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21. 发明专利

JPWO2008111488A1 キセノンの濃縮方法および濃縮装置有权
公开(公告)号：JPWO2008111488A1
公开(公告)日：2010-06-24
申请号：JP2009504011
申请日：2008-03-06
申请人：大陽日酸株式会社
发明人：中村　章寛 , 章寛中村 , 龍也飛弾野 , 龍也飛弾野 , 和彦藤江 , 和彦藤江
IPC分类号： C01B23/00 , B01D53/02 , B01D53/04 , B01J20/18 , B01J20/34
CPC分类号： F25J3/04757 , B01D53/0462 , B01D2253/108 , B01D2256/18 , B01D2257/11 , C01B23/0094 , C01B2210/0004 , C01B2210/0018 , C01B2210/0021 , C01B2210/0037 , C01B2210/004 , C01B2210/0045 , C01B2210/0062 , C01B2210/007 , C01B2210/0073 , C01B2210/0079 , C01B2210/0081 , C01B2210/0082 , C01B2210/0084 , F25J3/04412 , F25J2205/40 , F25J2205/60 , F25J2215/36
摘要：本発明は、温度スイング吸着法によるキセノンの濃縮方法であって、キセノンを含み、一酸化炭素を含まない常温の原料ガスを活性化したCu−ZSM5が充填された吸着筒に流通させる吸着工程と、加熱によりキセノンを脱着する脱着工程とを有し、これら2つの工程を交互に繰り返すことによってキセノンを濃縮する方法を提供する。

22. 发明授权

EP1079909B1 PROCEDE DE PURIFICATION, ET DE CONCENTRATION EN UN CONSTITUANT MINORITAIRE, D'UN MELANGE GAZEUX, PROCEDE DE DETECTION DE CE CONSTITUANT, ET INSTALLATION 有权
标题翻译：程序进行清洗和浓度外部气体混合物用于检测体和投资的组件，方法
公开(公告)号：EP1079909B1
公开(公告)日：2003-03-26
申请号：EP99919320.4
申请日：1999-05-11
申请人： COMMISSARIAT A L'ENERGIE ATOMIQUE
发明人： CHIAPPINI, Remo , FONTAINE, Jean-Pierre , HAMONET, Michel , THOUARD, Michel
IPC分类号： B01D53/22 , B01D53/04 , B01D59/50
CPC分类号： B01D53/229 , B01D53/04 , B01D59/12 , B01D59/22 , B01D59/50 , B01D2253/102 , B01D2256/18 , C01B23/0094 , C01B2210/001 , C01B2210/0014 , C01B2210/0026 , C01B2210/0028 , C01B2210/0037
摘要： The invention concerns a method for purifying, and concentrating into a minor constituent, a gaseous mixture, a method for detecting said constituent, and an installation for implementing said method. Said method comprises successively a selective permeation of the gaseous mixture through a specific membrane, a purifying step and a concentrating step. The treated gaseous mixture is atmospheric air whereof it is sought to concentrate some of the rare gases in particular xenon and the natural and radioactive species of xenon. The invention combined with nuclear spectrometry is therefore useful for detecting said species, whereof there is very little in the atmosphere, and for monitoring the environment of nuclear stations.

