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31. 发明专利

BR9913250A 未知
公开(公告)号：BR9913250A
公开(公告)日：2001-05-22
申请号：BR9913250
申请日：1999-08-17
申请人： BASF AG
发明人： LUYKEN HERMANN , OHLBACH FRANK , ANSMANN ANDREAS , BASSLER PETER , FISCHER ROLF , MELDER JOHANN-PETER , MERGER MARTIN , REHFINGER ALWIN , VOIT GUIDO , ACHHAMMER G NTHER
IPC分类号： C07B61/00 , C07C209/48 , C07C209/84 , C07C211/12 , C07C253/30 , C07C253/34 , C07C255/24
摘要： A process for the coproduction of 6-aminocapronitrile and hexamethylenediamine starting from adiponitrile bya) hydrogenating adiponitrile in the presence of a catalyst comprising an element of the eighth transition group as catalytically active component, to obtain a mixture comprising 6-aminocapronitrile, hexamethylenediamine, adiponitrile and high boilers,b) distillatively removing hexamethylenediamine from the mixture comprising 6-aminocapronitrile, hexamethylenediamine, adiponitrile and high boilers, and eithercl) distillatively removing 6-aminocapronitrile, and thend1) distillatively removing adiponitrile, orc2) simultaneously distillatively removing 6-aminocapronitrile and adiponitrile into separate fractionsis characterized by base of column temperatures below 185° C. in steps d1) or c2).

32. 发明专利

DE19954055A1 未知
公开(公告)号：DE19954055A1
公开(公告)日：2001-05-17
申请号：DE19954055
申请日：1999-11-10
申请人： BASF AG
发明人： BERRSCHE HELMUT , GABEL SABINE , IFFLAND GABRIELE , CIPRIAN JUERGEN , WENZEL ANNE , TELES JOAQUIM HENRIQUE , REHFINGER ALWIN
IPC分类号： B01J47/00 , B01J47/02 , B01J47/026 , C01B15/013 , C07D301/12
摘要： A device for removal of at least one salt from a hydrogen peroxide solution, by ion exchange, is characterised in that the device comprises at least one ion exchange bed (I) with a flow area F and height H, whereby the height H of the ion exchange bed is less than or equal to 2, 5.F .

33. 发明专利

BG104773A IRON-BASED CATALYST FOR HYDROGENATING ALPHA-, OMEGA-DINITRILES 未知
公开(公告)号：BG104773A
公开(公告)日：2001-04-30
申请号：BG10477300
申请日：2000-09-18
申请人： BASF AG
发明人： VOIT GUIDO , FISCHER ROLF , BASSLER PETER , ANSMANN ANDREAS , LUYKEN HERMANN , MERGER MARTIN , OHLBACH FRANK , REHFINGER ALWIN
IPC分类号： B01J23/78 , B01J23/889 , C07B61/00 , C07C209/48 , C07C211/12 , C07C253/30 , C07C255/24 , B01J23/74 , B01J23/00 , B01J23/02 , B01J23/32 , B01J21/06
摘要： The invention relates to a substance which is suitable for use as a catalyst, containing: (a) iron or a compound based on iron of mixtures thereof, (b) 0,001 to 0,3 wt. % in relation to (a) of a promoter based on 2, 3, 4, or 5 elements from the following group: aluminium, silicon, zirconium, titanium and vanadium; (c) 0 to 0.3 wt. % in relation to (a) of a compound based on an alkaline and/or alkaline earth metal, and (d) 0.001 to 1 wt. % in relation to (a) of manganese. The invention substances can be used as catalysts for the hydrogenation of alpha-, omega-dinitriles. 20 claims

34. 发明专利

BR9908972A 未知
公开(公告)号：BR9908972A
公开(公告)日：2000-12-05
申请号：BR9908972
申请日：1999-03-18
申请人： BASF AG
发明人： REHFINGER ALWIN , LUYKEN HERMANN
IPC分类号： C07D223/04 , B01D3/00 , C07C209/48 , C07C209/84 , C07C209/86 , C07C211/12 , C07C253/34 , C07C255/24 , C07D223/12
摘要： A process for distillative removal of part or all of an azepine derivative (III) selected from the group consisting of aminohexylideneimine, tetrahydroazepine, hexylhexahydroazepine and aminohexylhexahydroazepine from a mixture (II) comprising an azepine derivative (III) and an amine (I) comprises conducting the distillation with an overhead temperature of from 160 to 250° C.

