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21. 发明授权

US5447987A Organopolysiloxane compositions 失效
标题翻译：有机聚硅氧烷组合物
公开(公告)号：US5447987A
公开(公告)日：1995-09-05
申请号：US362948
申请日：1994-12-23
申请人： Shinichi Sato , Takashi Matsuda , Kenichi Fukuda , Tomofumi Sutou
发明人： Shinichi Sato , Takashi Matsuda , Kenichi Fukuda , Tomofumi Sutou
IPC分类号： C08L83/04 , C08K5/54
CPC分类号： C08L83/04 , C08G77/12 , C08G77/20 , C08G77/70
摘要： Organopolysiloxane compositions of the present invention are the curable compositions of the addition curable type, which comprise (A) an organopolysiloxane having aliphatic unsaturated groups, (B) an organohydrogen polysiloxane having SiH groups, (C) a fluorine containing organopolysiloxane expressed by the following general chemical formula (1): ##STR1## wherein R.sup.1, R.sup.2, R.sup.4 through R.sup.6, and R.sup.8 are monovalent hydrocarbon groups such as alkyl groups, R.sup.3 and R.sup.7 are bivalent hydrocarbon groups, such as alkylene groups, Rf is either a perfluoroalkyl group or a perfluoroalkyl ether group, subscripts k, p, and m are integers of at least 1, and the subscript n is an integer of at least 0, and (D) a platinum group metallic catalyst. The cured products obtained from the compositions of the present invention exhibit a superior adhesiveness towards substances to be adhered, such as glass, aluminum, iron and epoxy resins.
摘要翻译：本发明的有机聚硅氧烷组合物是可加成固化型的可固化组合物，其包含（A）具有脂族不饱和基团的有机聚硅氧烷，（B）具有SiH基团的有机氢聚硅氧烷，（C）由以下通式表示的含氟有机聚硅氧烷化学式（1）：nd R8是一价烃基，例如烷基，R 3和R 7是二价烃基，例如亚烷基，R f是全氟烷基或全氟烷基醚基，下标k，p和m是整数为1以上，下标n为0以上的整数，（D）铂族金属催化剂。由本发明组合物获得的固化产物对玻璃，铝，铁和环氧树脂等粘合物质的粘附性显示出优异的表现。

22. 发明授权

US5380811A Fluorine-containing organopolysiloxane composition 失效
标题翻译：含氟有机聚硅氧烷组合物
公开(公告)号：US5380811A
公开(公告)日：1995-01-10
申请号：US70223
申请日：1993-06-02
申请人： Hirofumi Kishita , Shinichi Sato , Noriyuki Koike , Takashi Matsuda
发明人： Hirofumi Kishita , Shinichi Sato , Noriyuki Koike , Takashi Matsuda
IPC分类号： C08L83/14 , C08L83/12
CPC分类号： C08L83/14
摘要： A room temperature curable fluorine-containing organopolysiloxane composition comprising:(A) a fluorine-containing organosilicon compound having the general formula (1):R.sup.2 --NHCO--[Rf--CONH--R.sup.1 --Q--R.sup.1 --NHCO].sub.a --Rf--CONH--R.sup.2 (1) wherein a is an integer of 0 or more, Rf is a divalent perfluoroalkylene group or a divalent perfluoropolyether group, R.sup.1 is a divalent hydrocarbon group, R.sup.2 is a monovalent aliphatic unsaturated group-containing hydrocarbon group, and Q is a divalent siloxane group(B) a hydrogenorganopolysiloxane containing at least two Si--H groups in its molecule, and(C) a platinum family metal catalyst. The cured product of this composition exhibits good solvent resistance against non-polar solvents as well as polar solvents, in addition to good chemical resistance, heat resistance, release properties and water repellency.
摘要翻译：一种室温固化型含氟有机聚硅氧烷组合物，其包含：（A）具有通式（1）的含氟有机硅化合物：R2-NHCO- [Rf-CONH-R1-Q-R1-NHCO] a-Rf-CONH -R2（1）其中a为0以上的整数，Rf为二价全氟亚烷基或二价全氟聚醚基，R 1为二价烃基，R 2为含脂肪族不饱和基团的一价烃基，Q为二价硅氧烷基（B）分子中含有至少两个Si-H基团的氢有机聚硅氧烷，（C）铂族金属催化剂。该组合物的固化产物除了具有良好的耐化学性，耐热性，脱模性和防水性外，对非极性溶剂以及极性溶剂表现出良好的耐溶剂性。

