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21. 发明公开

EP0455489A3 Preparation of a basic aluminium antiperspirant active material having enhanced activity 失效
标题翻译：具有增强活性的基础铝抗菌活性材料，含有这种材料的抗菌活性组合物及其制备方法和组合物
公开(公告)号：EP0455489A3
公开(公告)日：1992-05-13
申请号：EP91303978.0
申请日：1991-05-02
申请人： THE MENNEN COMPANY
发明人： Vincenti, Paul Joseph , Barr, Morton Lawrence
IPC分类号： C01F7/00 , C01F7/66 , A61K7/38 , C01B11/14 , C01B11/18 , C01B11/22 , A61K7/34
CPC分类号： C01F7/66 , A61K8/19 , A61K8/26 , A61K8/28 , A61K8/29 , A61K8/44 , A61K2800/58 , A61Q15/00 , C01B11/14 , C01B11/18 , C01B11/22 , C01F7/48
摘要： Disclosed is a basic aluminum material having enhanced antiperspirant activity, the material having the empirical formula Al₂(OH) 6-a X a , where 0.5 ≦ a ≦ 5.0, and X is a univalent complex oxoanion of nitrogen, chlorine and other halogens, which forms salts with Al³⁺ in aqueous solution so that these salts are essentially completely dissociated, which is readily soluble in water with metallic ions in the solution, and which forms conjugate acids that are strong acids; and wherein the material is characterized by:
(a) size exclusion high performance liquid chromatography peaks corresponding to peak 3 and peak 4 of size exclusion chromatograms formed by HPLC technique; (b) a peak 4 relative area of at least 25%, a peak 3 relative area of less than 60%, the sum of the relative peak 3 and peak 4 areas being at least 50%; and (c) less than 10% chromatographic peaks eluting at shorter retention times than peak 3, corresponding to peaks 1 and 2. Illustratively, the univalent oxoanion can be ClO₃⁻, ClO₄⁻, IO₄⁻, and preferably NO₃⁻. The material is characterized by having et least 25% by weight thereof in the form of Al b polyhydroxyaquoaluminum species. Also disclosed are antiperspirant compositions including the basic aluminum material, a zirconium, hafnium, titanium and/or tin antiperspirant active material and a neutral amino acid, and methods of forming the basic aluminum material and the antiperspirant composition. The basic aluminum material can be formed at relatively low temperatures, without first forming a dilute solution of a basic aluminum compound, and the basic aluminum material has a stable enhanced activity in aqueous solution over a relatively long period of time.

22. 发明申请

WO00075070A1 PROCESS FOR REGENERATING PERIODIC ACID 审中-公开
标题翻译：重现酸性酸的过程
公开(公告)号：WO00075070A1
公开(公告)日：2000-12-14
申请号：PCT/NL2000/000386
申请日：2000-06-07
IPC分类号： C01B11/22 , C08B31/18
CPC分类号： C01B11/22 , C08B31/18
摘要： The invention pertains to a process for the regeneration and recovery of periodate from a spent iodate solution, by reacting the iodate with at least an equimolar amount of hypohalite, and carrying out the recovery in the presence of a water-miscible organic solvent or potassium ions or divalent metal (especially calcium) ions. The regenerated periodate is especially suitable for oxidising carbohydrates to dialdehyde carbohydrates.
摘要翻译：本发明涉及一种通过使碘酸盐与至少等摩尔量的次卤酸盐反应，从废碘酸盐溶液中再生和回收高碘酸盐的方法，并在水混溶性有机溶剂或钾离子存在下进行回收或二价金属（特别是钙）离子。再生高碘酸盐特别适合于将碳水化合物氧化成二醛碳水化合物。