35. 发明专利

TR200002588T2 未知
公开(公告)号：TR200002588T2
公开(公告)日：2000-11-21
申请号：TR200002588
申请日：1999-02-23
申请人： BASF AG
发明人： VOIT GUIDO , FISCHER ROLF , BASSLER PETER , ANSMANN ANDREAS , LUYKEN HERMANN , MERGER MARTIN , OHLBACH FRANK , REHFINGER ALWIN
IPC分类号： B01J23/78 , B01J23/889 , C07B61/00 , C07C209/48 , C07C211/12 , C07C253/30 , C07C255/24
摘要： A material useful as catalyst for the hydrogenation of alpha, omega-dinitriles comprises (a) iron or a compound based on iron or mixtures thereof, (b) from 0.001 to 0.3% by weight based on (a) of a promoter based on 2, 3, 4 or 5 elements selected from the group consisting of aluminum, silicon, zirconium, titanium and vanadium, (c) from 0 to 0.3% by weight based on (a) of a compound based on an alkali and/or alkaline earth metal, and also (d) from 0.001 to 1% by weight based on (a) of manganese.

36. 发明专利

BR9908506A 未知
公开(公告)号：BR9908506A
公开(公告)日：2000-11-21
申请号：BR9908506
申请日：1999-02-23
申请人： BASF AG
发明人： VOIT GUIDO , FISCHER ROLF , BASSLER PETER , ANSMANN ANDREAS , LUYKEN HERMANN , MERGER MARTIN , OHLBACH FRANK , REHFINGER ALWIN
IPC分类号： B01J23/78 , B01J23/745 , C07B61/00 , C07C209/48 , C07C211/09 , C07C211/12 , C07C253/30 , C07C255/24
摘要： A process for preparing aliphatic alpha, omega-diamines by hydrogenation of aliphatic alpha, omega-dinitriles in the presence of a catalyst comprises using a hydrogenation catalyst comprising(a) iron or a compound based on iron or mixtures thereof,(b) from 0.001 to 0.3% by weight based on (a) of a promoter based on 2, 3, 4 or 5 elements selected from the group consisting of aluminum, silicon, zirconium, titanium and vanadium, and also(c) from 0 to 0.3% by weight based on (a) of a compound based on an alkali and/or alkaline earth metal.

37. 发明专利

DK0800508T3 未知
公开(公告)号：DK0800508T3
公开(公告)日：2000-07-17
申请号：DK95941718
申请日：1995-12-16
申请人： BASF AG
发明人： FISCHER ROLF , SCHNURR WERNER , WITZEL TOM , HARDER WOLFGANG , EBEL KLAUS , FLICK KLEMENS , MELDER JOHANN-PETER , REHFINGER ALWIN
IPC分类号： B01J23/76 , B01J23/889 , B01J23/89 , B01J27/18 , B01J37/02 , C07B61/00 , C07C253/30 , C07C255/24
摘要： Aliphatic alpha,omega-aminonitriles are prepared by partial hydrogenation of aliphatic alpha,omega-dinitriles at elevated temperatures and superatmospheric pressure in the presence of a solvent and of a catalyst by a process which comprises using a catalyst which (a) contains a compound based on a metal selected from the group consisting of nickel, cobalt, iron, ruthenium and rhodium and (b) contains from 0.01 to 25% by weight, based on (a), of a promoter based on a metal selected from the group consisting of palladium, platinum, iridium, osmium, copper, silver, gold, chromium, molybdenum, tungsten, manganese, rhenium, zinc, cadmium, lead, aluminum, tin, phosphorus, arsenic, antimony, bismuth and rare earth metals and (c) from 0 to 5% by weight, based on (a), of a compound based on an alkali metal or on an alkaline earth metal. with the proviso that the component (a) is not based on iron or iron and one of the metals selected from the group consisting of cobalt, ruthenium and rhodium when (b) is a promoter based on a metal selected from the group consisting of titanium, manganese, chromium and molybdenum, and with the further proviso that, when a compound based on only ruthenium or rhodium or ruthenium and rhodium or nickel and rhodium is selected as component (a), the promoter (b) may be dispensed with.

