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31. 发明授权

US5260393A Vinylidene fluoride based fluoroelastomeric copolymers modified with perfluoroalkylvinylether 失效
标题翻译：用全氟烷基乙烯醚改性的偏二氟乙烯基氟弹性体共聚物
公开(公告)号：US5260393A
公开(公告)日：1993-11-09
申请号：US15266
申请日：1993-02-08
申请人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Anna Minutillo , Graziella Chiodini
发明人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Anna Minutillo , Graziella Chiodini
IPC分类号： C08F214/22 , C08F16/24
CPC分类号： C08F214/222
摘要： Fluoroelastic copolymers, suitable for the manufacture of O-rings, comprising by weight:48-65% of VDF units21-36% of HFP units3-9% of PAVE units0-17% of TFE units
摘要翻译：适用于制造O型圈的氟弹性共聚物，其重量百分比：48-65％VDF单元21-36％HFP单元3-9％PAVE单元0-17％TFE单元

32. 发明授权

US5219964A Fluoroelastomers endowed with improved processability and process for preparing them 失效
标题翻译：氟弹性体具有改进的加工性和制备它们的方法
公开(公告)号：US5219964A
公开(公告)日：1993-06-15
申请号：US925845
申请日：1992-08-07
申请人： Margherita Albano , Giulio Brinati , Vincenzo Arcella , Enzo Giannetti
发明人： Margherita Albano , Giulio Brinati , Vincenzo Arcella , Enzo Giannetti
IPC分类号： C08F4/08 , C08F214/22 , C08F214/26
CPC分类号： C08F214/22 , C08F214/26
摘要： Fluoroelastomers characterized by the presence of iodine or bromine atoms at the end of the polymeric chain in an amount equal to or lower than 1 iodine or bromine atom per polymeric chain, and by a bromine content in the chain ranging from 0.05 to 2% by weight referred to the total weight of the monomeric units.Said fluoroelastomers exhibit improved characteristics of processability, particularly as regards the utilization in injection molding processes and the detaching from the molds, as well as of stability to heat.A process for preparing fluoroelastomers containing iodine or bromine atoms at the ends of the polymeric chain, in an amount equal to or lower than 1 iodine or bromine atom per polymeric chain, which process comprises polymerizing mixes of fluorinated monomers (VDF, TFE, HFP, FVE) in bulk, in suspension, in aqueous emulsion, or in solution of organic solvents by means of radical starters, in the presence of compounds capable of providing I.sup.- or Br.sup.- ions in the polymerization medium and conditions.
摘要翻译：其特征在于聚合物链末端存在碘或溴原子，其量为每个聚合物链等于或低于1个碘或溴原子，并且链中的溴含量为0.05-2重量％指单体单元的总重量。所述含氟弹性体表现出改进的加工性能，特别是关于注射成型工艺的利用和从模具的分离以及对热的稳定性。在聚合物链的末端制备含有碘或溴原子的含氟弹性体的方法，其量等于或低于每个聚合物链1个碘或溴原子，该方法包括将氟化单体（VDF，TFE，HFP， FVE）在悬浮液中，在水性乳液中，或在有机溶剂的溶液中，通过自由基引发剂在能够在聚合介质和条件下提供I-或Br离子的化合物存在下进行。

33. 发明授权

US08513351B2 Fluoroelastomer gels 有权
标题翻译：氟弹性体凝胶
公开(公告)号：US08513351B2
公开(公告)日：2013-08-20
申请号：US11158334
申请日：2005-06-22
申请人： Marco Apostolo , Stefano Arrigoni , Margherita Albano
发明人： Marco Apostolo , Stefano Arrigoni , Margherita Albano
IPC分类号： C08F116/12
CPC分类号： C08L27/20 , C08F214/18 , C08F214/22 , C08K3/20 , C08L27/16 , C08L27/18 , C08L2205/02 , C08L2666/04
摘要： Fluoroelastomeric gel having the following properties: appearance: transparent gelatinous solid; water content between 10% and 90% by weight; a density between 1.1 and 2.1 g/cm3; said gel satisfies the following test: dried in a stove at 90° C. until a constant weight gives curable fluoroelastomers.
摘要翻译：具有以下性质的氟弹性体凝胶：外观：透明凝胶状固体; 水含量在10％至90％之间; 密度在1.1和2.1g / cm3之间; 所述凝胶满足以下试验：在90℃的炉子中干燥直到恒重为固化性的含氟弹性体。

