 5 to obtain a stream 6 enriched with extractant as the top product which comprises the catalyst, and a stream 7 depleted in extractant as the bottom product which comprises catalyst degradation products, the at least one promoter, pentenenitriles, adiponitrile and methylglutaronitrile, (d) distilling the stream 6 to obtain a stream 8 comprising the catalyst as the bottom product and a stream 9 comprising the extractant as the top product, (e) distilling the stream 7 to obtain a stream 10 as the bottom product which comprises catalyst degradation products, the at least one promoter, pentenenitriles, adiponitrile and methylglutaronitrile, and a stream 11 comprising the extractant as the top product, (f) distilling the stream 10 to obtain a stream 12 as the bottom product which comprises catalyst degradation products, the at least one promoter, adiponitrile and methylglutaronitrile, and a stream 13 comprising pentenenitriles as the top product, (g) distilling the stream 12 to obtain a stream 14 as the bottom product which comprises catalyst degradation products and the at least one promoter, and a stream 15 as the top product which comprises adiponitrile and methylglutaronitrile, (h) distilling the stream 15 to obtain a stream 16 comprising adiponitrile as the bottoms and a stream 17 comprising methylglutaronitrile as the top product.

35. 发明授权

US07084294B2 Method for the recycling of a Lewis acid 失效
标题翻译：路易斯酸回收方法
公开(公告)号：US07084294B2
公开(公告)日：2006-08-01
申请号：US10520007
申请日：2003-07-04
申请人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
发明人： Tim Jungkamp , Jens Scheidel , Hermann Luyken , Michael Bartsch , Robert Baumann , Gerd Haderlein
IPC分类号： C07C253/10
CPC分类号： B01J31/24 , B01J27/32 , B01J31/1845 , B01J31/4015 , B01J31/403 , B01J2231/343 , C07C253/10 , Y02P20/584 , C07C255/07
摘要： A process for the recovery of a Lewis acid from a reaction mixture (I) which has been obtained in the hydrocyanation of an olefinically unsaturated compound to a nitrile which has a miscibility gap with water under certain pressure and temperature conditions, in the presence of a catalyst system comprising a Lewis acid and a complex compound. The method comprises a) removing the complex compound from mixture (I) to give a mixture (II), b) adding water to mixture (II) and placing mixture (II) under pressure and temperature conditions to provide a phase (III) and a phase (IV), c) adding a liquid diluent (V) which c1) does not form an azeotrope with water and whose boiling point under certain pressure conditions is higher than that of water, or c2) forms an azeotrope or heteroazeotrope with water under certain pressure conditions, to phase (III), d) subjecting the mixture of phase (III) and liquid diluent (V) to distillation under the pressure conditions mentioned in step c1) or c2), and e) subjecting mixture (VII) to hydrocyanation of an olefinically unsaturated compound to give the nitrile.
摘要翻译：从在不饱和化合物的氢氰化中获得的反应混合物（I）中回收路易斯酸的方法，该反应混合物在一定压力和温度条件下，在与催化剂体系包含路易斯酸和络合物。该方法包括：a）从混合物（I）中除去配合物，得到混合物（II），b）在混合物（II）中加入水并将混合物（II）置于压力和温度条件下以提供相（III）和相（Ⅳ），c）加入一种不与水形成共沸物的液体稀释剂（Ⅴ），其某些压力条件下的沸点高于水，或c2）与水形成共沸混合物（III），d）在步骤c1）或c2）所述的压力条件下使相（III）和液体稀释剂（V）的混合物进行蒸馏，和e）使混合物（VII）对烯属不饱和化合物进行氢化，得到腈。

36. 发明申请

US20110166377A1 METHOD FOR THE SEPARATION OF PENTENENITRILE ISOMERS 有权
标题翻译：用于分离PENTENENITRILE异构体的方法
公开(公告)号：US20110166377A1
公开(公告)日：2011-07-07
申请号：US13047212
申请日：2011-03-14
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C253/34
CPC分类号： C07C253/34 , C07C255/07
摘要： A process is described for separating mixtures of isomeric pentenenitriles, in which at least one isomer is removed from the mixture, wherein the separation of the substance mixtures of isomeric pentenenitriles is effected distillatively under reduced pressure.
摘要翻译：描述了用于分离异构戊烯腈混合物的方法，其中从混合物中除去至少一种异构体，其中异构戊烯腈的物质混合物的分离在减压下进行蒸馏。