38. 发明专利

TR9901895T2 未知
公开(公告)号：TR9901895T2
公开(公告)日：2000-04-21
申请号：TR9901895
申请日：1998-01-17
申请人： BASF AG
发明人： BASSLER PETER , LUYKEN HERMANN , REHFINGER ALWIN , RUST HARALD
IPC分类号： C07C255/24 , C07C253/34
CPC分类号： C07C253/34 , C07C255/24

39. 发明专利

CA2342178A1 IMPROVED METHOD FOR PRODUCING HEXAMETHYLENE DIAMINE 未知
公开(公告)号：CA2342178A1
公开(公告)日：2000-03-09
申请号：CA2342178
申请日：1999-08-17
申请人： BASF AG
发明人： REHFINGER ALWIN , FISCHER ROLF , VOIT GUIDO , MELDER JOHANN-PETER , MERGER MARTIN , ANSMANN ANDREAS , BASSLER PETER , OHLBACH FRANK , LUYKEN HERMANN
IPC分类号： C07B61/00 , C07C209/48 , C07C209/86 , C07C211/12
摘要： The invention relates to a method for the catalytic hydrogenation of adipodinitrile to hexamethylene diamine at a high temperature and at high pressure in the presence of catalysts based on elementary iron as the catalytic component, and ammonia as a solvent. The method is characterised i n that a) adipodinitrile is hydrogenated at temperatures of 70 to 220 ~C and a t pressures of 100 to 400 bar in the presence of catalysts based on elementary iron as the catalytic component, and ammonia as a solvent to produce a mixtu re containing adipodinitrile, 6-aminocapronitrile, hexamethylene diamine and hi gh boilers, until the sum of the 6-aminocapronitrile and adipodinitrile concentration is 1 to 50 wt. % in relation to the ammonia-free hydrogenation mixture; b) ammonia is separated out of the hydrogenation discharge; c) hexamethylene diamine is separated out of the remaining mixture; d) 6- aminocapronitrile and adipodinitrile are separated from the high boilers together or separately and e) 6-aminocapronitrile, adipodinitrile or their mixtures are returned to step a).

40. 发明专利

DE19839338A1 未知
公开(公告)号：DE19839338A1
公开(公告)日：2000-03-02
申请号：DE19839338
申请日：1998-08-28
申请人： BASF AG
发明人： LUYKEN HERMANN , OHLBACH FRANK , ANSMANN ANDREAS , BASLER PETER , FISCHER ROLF , MELDER JOHANN-PETER , MERGER MARTIN , REHFINGER ALWIN , VOIT GUIDO , ACHHAMMER GUENTHER
IPC分类号： C07B61/00 , C07C209/48 , C07C209/84 , C07C211/12 , C07C253/30 , C07C253/34 , C07C255/24
摘要： The invention relates to a method for simultaneous preparation of 6-aminocapronitrile and hexamethylene diamine from adipodinitrile, comprising the following steps: a) hydrogenating adipodinitrile in the presence of a catalyst containing an element of the eight subgroup as catalytically active component to obtain a mixture containing 6-aminocapronitrile, hexamethylene diamine, adipodinitrile and high boilers; b) separating by distillation hexamethylene diamine from the mixture containing 6-aminocapronitrile, hexamethylene diamine, adipodinitrile and high boilers and c1) separating by distillation 6-aminocapronitrile and subsequently d1) separating by distillation adipodinitrile or c2) simultaneously separating by distillation 6-aminocapronitrile and adipodinitrile into separate fractions. The method is characterized in that the temperature of the bottom in steps d1) or c2) is below 185 DEG C.

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