23. 发明申请

WO1998011016A1 METHOD FOR SYNTHESIS OF HYPOHALOUS ACID 审中-公开
标题翻译： HYPOHALOUS酸的合成方法
公开(公告)号：WO1998011016A1
公开(公告)日：1998-03-19
申请号：PCT/US1997015963
申请日：1997-09-10
申请人： THE DOW CHEMICAL COMPANY , QUARDERER, George, J. , TRENT, David, L. , STEWART, Erik, J. , TIRTOWIDJOJO, Danil , MEHTA, Anil, J. , TIRTOWIDJOJO, Cheryl, A.
发明人： THE DOW CHEMICAL COMPANY
IPC分类号： C01B11/04
CPC分类号： C01B11/24 , B01J19/0066 , B01J19/0073 , B01J19/1806 , B01J2219/00103 , C01B11/04 , C01B11/20 , C01B11/22 , Y02P20/149
摘要： This invention is a method for forming hypohalous acid in a mass transfer device. The method comprises: (1) feeding into the device a stream of caustic solution comprising at least one alkali or alkaline earth metal of a hydroxide, oxide, hypohalite, bicarbonate, or carbonate; (2) feeding a stream comprising halogen gas into the device; (3) reacting at least some of the halogen gas with the caustic solution to form a solution containing hypohalous acid; (4) desorbing the hypohalous acid from the solution and into the stream of halogen gas; and (5) removing the stream of halogen gas from the device. In this method, the mass transfer device comprises a porous rotor which is permeable to the streams, and is rotated about an axis such that the streams flow through the rotor and the stream of caustic solution flows radially outward from the axis.
摘要翻译：本发明是在传质装置中形成次卤酸的方法。该方法包括：（1）将包含至少一种氢氧化物，氧化物，次卤酸盐，碳酸氢盐或碳酸盐的碱金属或碱土金属的苛性碱溶液送入该装置; （2）将包含卤素气体的物流送入装置; （3）使至少一些卤素气体与苛性碱溶液反应，形成含有次卤酸的溶液; （4）从溶液中将次卤酸解吸到卤素气流中; 和（5）从装置中除去卤素气流。在该方法中，传质装置包括可流动的多孔转子，并且绕轴旋转，使得流流过转子，并且苛性碱流从轴线径向向外流动。

24. 发明申请

WO2016026130A1 SODIUM ANTI-PEROVSKITE SOLID ELECTROLYTE COMPOSITIONS 审中-公开
标题翻译：钠抗静电固体电解质组合物
公开(公告)号：WO2016026130A1
公开(公告)日：2016-02-25
申请号：PCT/CN2014/084981
申请日：2014-08-22
申请人： THE BOARD OF REGENTS OF THE NEVADA SYSTEM OF HIGHER EDUCATION on behalf of THE UNIVERSITY OF NEVADA, LAS VEGAS , ZHAO, Yusheng , WANG, Yonggang , ZOU, Ruqiang
发明人： ZHAO, Yusheng , WANG, Yonggang , ZOU, Ruqiang
IPC分类号： H01M10/0562 , H01G9/025
CPC分类号： C01D3/04 , C01B11/062 , C01B11/064 , C01B11/20 , C01B11/22 , C01D3/00 , C01D13/00 , C01F5/00 , C01F7/002 , C01F11/00 , C01F17/0012 , C01G9/006 , C01G15/006 , C01P2002/30 , C01P2002/34 , C01P2002/72 , C01P2002/77 , C01P2002/88 , C01P2006/40 , C04B35/5152 , C04B35/62665 , C04B2235/3201 , C04B2235/5436 , C04B2235/768 , C30B11/00 , C30B11/003 , C30B29/12 , H01G9/0036 , H01G9/025 , H01G9/032 , H01M10/054 , H01M10/0562 , H01M2300/0071 , H01M2300/008
摘要： Na-rich electrolyte compositions provided herein can be used in a variety of devices, such as sodium ionic batteries, capacitors and other electrochemical devices. Na-rich electrolyte compositions provided herein can have a chemical formula of Na 3 OX, Na 3 SX, Na (3-δ) M δ/2 OX and Na (3-δ) M δ/2 SX wherein 0 - , CN - , BF 4 - , BH 4 - , ClO 4 - , CH 3 - , NO 2 - , NH 2 - and mixtures thereof, and wherein M is a divalent metal selected from the group consisting of magnesium, calcium, barium, strontium and mixtures thereof. Na-rich electrolyte compositions provided herein can have a chemical formula of Na (3-δ) M δ/3 OX and/or Na (3-δ) M δ/3 SX； wherein 0 +3 , and wherein X is selected from fluoride, chloride, bromide, iodide, H - , CN - , BF 4 - , BH 4 - , ClO 4 - , CH 3 - , NO 2 - , NH 2 - and mixtures thereof. Synthesis and processing methods of NaRAP compositions for battery, capacitor, and other electrochemical applications are also provided.
摘要翻译：本文提供的富含Na的电解质组合物可用于各种装置，例如钠离子电池，电容器和其它电化学装置。本文提供的富钠电解质组合物可以具有化学式Na 3 X 3，Na 3 S X，Na（3-δ）Mδ/ 2X和Na（3-δ）Mδ/ 2SX，其中0 <δ<0.8，其中X是选择的一价阴离子来自氟化物，氯化物，溴化物，碘化物，H，CN-，BF 4 - ，BH 4 - ，ClO 4 - ，CH 3 - ，NO 2 - ，NH 2 - 及其混合物，其中M是二价金属，，钙，钡，锶及其混合物。本文提供的富钠电解质组合物可具有化学式为Na（3-δ）Mδ/ 30X和/或Na（3-δ）Mδ/ 3SX; 其中0 <δ<0.5，其中M是三价阳离子M + 3，其中X选自氟化物，氯化物，溴化物，碘化物，H，CN-，BF 4 - ，BH 4 - ，ClO 4 - ，CH 3 - ，NO 2 - ，NH 2 - 及其混合物。还提供了用于电池，电容器和其它电化学应用的NaRAP组合物的合成和加工方法。