23. 发明公开

EP0956928A4 METHOD AND APPARATUS FOR PURIFICATION OF ARGON 审中-公开
标题翻译：方法和设备清洗氩
公开(公告)号：EP0956928A4
公开(公告)日：2001-06-13
申请号：EP98941722
申请日：1998-09-04
申请人： AIR LIQUIDE JAPAN LTD
发明人： YAMAMOTO TAKAO , YAMASHITA NAOHIKO
IPC分类号： B01D53/04 , B01D53/047 , C01B23/00 , F25J3/02 , B25J3/02
CPC分类号： F25J3/08 , B01D53/04 , B01D53/0462 , B01D53/047 , B01D53/261 , B01D2253/104 , B01D2253/108 , B01D2256/18 , B01D2257/504 , B01D2257/80 , B01D2259/40001 , B01D2259/40052 , B01D2259/40056 , C01B23/0094 , C01B2210/0004 , C01B2210/0006 , C01B2210/0014 , F25J3/0285 , F25J2200/02 , F25J2200/74 , F25J2205/40 , F25J2205/82 , F25J2210/04 , F25J2215/58 , F25J2245/58 , F25J2270/12 , F25J2290/42 , Y02C10/08 , Y02P20/152
摘要： A method for the purification of argon through simple steps with low energy consumption. Oxygen is added to argon gas containing nitrogen, carbon monoxide, oxygen, and methane as impurities, and carbon monoxide is oxidized carbon dioxide in a carbon monoxide oxidation column (31) in the presence of a catalyst. Hydrogen is added to the argon gas, and oxygen is reacted with hydrogen in a deoxo column (33) in the presence of a catalyst to conduct conversion to water. The carbon dioxide and water are removed from the argon gas in a carbon removal/drying unit (50) using an adsorbent. The resultant argon gas is cooled in a main heat exchanger (60) or the like for liquefaction. The formed liquid is then introduced into a rectifying column (70), where rectification is conducted by using the reflux composed mainly of argon. Nitrogen-enriched argon gas is separated from a head (76) of the rectifying column, while methane-enriched liquid argon is separated from a bottom (77), and high-purity argon gas is recovered from a gas phase in a middle stage.

24. 发明公开

EP0956928A1 METHOD AND APPARATUS FOR PURIFICATION OF ARGON 审中-公开
标题翻译： VERFAHREN UND VORRICHTUNG ZUR REINIGUNG VON ARGON
公开(公告)号：EP0956928A1
公开(公告)日：1999-11-17
申请号：EP98941722.5
申请日：1998-09-04
申请人： AIR LIQUIDE Japan, Ltd.
发明人： YAMAMOTO, Takao, Harima Technical Center , YAMASHITA, Naohiko, Harima Technical Center
IPC分类号： B25J3/02
CPC分类号： F25J3/08 , B01D53/04 , B01D53/0462 , B01D53/047 , B01D53/261 , B01D2253/104 , B01D2253/108 , B01D2256/18 , B01D2257/504 , B01D2257/80 , B01D2259/40001 , B01D2259/40052 , B01D2259/40056 , C01B23/0094 , C01B2210/0004 , C01B2210/0006 , C01B2210/0014 , F25J3/0285 , F25J2200/02 , F25J2200/74 , F25J2205/40 , F25J2205/82 , F25J2210/04 , F25J2215/58 , F25J2245/58 , F25J2270/12 , F25J2290/42 , Y02C10/08 , Y02P20/152
摘要： The present invention provides a process for purifying argon in simplified steps and with low energy consumption.
Oxygen is added to argon gas containing nitrogen, carbon monoxide, oxygen and methane as impurities. Carbon monoxide is oxidized into carbon dioxide in the presence of a catalyst in a carbon monoxide oxidation tower 31. Hydrogen is added to the argon gas to react oxygen with the hydrogen into water in the presence of a catalyst in a deoxo tower 33. The carbon dioxide and the water are removed from the argon gas in a water and carbon-dioxide removing unit 50 by use of an adsorbent. After cooled and liquefied in a main heat exchanger 60, the liquified argon is introduced into a distillation column 70 to perform distillation by use of a reflux containing argon as a main component. Nitrogen-condensed argon gas is withdrawn from a top portion 76 of the distillation column and methane-condensed liquid argon is withdrawn from the bottom 77, and then, high-purity argon gas is recovered from a gaseous phase of the middle stage.
摘要翻译：本发明提供了一种简化步骤和低能耗纯化氩气的方法。将氧气加入到含有氮气，一氧化碳，氧气和甲烷的氩气中作为杂质。一氧化碳在一氧化碳氧化塔31中的催化剂存在下被氧化成二氧化碳。在脱氧塔33中的催化剂存在下，向氩气中加入氢气以将氧气与氢气反应成水。碳通过使用吸附剂在水和二氧化碳去除单元50中从氩气中除去水。在主热交换器60中冷却并液化后，将液化的氩气引入蒸馏塔70中，通过使用以氩气为主要成分的回流进行蒸馏。从蒸馏塔的顶部部分76排出氮浓缩的氩气，从底部77排出甲烷冷凝的液体氩，然后从中间阶段的气相回收高纯度的氩气。