23. 发明授权

US5196560A Process for preparing fluorine-containing dimethylchlorosilanes 失效
标题翻译：制备含氟二甲基氯硅烷的方法
公开(公告)号：US5196560A
公开(公告)日：1993-03-23
申请号：US720705
申请日：1991-06-25
申请人： Shinichi Sato , Hitoshi Kinami , Takashi Matsuda , Hirokazu Yamada
发明人： Shinichi Sato , Hitoshi Kinami , Takashi Matsuda , Hirokazu Yamada
IPC分类号： B01J31/22 , B01J31/24 , C07B61/00 , C07F7/12 , C07F7/14
CPC分类号： C07F7/14
摘要： Fluorine-containing dimethylchlorosilanes are prepared by reacting an ethylene compound having a fluorine-containing organic group with dimethylchlorosilane in the presence of a rhodium complex, for instance RhCl(PPh.sub.3) (Ph: phenyl group), as a catalyst. The use of a rhodium complex as a catalyst enables preparation in high yield of the fluorine-containing dimethylchlorosilane, which has been heretofore obtainable only in low yields.
摘要翻译：含氟二甲基氯硅烷是通过在铑络合物例如RhCl（PPh 3）（Ph：苯基））作为催化剂的存在下使具有含氟有机基团的乙烯化合物与二甲基氯硅烷反应来制备的。使用铑配合物作为催化剂使得能够以高产率制备含氟二甲基氯硅烷，其迄今为止仅以低收率获得。

24. 发明授权

US06576701B2 Fluororubber compositions 失效
标题翻译：氟橡胶组合物
公开(公告)号：US06576701B2
公开(公告)日：2003-06-10
申请号：US09729774
申请日：2000-12-06
申请人： Yasuhisa Osawa , Shinichi Sato , Takashi Matsuda , Makoto Sato
发明人： Yasuhisa Osawa , Shinichi Sato , Takashi Matsuda , Makoto Sato
IPC分类号： C08L2712
CPC分类号： C08K5/5415 , C08G65/007 , C08K5/5425
摘要： A crosslinkable fluororubber composition comprising (A) a perfluoro compound having at least two alkenyl groups and a divalent perfluoroalkylene or perfluoropolyether structure in the backbone or a polymer obtained by adding a compound having at least two hydrosilyl groups in the molecule to some alkenyl groups on the perfluoro compound, (B) a reinforcing filler, (C) a addition reaction crosslinking agent having a hydrosilyl group or a peroxide crosslinking agent, and (D) a surface treating agent having at least one fluoroalkyl or fluoropolyalkyl ether group and silanol groups is improved in heat resistance in the cured state by adding thereto (E) a heat resistance modifier selected from carbon black, metal oxides and metal hydroxides.
摘要翻译：一种交联性氟橡胶组合物，其包含（A）在骨架中具有至少两个烯基和二价全氟亚烷基或全氟聚醚结构的全氟化合物或通过将分子中具有至少两个氢化甲硅烷基的化合物加入到全氟化合物，（B）增强填料，（C）具有氢化硅烷基或过氧化物交联剂的加成反应交联剂，（D）具有至少一个氟代烷基或氟代烷基醚基团和硅烷醇基团的表面处理剂得到改善在固化状态下的耐热性通过加入（E）选自碳黑，金属氧化物和金属氢氧化物的耐热改性剂。