37. 发明授权

US07709675B2 Continuous method for the production of linear pentene nitriles 有权
标题翻译：连续生产线性戊烯腈的方法
公开(公告)号：US07709675B2
公开(公告)日：2010-05-04
申请号：US10587028
申请日：2005-01-27
申请人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Jens Scheidel , Tim Jungkamp , Hermann Luyken
发明人： Michael Bartsch , Robert Baumann , Gerd Haderlein , Jens Scheidel , Tim Jungkamp , Hermann Luyken
IPC分类号： C07C253/10
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for continuously hydrocyanating 1,3-butadiene in the presence of at least one nickel(0) catalyst with chelate ligands, wherein 1,3-butadiene and hydrogen cyanide are used in a molar ratio of from 1.6:1 to 1.1:1.
摘要翻译：描述了在至少一种具有螯合配体的镍（O）催化剂的存在下连续氢氰化1,3-丁二烯的方法，其中使用1,3-丁二烯和氰化氢，摩尔比为1.6:1至1.1 ：1。

38. 发明授权

US07538240B2 Method for the hydrocyanation of butadiene 有权
标题翻译：丁二烯氢氰化方法
公开(公告)号：US07538240B2
公开(公告)日：2009-05-26
申请号：US10587026
申请日：2005-01-27
申请人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： C07C255/01
CPC分类号： C07C253/10 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene in the presence of at least one catalyst, wherein the reaction is carried out in a loop reactor having external pumped circulation and jet nozzle for driving the internal circulation.
摘要翻译：描述了一种通过在至少一种催化剂存在下氢化1,3-丁二烯来制备3-戊烯腈的方法，其中反应在具有外部泵送循环的环流反应器和用于驱动内部循环的喷嘴中进行。

39. 发明申请

US20080227214A1 Method for the Hydrocyanation of 1,3-Butadiene 审中-公开
标题翻译： 1,3-丁二烯氢化方法
公开(公告)号：US20080227214A1
公开(公告)日：2008-09-18
申请号：US10586473
申请日：2005-01-26
申请人： Tim Jungkamp , Robert Baumann , Thorsten Schroder , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
发明人： Tim Jungkamp , Robert Baumann , Thorsten Schroder , Michael Bartsch , Gerd Haderlein , Hermann Luyken , Jens Scheidel
IPC分类号： G01N31/16 , C07C253/10 , G01J5/02 , G01N9/00 , G01N30/02 , G01N25/18
CPC分类号： C07C253/10 , Y10T436/172307 , C07C255/07
摘要： A process is described for preparing 3-pentenenitrile by hydrocyanating 1,3-butadiene in the presence of at least one catalyst, wherein unhydrocyanated 1,3-butadiene is removed from the effluent of the hydrocyanation and recycled into the process, and the recycled 1,3-butadiene is monitored for the content of hydrogen cyanide.
摘要翻译：描述了一种通过在至少一种催化剂存在下氢化1,3-丁二烯制备3-戊烯腈的方法，其中将未氢化的1,3-丁二烯从氢化氰化物的流出物中除去并再循环至该方法中，监测氰化氢含量的3-丁二烯。

40. 发明申请

US20070287851A1 Isomerisation of Cis-2-Pentenenitrile to Form 3-Pentenenitrile in a Reactive Distillation 失效
标题翻译： Cis-2-戊烯腈在活性蒸馏中异构化形成3-戊烯腈
公开(公告)号：US20070287851A1
公开(公告)日：2007-12-13
申请号：US10585626
申请日：2005-01-27
申请人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
发明人： Jens Scheidel , Tim Jungkamp , Michael Bartsch , Gerd Haderlein , Robert Baumann , Hermann Luyken
IPC分类号： C07C291/00
CPC分类号： C07C253/30 , Y02P20/127 , C07C255/07
摘要： A process is described for isomerizing pentenenitrile in a reactant stream, wherein the isomerization is effected over a heterogeneous catalyst in a distillation column in such a way that, during the isomerization of the isomerization reactant, it is distillatively depleted in relation to the isomerization product in the reaction column of the distillation column.
摘要翻译：描述了在反应物流中异构化戊烯腈的方法，其中异构化在蒸馏塔中在非均相催化剂上进行，使得在异构化反应物的异构化期间，其相对于异构化产物馏出贫化蒸馏塔的反应塔。

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