25. 发明申请

WO2013089584A3 METHOD AND DEVICE FOR PRODUCING A KRYPTON/XENON MIXTURE 审中-公开
标题翻译：用于生产KRYPTON / XENON MIXTURE的方法和装置
公开(公告)号：WO2013089584A3
公开(公告)日：2013-10-31
申请号：PCT/RU2012000762
申请日：2012-09-14
申请人： BONDARENKO VITALY LEONIDOVICH
发明人： BONDARENKO VITALY LEONIDOVICH , LOSYAKOV NIKOLAY PETROVICH , VOROTYNTSEV VALERIY BORISOVICH , GRAFOV ALEKSANDR PETROVICH , CHEREPANOV VALENTIN IVANOVICH , ALEKSAHIN VLADISLAV VASILEVICH
IPC分类号： B01D53/02 , F25J3/02
CPC分类号： C01B23/0094 , B01D53/002 , B01D53/02 , B01D53/75 , B01D53/864 , B01D2256/18 , B01D2257/104 , B01J7/00 , C01B23/0021 , C01B2210/0035 , C01B2210/0037 , C01B2210/0048 , C01B2210/0087 , F25J3/04757 , F25J2200/02 , F25J2205/82 , F25J2210/42 , F25J2270/904
摘要： The invention relates to inert gas production processes and can be used for producing a krypton/xenon mixture from a stream of oxygen derived from air separation plants and containing 0.05 - 0.5% krypton and xenon. The method for producing a krypton/xenon mixture involves purifying a stream of gaseous primary concentrate by the catalytic combustion thereof and subsequently cooling same, purifying the primary concentrate of catalytic combustion products, carrying out cooling upon completion of purification, fractionating the primary concentrate in a fractionating column to form a stream of krypton/xenon mixture and a stream of stripped oxygen and removing the stream of krypton/xenon mixture from the fractionating column in the form of a target product, as well as purifying the krypton/xenon mixture of radon. The invention makes it possible to extend the scope of use of the krypton/xenon mixture.
摘要翻译：本发明涉及惰性气体生产方法，可用于从空气分离装置产生的氧气流中生产氪/氙混合物，并含有0.05-0.5％的氪和氙。生产氪/氙混合物的方法包括通过其催化燃烧来纯化气态初级浓缩物流，随后冷却，纯化催化燃烧产物的主要浓缩物，在纯化完成后进行冷却，将初级浓缩物分馏成分离塔以形成氪/氙气混合物流和汽提氧气流，并从目标产物形式的分馏塔中除去氪/氙混合物流，以及纯化氡的氪/氙混合物。本发明可以延长氪/氙气混合物的使用范围。