25. 发明申请

WO2004083117A1 パラ過ヨウ素酸二ナトリウムの製造方法审中-公开
标题翻译：制备二磷酸二钠的方法
公开(公告)号：WO2004083117A1
公开(公告)日：2004-09-30
申请号：PCT/JP2004/003491
申请日：2004-03-16
申请人：住友化学工業株式会社 , 吉川享志
发明人：吉川享志
IPC分类号： C01B11/22
CPC分类号： C01B11/22
摘要：ヨウ素酸ナトリウム、ヨウ素酸またはそれらの混合物と次亜塩素酸ナトリウムを水酸化ナトリウムを用いて反応させて生成する反応混合物のｐＨをｐＨ５以上１０以下のｐＨ範囲にすることを特徴とするパラ過ヨウ素酸二ナトリウムの製造方法を提供する。
摘要翻译：一种制备偏高碘酸二钠的方法，其特征在于，将碘酸钠，碘酸或其混合物与次氯酸钠与氢氧化钠反应以提供反应混合物，然后将反应混合物的pH调节至5至10 。

26. 发明申请

US20170275172A1 SODIUM ANTI-PEROVSKITE SOLID ELECTROLYTE COMPOSITIONS 审中-公开
公开(公告)号：US20170275172A1
公开(公告)日：2017-09-28
申请号：US15505890
申请日：2014-08-22
申请人： THE BOARD OF REGENTS OF THE NEVADA SYSTEM OF HIGHER EDUCATION ON BEHALF OF THE UNIVERSITY OF NE
发明人： Yusheng ZHAO , Yonggang WANG , Ruqiang ZOU
IPC分类号： C01D3/04 , H01G9/00 , H01M10/054 , C01B11/22 , C30B29/12 , C30B11/00 , C01B11/06 , C01B11/20 , H01G9/032 , H01M10/0562
CPC分类号： C01D3/04 , C01B11/062 , C01B11/064 , C01B11/20 , C01B11/22 , C01D3/00 , C01D13/00 , C01F5/00 , C01F7/002 , C01F11/00 , C01F17/0012 , C01G9/006 , C01G15/006 , C01P2002/30 , C01P2002/34 , C01P2002/72 , C01P2002/77 , C01P2002/88 , C01P2006/40 , C04B35/5152 , C04B35/62665 , C04B2235/3201 , C04B2235/5436 , C04B2235/768 , C30B11/00 , C30B11/003 , C30B29/12 , H01G9/0036 , H01G9/025 , H01G9/032 , H01M10/054 , H01M10/0562 , H01M2300/0071 , H01M2300/008
摘要： Na-rich electrolyte compositions provided herein can be used in a variety of devices, such as sodium ionic batteries, capacitors and other electrochemical devices. Na-rich electrolyte compositions provided herein can have a chemical formula of Na3OX, Na3SX, Na (3-δ) Mδ/2OX and Na (3-δ) Mδ/2SX wherein 0