34. 发明授权

US08476356B2 (Per)fluoroelastomeric compositions 失效
标题翻译：（Per）含氟弹性体组合物
公开(公告)号：US08476356B2
公开(公告)日：2013-07-02
申请号：US12307224
申请日：2007-06-28
申请人： Milena Stanga , Giovanni Comino , Stefano Arrigoni , Margherita Albano
发明人： Milena Stanga , Giovanni Comino , Stefano Arrigoni , Margherita Albano
IPC分类号： C08K5/04
CPC分类号： C08G65/007 , C08K3/04 , C08K5/01 , C08K13/02 , C08L27/12 , C08L27/18 , C08L2205/02 , C08L2666/04
摘要： A (per)fluoroelastomeric composition curable by peroxidic way comprising for 100 phr of (per)fluoroelastomer: as filler, from 2 to 70 phr of carbon black having a surface area between 25 and 35 m2/g; as crosslinking agent, from 0.5 to 10 phr of a bis-olefin having general formula: wherein: R1, R2, R3, R4, R5, R6, equal to or different from each other, are H or C1-C5 alkyls; Z is selected between a linear or branched C1-C18 alkylene or cycloalkylene radical, optionally containing oxygen atoms, preferably at least partially fluorinated, or a (per)fluoropolyoxyalkylene radical.
摘要翻译：包含100phr（per）含氟弹性体：作为填料，2-70phr表面积为25-35m2 / g的炭黑的过氧化物可固化的（全）氟弹性体组合物; 作为交联剂，0.5至10phr具有以下通式的双烯烃：其中：R 1，R 2，R 3，R 4，R 5，R 6彼此相同或不同，为H或C 1 -C 5烷基; Z选自直链或支链C 1 -C 18亚烷基或亚环烷基，任选地含有氧原子，优选至少部分氟化的或（全）氟聚氧亚烷基。

35. 发明授权

US08263708B2 Vulcanized (per) fluoroelastomer sealing articles 有权
标题翻译：硫化（per）含氟弹性体密封制品
公开(公告)号：US08263708B2
公开(公告)日：2012-09-11
申请号：US13132333
申请日：2009-12-03
申请人： Milena Stanga , Claudia Manzoni , Giovanni Comino , Margherita Albano
发明人： Milena Stanga , Claudia Manzoni , Giovanni Comino , Margherita Albano
IPC分类号： C08L27/12 , C08F214/26
CPC分类号： C09K3/1009 , C08L27/16 , C08L2205/02 , C08L2666/04
摘要： This invention pertains to sealing articles of vulcanized (per)fluoroelastomer compositions incorporating particles of a vinylidene fluoride (VDF) polymers having a Shore A hardness of at least 85 when determined according to ASTM D 2240 Type A Durometer method, and a compression set of less than 30%, when determined according to ASTM D395 at 200° C. for 70 h on O-ring according to ASTM D1414, and to a process for their manufacture by vulcanizing-molding and thermal post-treating at a temperature above the melting point of the VDF polymer.
摘要翻译：本发明涉及根据ASTM D 2240 A型硬度计方法测定的硫化（每）含氟弹性体组合物的密封制品，该组合物结合了具有至少85的肖氏A硬度的偏二氟乙烯（VDF）聚合物的颗粒，并且压缩永久变形当根据ASTM D395在200℃下根据ASTM D1414在O型圈上测定70小时时，其含量超过30％，以及在高于熔点的温度下通过硫化模塑和热后处理制造的方法的VDF聚合物。