26. 发明申请

WO1997016687A1 METHOD AND APPARATUS FOR PRODUCING LIQUID NITROGEN 审中-公开
标题翻译：生产液氮的方法和装置
公开(公告)号：WO1997016687A1
公开(公告)日：1997-05-09
申请号：PCT/CA1996000704
申请日：1996-10-24
申请人： GARDNER, Thomas, W.
IPC分类号： F25J01/00
CPC分类号： F25J1/0015 , C01B23/0094 , C01B2210/001 , C01B2210/0014 , F25J1/0037 , F25J1/004 , F25J1/0045 , F25J1/0202 , F25J1/0247 , F25J1/0288 , F25J1/0294 , F25J2205/40 , F25J2205/60 , F25J2205/80 , F25J2210/40 , F25J2230/30 , F25J2230/40 , F25J2230/42 , F25J2270/06
摘要： A method and apparatus for producing liquid nitrogen from air comprising a gaseous mixture of about 78 % by volume of nitrogen, about 21 % by volume of oxygen, less than 1.0 % by volume of argon, and small amounts of carbon dioxide, water vapour, and other trace elements and compounds comprise an extractor that extracts portions of the oxygen, carbon dioxide, and water vapour so as to produce a nitrogen-rich gaseous mixture comprising about 90 % to about 99 % by volume of nitrogen, about 10 % to about 1 % by volume of oxygen, and no more than trace amounts of carbon dioxide, water vapour, and other elements and compounds. A nitrogen recycle compressor compresses the nitrogen-rich gaseous mixture to a specified pressure. A gas expander expands and thereby cools the compressed nitrogen-rich gaseous mixture to a lower specified pressure which is slightly above atmospheric pressure, thereby cooling the nitrogen-rich gaseous mixture, which is fed into a heat exchanger, which cools a higher pressure nitrogen-rich gaseous mixture flowing in a separate pass of the heat exchanger, until at least a portion of the higher pressure nitrogen-rich gaseous mixture condenses to liquid state. A liquid/gas separator separates the liquid nitrogen from the nitrogen-rich gaseous mixture, which liquid nitrogen is extracted from the apparatus, through an outlet, for subsequent storage or use.
摘要翻译：一种用于从空气中产生液氮的方法和装置，包括约78体积％的氮气，约21体积％的氧气，小于1.0体积％的氩气和少量二氧化碳，水蒸汽，和其它微量元素和化合物包括提取器，其提取部分氧气，二氧化碳和水蒸汽，以便产生富含氮的气体混合物，其包含约90％至约99体积％的氮气，约10％至约 1体积％的氧，不超过痕量的二氧化碳，水蒸汽等元素和化合物。氮气再循环压缩机将富氮气体混合物压缩至特定压力。气体膨胀器膨胀，从而将压缩的富氮气体混合物冷却至略高于大气压的较低规定压力，从而冷却富氮气态混合物，该混合物进料到热交换器中，富集的气体混合物在热交换器的单独通道中流动，直到至少一部分较高压力的富氮气态混合物冷凝至液态。液体/气体分离器将液氮从富氮气体混合物中分离，氮气从设备中提取出来，通过出口进行存储或使用。

27. 发明申请

WO2015094175A1 PURIFICATION OF INERT GASES TO REMOVE TRACE IMPURITIES 审中-公开
标题翻译：净化气体去除痕迹污染物
公开(公告)号：WO2015094175A1
公开(公告)日：2015-06-25
申请号：PCT/US2013/075578
申请日：2013-12-17
申请人： L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE , HA, Bao , GARY, Daniel , SHANBHAG, Purushottam V.
发明人： HA, Bao , GARY, Daniel , SHANBHAG, Purushottam V.
IPC分类号： C01B23/00 , F25J3/02 , F25J3/08
CPC分类号： C01B23/0094 , C01B2210/0004 , C01B2210/0009 , C01B2210/0015 , C01B2210/0034 , C01B2210/0045 , C01B2210/0046 , C01B2210/005 , C01B2210/0051 , C01B2210/0053 , C01B2210/0062 , C01B2210/007 , F25J3/0285 , F25J3/08 , F25J2200/02 , F25J2200/04 , F25J2200/40 , F25J2200/50 , F25J2200/72 , F25J2205/40 , F25J2205/60 , F25J2210/58 , F25J2220/04 , F25J2235/06 , F25J2235/58 , F25J2270/58 , F25J2270/904
摘要： An argon purification system is provided which includes a cryogenic heat exchanger, a cryogenic distillation column. The cryogenic heat exchanger is configured to remove heat from a pre-treated argon waste stream to create a cold feed stream. The cryogenic distillation column includes packing, a reboiler, and an overhead condenser, as well as an upper portion and a lower portion and is configured to receive a liquid feed stream and to produce a bottoms argon product stream and a gas waste stream. The reboiler is positioned in the lower portion of the cryogenic distillation column and is configured to condense the cold feed stream to produce the liquid feed stream. The condenser is positioned in the upper portion of the cryogenic distillation column and is configured to heat the bottoms argon product stream such that the bottoms argon product stream evaporates to a purified vapor phase argon stream.
摘要翻译：提供了一种氩气净化系统，其包括低温热交换器，低温蒸馏塔。低温热交换器被配置为从预处理的氩废物流中除去热量以产生冷进料流。低温蒸馏塔包括填料，再沸器和顶部冷凝器，以及上部和下部，并且构造成接收液体进料流并产生塔底氩产物流和废气流。再沸器位于低温蒸馏塔的下部，并且构造成冷凝冷进料流以产生液体进料流。冷凝器定位在低温蒸馏塔的上部，并且构造成加热底部氩产物流，使得塔底氩产物流蒸发成纯化的气相氩气流。