27. 发明授权

US06620928B2 Recovery process for spent periodate 失效
公开(公告)号：US06620928B2
公开(公告)日：2003-09-16
申请号：US10013449
申请日：2001-12-13
申请人： Arie Besemer
发明人： Arie Besemer
IPC分类号： C08B3118
CPC分类号： C01B11/22 , C08B31/18
摘要： The invention pertains to a process for the regeneration and recovery of periodate from a spent iodate solution, by reacting the iodate with at least an equimolar amount of peroxosulfate. The regenerated periodate is especially suitable for oxidizing carbohydrates to dialdehyde carbohydrates. The oxidation and regeneration can also be carried out in a single stage using a catalytic amount of periodate only.

28. 发明授权

US6017506A Process for the preparation of periodates 失效
标题翻译：制备高碘酸盐的过程
公开(公告)号：US6017506A
公开(公告)日：2000-01-25
申请号：US181669
申请日：1998-10-29
申请人： Antonius L. B. Dijt , Wilhelmus R. M. Martens , Johan T. Tinge , Jan C. Wisse , Rudolf M. Eder
发明人： Antonius L. B. Dijt , Wilhelmus R. M. Martens , Johan T. Tinge , Jan C. Wisse , Rudolf M. Eder
IPC分类号： A61K33/18 , C01B11/22
CPC分类号： C01B11/22
摘要： Process for the preparation of a sodium paraperiodate wherein an iodine compound is converted into the sodium paraperiodate in the presence of Na.sup.+ ions by means of an alkali metal hydroxide and an alkali metal hypochlorite. The iodine compound is applied in the form of an iodine-containing mixture in which besides the iodine compound in the form of I.sub.2, iodide or iodate compounds, one or more compounds chosen from the group of chlorides, bromides, sulphates, sulphites, carbonates, bicarbonates, nitrates and dissolved organic components are also present. The invention also relates to the preparation of sodium metaperiodate and other alkali and alkali earth metal periodates, wherein the sodium paraperiodate obtained is converted into sodium periodate or into an alkali or alkali earth metal periodate by means of an acid or an alkali and alkali earth metal salt at an elevated temperature. The acid used preferably is HNO.sub.3.
摘要翻译：制备偏高碘酸钠的方法，其中碘化合物通过碱金属氢氧化物和碱金属次氯酸盐在Na +离子存在下转化成偏高碘酸钠。碘化合物以含碘混合物的形式施用，其中除碘，碘化物或碘酸盐化合物形式的碘化合物之外还有一种或多种选自氯化物，溴化物，硫酸盐，亚硫酸盐，碳酸盐，也存在碳酸氢盐，硝酸盐和溶解的有机组分。本发明还涉及偏高碘酸钠和其它碱金属和碱土金属高碘酸钠的制备，其中所得的偏高尿酸钠通过酸或碱和碱土金属转化成高碘酸钠或高碱性碱金属或碱土金属高碘酸盐盐在升高的温度。所使用的酸最好是HNO3。