36. 发明授权

US08198372B2 Vulcanisable fluoroelastomeric compositions 有权
标题翻译：可硫化含氟弹性体组合物
公开(公告)号：US08198372B2
公开(公告)日：2012-06-12
申请号：US12743204
申请日：2008-11-20
申请人： Giovanni Comino , Claudia Manzoni , Milena Stanga , Margherita Albano
发明人： Giovanni Comino , Claudia Manzoni , Milena Stanga , Margherita Albano
IPC分类号： C08L27/12
CPC分类号： C08L27/16 , C08L27/12 , C08L27/18 , C08L27/20 , C08L51/003 , C08L2205/02 , C08L2666/24 , C08L2666/04
摘要： Vulcanizable fluoroelastomer compositions comprising: A) a fluoroelastomer matrix based on vinylidene fluoride (VDF) with a Mooney viscosity (1+10) at 121° C. of less than 35 MU (Mooney Units) measured according to ASTM standard D 1646; and B) a semi-crystalline fluoropolymer, in an amount of from 20% to 70% by weight relative to the total weight of A)+B), the semi-crystalline fluoropolymer being constituted of tetrafluoroethylene (TFE) homopolymers and copolymers of TFE with one or more monomers containing at least one unsaturation of ethylenic type, in an amount of from 0.01 to 10 mol %, said semi-crystalline fluoropolymer having a mean particle size between 10 and 400 nm.
摘要翻译：可硫化的含氟弹性体组合物，其包含：A）基于偏二氟乙烯（VDF）的氟弹性体基体，其在121℃下的门尼粘度（1 + 10）根据ASTM标准D1646测量小于35MU（门尼单位）; 和B）相对于A）+ B）的总重量为20重量％至70重量％的半结晶含氟聚合物），半结晶含氟聚合物由四氟乙烯（TFE）均聚物和TFE共聚物构成所述半结晶含氟聚合物的平均粒度为10-400nm，其中一种或多种含有烯属型不饱和键的单体的量为0.01至10mol％。

37. 发明申请

US20110294944A1 Perfluoroelastomer 审中-公开
标题翻译：全氟弹性体
公开(公告)号：US20110294944A1
公开(公告)日：2011-12-01
申请号：US13148062
申请日：2010-02-08
申请人： Claudia Manzoni , Milena Stanga , Margherita Albano
发明人： Claudia Manzoni , Milena Stanga , Margherita Albano
IPC分类号： C08L27/18 , C08F8/00 , B29C41/46 , C08F16/24
CPC分类号： C08F214/262 , C08F214/26
摘要： A peroxide curable perfluoroelastomer comprising: recurring units derived from tetrafluoroethylene (TFE); recurring units derived from perfluoroethylvinylether (EVE), in an amount of between 2 and 17% by moles, with respect to total recurring units derived from TFE, perfluoromethylvinylether (MVE) and EVE; and recurring units derived from perfluoromethylvinylether (MVE), in an amount of between 23 and 35% by moles, with respect to total recurring units derived from TFE, perfluoromethylvinylether (MVE) and EVE. A process for its manufacture and its use for the manufacture of cured articles.
摘要翻译：一种过氧化物可固化的全氟弹性体，包括：衍生自四氟乙烯（TFE）的重复单元; 相对于衍生自TFE，全氟甲基乙烯基醚（MVE）和EVE的总重复单元，衍生自全氟乙基乙烯基醚（EVE）的重复单元的量为2至17摩尔％相对于衍生自TFE，全氟甲基乙烯基醚（MVE）和EVE的总重复单元，衍生自全氟甲基乙烯基醚（MVE）的重复单元的量为23至35摩尔％。其制造方法及其用于制造固化物品的方法。

38. 发明授权

US07767763B2 Fluoroelastomers 有权
标题翻译：氟弹性体
公开(公告)号：US07767763B2
公开(公告)日：2010-08-03
申请号：US12161638
申请日：2007-01-15
申请人： Francesco Triulzi , Margherita Albano , Milena Stanga
发明人： Francesco Triulzi , Margherita Albano , Milena Stanga
IPC分类号： C08F14/18
CPC分类号： C08F214/22 , C08F214/225 , C08F216/1408 , C08F236/20
摘要： VDF-based curable fluoroelastomers, having a glass transition temperature lower than −49° C., preferably lower than −50° C., and having the following composition, as percent moles: A) from 25% to 50%, preferably from 30% to 45%, of the monomer of formula: CF2═CFOCF2OCF3 (a); B) one or more (per)fluorinated comonomers having at least one unsaturation of ethylene type in amounts from 75% to 50%; preferably from 70% to 55%; said one or more comonomers comprising vinylidene fluoride (VDF) in amounts from 50% to 75% on the total of the monomer moles; the sum of the molar percentages of the monomers being 100%; said fluoroelastomers containing an amount of —COF end groups in the polymer lower than the sensitivity limit of the method reported in the description.
摘要翻译：玻璃化转变温度低于-49℃，优选低于-50℃，具有以下组成，以摩尔百分比计的VDF基可固化含氟弹性体：A）25％-50％，优选30 ％〜45％的式：CF2 = CFOCF2OCF3（a）的单体; B）一种或多种具有75％至50％的乙烯类型的至少一种不饱和度的（全）氟化共聚单体; 优选70％至55％; 所述一种或多种共聚单体包含单体摩尔数总计为50％至75％的偏二氟乙烯（VDF）; 单体的摩尔百分比之和为100％; 所述含氟弹性体在聚合物中含有一定量的-COF端基，低于说明书中报道的方法的灵敏度极限。