28. 发明申请

WO99011437A1 METHOD AND APPARATUS FOR PURIFICATION OF ARGON 审中-公开
标题翻译： ARGON净化方法与装置
公开(公告)号：WO99011437A1
公开(公告)日：1999-03-11
申请号：PCT/JP1998/003977
申请日：1998-09-04
IPC分类号： B01D53/04 , B01D53/047 , C01B23/00 , F25J3/02 , B25J3/02
CPC分类号： F25J3/08 , B01D53/04 , B01D53/0462 , B01D53/047 , B01D53/261 , B01D2253/104 , B01D2253/108 , B01D2256/18 , B01D2257/504 , B01D2257/80 , B01D2259/40001 , B01D2259/40052 , B01D2259/40056 , C01B23/0094 , C01B2210/0004 , C01B2210/0006 , C01B2210/0014 , F25J3/0285 , F25J2200/02 , F25J2200/74 , F25J2205/40 , F25J2205/82 , F25J2210/04 , F25J2215/58 , F25J2245/58 , F25J2270/12 , F25J2290/42 , Y02C10/08 , Y02P20/152
摘要： A method for the purification of argon through simple steps with low energy consumption. Oxygen is added to argon gas containing nitrogen, carbon monoxide, oxygen, and methane as impurities, and carbon monoxide is oxidized carbon dioxide in a carbon monoxide oxidation column (31) in the presence of a catalyst. Hydrogen is added to the argon gas, and oxygen is reacted with hydrogen in a deoxo column (33) in the presence of a catalyst to conduct conversion to water. The carbon dioxide and water are removed from the argon gas in a carbon removal/drying unit (50) using an adsorbent. The resultant argon gas is cooled in a main heat exchanger (60) or the like for liquefaction. The formed liquid is then introduced into a rectifying column (70), where rectification is conducted by using the reflux composed mainly of argon. Nitrogen-enriched argon gas is separated from a head (76) of the rectifying column, while methane-enriched liquid argon is separated from a bottom (77), and high-purity argon gas is recovered from a gas phase in a middle stage.
摘要翻译：一种通过简单的步骤纯化氩气的方法，能耗低。将氧气加入到含有氮气，一氧化碳，氧气和甲烷的氩气中作为杂质，一氧化碳是在一氧化碳氧化塔（31）中在催化剂存在下被氧化的二氧化碳。在氩气中加入氢气，在催化剂存在下，氧气与脱氧塔（33）中的氢气反应，导致水转化。使用吸附剂在碳去除/干燥单元（50）中从氩气中除去二氧化碳和水。所得氩气在主热交换器（60）等中冷却以进行液化。然后将形成的液体引入精馏塔（70），其中通过使用主要由氩组成的回流来进行精馏。从精馏塔的头部（76）分离出富氮氩气，同时从底部（77）分离出富甲液体的氩气，在中间阶段从气相回收高纯度的氩气。