29. 发明授权

US5595729A Basic aluminum antiperspirant active materials having enhanced activity, antiperspirant active compositions containing such materials, and methods for preparation of such materials and compositions 失效
标题翻译：具有增强活性的碱性铝止汗剂活性物质，含有这些材料的止汗活性组合物，以及制备这种材料和组合物的方法
公开(公告)号：US5595729A
公开(公告)日：1997-01-21
申请号：US97620
申请日：1993-07-27
申请人： Morton L. Barr , Paul J. Vincenti , Elaine L. Vanderhoof
发明人： Morton L. Barr , Paul J. Vincenti , Elaine L. Vanderhoof
IPC分类号： A61K8/19 , A61K8/26 , A61K8/28 , A61K8/29 , A61K8/44 , A61Q15/00 , C01B11/14 , C01B11/18 , C01B11/22 , C01F7/00 , C01F7/48 , C01F7/66 , A61K7/38
CPC分类号： C01F7/66 , A61K8/19 , A61K8/26 , A61K8/28 , A61K8/29 , A61K8/44 , A61Q15/00 , C01B11/14 , C01B11/18 , C01B11/22 , C01F7/002 , C01F7/48 , A61K2800/58 , C01P2002/86 , C01P2002/87
摘要： Disclosed are basic aluminum antiperspirant materials having univalent complex oxoanions (e.g., nitrate); methods of making such materials; antiperspirant compositions containing such basic aluminum materials, another antiperspirant active material (e.g., a basic zirconium halide salt), and optionally a neutral amino acid; and methods of making such compositions. Size exclusion high performance liquid chromatography chromatograms of the disclosed basic aluminum materials have a peak 4 relative area of at least 25%, a peak 3 relative area of less than 60%, the sum of the peaks 3 and 4 being at least 50%; and less than 10% of the chromatographic peaks eluting at peaks 1 and 2. The disclosed basic aluminum materials have less than 25% of the aluminum in the form of Al.sup.b polyhydroxyaquoaluminum, and have a .sup.27 Al NMR spectrum in which the area of the 71.5-73.5 ppm resonance line includes more than 50% of the combined areas of the 62.5-63.5 ppm and 71.5-73.5 ppm resonance lines, and 5%-30% of the total area under the spectrum from 140 ppm to -80 ppm is contained in the resonance line at 71.5-73.5 ppm. The basic aluminum material of the present invention can be produced by adding a stoichiometric or near-stoichiometric amount of aluminum metal to a solution of an aluminum salt having a univalent complex oxoanion; the basic aluminum material can also be made by adding to such solution of the aluminum salt, aluminum metal having, in total, a relatively small surface area (large-sized particles of aluminum).
摘要翻译：公开了具有单价复合氧代阴离子（例如硝酸盐）的碱性止汗剂材料; 制作这种材料的方法; 含有这种碱性铝材料的止汗组合物，另一种止汗剂活性物质（例如碱性卤化锆盐）和任选的中性氨基酸; 以及制备这种组合物的方法。所公开的碱性铝材料的尺寸排阻高效液相色谱色谱图具有至少25％的峰4相对面积，峰3相对面积小于60％，峰3和4的总和至少为50％; 并且在峰1和2处洗脱的色谱峰小于10％。所公开的碱性铝材料具有少于25％的Alb聚羟基铝形式的铝，并且具有27Al NMR谱，其中71.5- 73.5ppm共振线包括62.5-63.5ppm和71.5-73.5ppm共振线的组合面积的50％以上，并且在140ppm至-80ppm的光谱范围内的总面积的5％-30％包含在共振线为71.5-73.5ppm。本发明的碱性铝材料可以通过将化学计量或近化学计量的铝金属加入到具有一价复合氧阴离子的铝盐溶液中来制备; 碱性铝材料也可以通过向铝盐，总共具有相对小的表面积（大尺寸的铝颗粒）的铝金属溶液中加入来制备。

30. 发明授权

US3808310A Process for preparing a composition containing pentacalcium orthoperiodate 失效
标题翻译：制备含有正辛醇钠的组合物的方法
公开(公告)号：US3808310A
公开(公告)日：1974-04-30
申请号：US19550671
申请日：1971-11-03
申请人： MORTON NORWICH PRODUCTS INC
发明人： ANDELFINGER G , KUHAJEK E
IPC分类号： A23K1/175 , C01B11/22 , C01B11/00
CPC分类号： C01B11/22 , A23K20/22 , A23K20/24 , A23K20/30
摘要： THE PREPARATION AND USE OF PENTACALCIUM ORTHOPERIODATE, CA5(IO6)2, IN A SALT BLOCK AND FEEDS AS AN ASSIMILABLE SOURCE OF IODINE FOR THE SUPPLEMENTATION OF THE DIET OF ANIMALS.

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