39. 发明申请

US20090286922A1 (PER)FLUOROELASTOMERIC COMPOSITIONS 有权
标题翻译：（PER）荧光材料组合物
公开(公告)号：US20090286922A1
公开(公告)日：2009-11-19
申请号：US12307061
申请日：2007-06-28
申请人： Milena Stanga , Giovanni Comino , Margherita Albano
发明人： Milena Stanga , Giovanni Comino , Margherita Albano
IPC分类号： C08L27/12
CPC分类号： C08K3/36 , C08F214/16 , C08F214/18 , C08F214/184 , C08F214/26 , C08K5/0025 , C08L27/12
摘要： A (per)fluoroelastomeric composition curable by peroxidic way comprising: 100 phr as (per)fluoroelastomer as filler, 0.5-50 phr of silica having a pH value, determined according to the DIN ISO 787-9 standard, higher than 7, preferably higher than 8, as crosslinking agent, from 0.5 to 10 phr of a bis-olefin having general formula: wherein: R1, R2, R3, R4, R5, R6, equal to or different from each other, are H or C1-C5 alkyls; Z is selected between a C1-C18 linear or branched alkylene or cycloalkylene radical, optionally containing oxygen atoms, preferably at least partially fluorinated, or a (per)fluoropolyoxyalkylene radical.
摘要翻译：通过过氧化物方法可固化的（全）含氟弹性体组合物，其包含：100phr作为（作为填料）的（含氟弹性体），0.5-50phr的具有pH值的二氧化硅，根据DIN ISO 787-9标准测定，高于7，优选较高作为交联剂，为0.5〜10phr的具有以下通式的双烯烃：其中：R 1，R 2，R 3，R 4，R 5，R 6，彼此相同或不同，为H或C 1 -C 5烷基 ; Z选自C1-C18直链或支链亚烷基或亚环烷基，任选地含有氧原子，优选至少部分氟化，或（全）氟聚氧亚烷基。

40. 发明申请

US20090030153A1 FLUOROELASTOMERS 有权
标题翻译：荧光素
公开(公告)号：US20090030153A1
公开(公告)日：2009-01-29
申请号：US12162458
申请日：2007-01-15
申请人： Milena Stanga , Francesco Triulzi , Margherita Albano
发明人： Milena Stanga , Francesco Triulzi , Margherita Albano
IPC分类号： C08F214/22
CPC分类号： C08F214/22 , C08F214/222 , C08L27/16 , C08L27/18 , C08L2205/02 , C08L2666/04
摘要： VDF curable fluoroelastomers, ionically cured, having a compression set after a time of 24 h (ASTM D 39/B) at −10° C. lower than 60%, preferably lower than 50% and at −25° C. lower than 90%, preferably lower than 75%, comprising hexafluoropropene (HFP) in amounts higher than 10% by moles and one vinylether of formula: CF2═CFOCF2OCF3 (a), an amount of —COF and groups in the polymer lower than the sensitivity limit of the method using the FT-IR spectroscopy described in the present application.
摘要翻译： VDF固化的含氟弹性体，在-10℃下在24小时后（ASTM D 39 / B）具有压缩永久变形，低于60％，优选低于50％和-25℃，低于90° ％，优选低于75％，其含量高于10％摩尔的六氟丙烯（HFP）和一种式CF2-CFOCF2OCF3（a）的乙烯基醚，其中-COF和聚合物中的基团低于敏感度极限该方法使用本申请中描述的FT-IR光谱。

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