29. 发明申请

US20180050301A1 METHODS AND SYSTEMS FOR MANAGING GAS PURIFICATION 审中-公开
公开(公告)号：US20180050301A1
公开(公告)日：2018-02-22
申请号：US15555193
申请日：2016-03-04
申请人： MÉCANIQUE ANALYTIQUE INC.
发明人： Yves GAMACHE
IPC分类号： B01D53/34 , B01D53/32 , B01D53/04 , B01D53/30 , C01B23/00 , B01J20/02 , B01J20/34
CPC分类号： B01D53/346 , B01D53/0407 , B01D53/0423 , B01D53/0454 , B01D53/30 , B01D53/32 , B01D53/323 , B01D53/8696 , B01D2251/102 , B01D2253/102 , B01D2253/108 , B01D2253/116 , B01D2255/20707 , B01D2255/20715 , B01D2255/20723 , B01D2255/20738 , B01D2256/10 , B01D2256/18 , B01D2257/102 , B01D2257/108 , B01D2257/502 , B01D2257/504 , B01D2257/702 , B01D2257/7025 , B01D2257/80 , B01D2259/818 , B01J20/02 , B01J20/18 , B01J20/20 , B01J20/3408 , B01J20/3416 , B01J20/3433 , B01J20/3441 , C01B23/0015 , C01B23/0073 , C01B23/0094 , C01B2210/0029 , C01B2210/0046 , C01B2210/005 , C01B2210/0051 , C01B2210/0053 , C01B2210/0062 , C01B2210/007 , Y02C10/08 , Y02C20/20 , Y02P20/152 , Y02P20/156
摘要： A method for extending useful life of a sorbent for purifying a gas by sorption of an impurity is provided. The method generating a electrical discharge within the gas to obtain a spectral emission representative of a concentration of the impurity. The method also includes monitoring the concentration of the impurity according to the spectral emission. The method also includes lowering the concentration of the impurity by conversion of at least a portion of the impurity into a secondary impurity having a greater affinity to the sorbent than the impurity. The method also includes comparing the concentration of the impurity to a polluting concentration and managing the sorption of the gas onto the sorbent according to the comparison.

30. 发明申请

US20160115029A1 HELIUM RECOVERY PROCESS AND APPARATUS 审中-公开
公开(公告)号：US20160115029A1
公开(公告)日：2016-04-28
申请号：US14919816
申请日：2015-10-22
申请人： UOP LLC
发明人： Manu G. R. Van Leuvenhaege , Cedric F. Vercammen , Pavel V. Ryabchenko
IPC分类号： C01B23/00 , B01D53/22 , B01D53/047
CPC分类号： C01B23/0094 , B01D53/002 , B01D53/047 , B01D53/228 , B01D53/229 , B01D53/72 , B01D53/75 , B01D53/864 , B01D2251/102 , B01D2253/102 , B01D2253/104 , B01D2253/106 , B01D2253/108 , B01D2256/18 , B01D2257/108 , B01D2257/502 , B01D2257/504 , B01D2257/7022 , B01D2257/7025 , B01D2257/80 , C01B2210/0004 , C01B2210/001 , C01B2210/0014 , C01B2210/0031 , Y02C10/10 , Y02C20/20 , Y02P20/152 , Y02P20/156
摘要： A process and apparatus for increasing recovery of helium are described. The process includes introducing the stream containing helium and at least one oxidizable component into an oxidation zone in the presence of oxygen to oxidize the oxidizable component forming a first vapor stream and a first liquid stream. The first vapor stream is introduced into a pressure swing adsorption zone to form a purified helium stream and a tail gas stream. The tail gas stream is compressed. The compressed tail gas stream is introduced into a membrane separation zone to form a helium rich permeate stream and a retentate stream. The helium rich permeate stream is compressed and introduced into the oxidation system.
摘要翻译：描述了用于提高氦回收率的方法和装置。该方法包括在氧的存在下将含有氦和至少一种可氧化组分的物流引入氧化区，以氧化形成第一蒸气流和第一液流的可氧化组分。将第一蒸气流引入变压吸附区以形成纯化的氦气流和尾气流。尾气流被压缩。将压缩的尾气流引入膜分离区以形成富氦渗透物流和滞留物流。将富氦的渗透物流压缩并引入氧化体系。

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