25. 发明授权

US06512041B2 Fluororubber compositions and method of making 有权
标题翻译：氟橡胶组合物和制备方法
公开(公告)号：US06512041B2
公开(公告)日：2003-01-28
申请号：US09929083
申请日：2001-08-15
申请人： Yasuhisa Osawa , Shinichi Sato , Takashi Matsuda
发明人： Yasuhisa Osawa , Shinichi Sato , Takashi Matsuda
IPC分类号： C08K906
CPC分类号： C08G65/336 , C08G65/007 , C08L101/02 , C08L83/00 , C08L2666/54
摘要： A crosslinkable fluororubber composition comprising (A) a polymer comprising a perfluoro compound having at least two alkenyl groups and a divalent perfluoroalkylene or perfluoropolyether structure a compound having at least two hydrosilyl groups, the hydrosilyl-bearing compound being added to some of the alkenyl groups in the perfluoro compound, (B) a reinforcing filler, and (C) a crosslinking agent having a hydrosilyl group and capable of addition reaction or a peroxide crosslinking agent, and (D) a surface treating agent having at least one fluoroalkenyl group and silanol group in the molecule, is roll millable and compression moldable. It cures into products having satisfactory solvent resistance, chemical resistance, heat resistance, and low-temperature properties.
摘要翻译：一种可交联氟橡胶组合物，其包含（A）包含具有至少两个烯基的全氟化合物和二价全氟亚烷基或全氟聚醚结构的聚合物的聚合物，具有至少两个氢化甲硅烷基的化合物，所述含氢硅烷基的化合物加入到一些烯基中全氟化合物，（B）增强填料和（C）具有氢化甲硅烷基且能够进行加成反应的交联剂或过氧化物交联剂，（D）具有至少一个氟烯基和硅烷醇基的表面处理剂在分子中，可辊压可压缩成型。它可以固化成具有令人满意的耐溶剂性，耐化学性，耐热性和低温性能的产品。

26. 发明授权

US06441079B2 Curable fluoropolyether base rubber compositions 有权
标题翻译：可固化氟聚醚基橡胶组合物
公开(公告)号：US06441079B2
公开(公告)日：2002-08-27
申请号：US09754319
申请日：2001-01-05
申请人： Makoto Sato , Takashi Matsuda , Shinichi Sato , Masatoshi Arai
发明人： Makoto Sato , Takashi Matsuda , Shinichi Sato , Masatoshi Arai
IPC分类号： C08K334
CPC分类号： C08K5/5425 , C08G65/007 , C08G65/336 , C08K3/36 , C08K5/5406 , C08L71/00
摘要： A curable fluoropolyether base rubber composition contains (A) 100 parts by weight of a linear fluoropolyether compound having at least two alkenyl groups in a molecule and a perfluoroalkyl ether structure in its backbone, (B) 10-40 parts by weight of a silica filler having a specific surface area of at least 50 m2/g, (C) 5-35 parts by weight of diatomaceous earth, (D) an organosilicon compound having at least two Si—H groups, and (E) a hydrosilylation catalyst. The inclusion of diatomaceous earth is effective for preventing the composition from outgassing and from changing its curing behavior with time.
摘要翻译：可固化的氟聚醚基橡胶组合物含有（A）100重量份的分子中具有至少两个烯基的直链含氟聚醚化合物及其主链中的全氟烷基醚结构，（B）10-40重量份二氧化硅填料具有至少50m 2 / g的比表面积，（C）5-35重量份的硅藻土，（D）具有至少两个Si-H基团的有机硅化合物和（E）氢化硅烷化催化剂。包含硅藻土对于防止组合物逸出并随时间改变其固化行为是有效的。

27. 发明授权

US6020450A Room temperature curable fluoropolymer composition; and fluorine-containing organosilicon compounds, a method of producing the same, and room temperature curable silicone composition containing the same 失效
标题翻译：室温可固化含氟聚合物组合物; 和含氟有机硅化合物，其制备方法和含有它们的室温可固化的有机硅组合物
公开(公告)号：US6020450A
公开(公告)日：2000-02-01
申请号：US204156
申请日：1998-12-03
申请人： Takashi Matsuda , Takafumi Sakamoto , Shinichi Sato , Noriyuki Koike , Yasuo Tarumi , Tsuneo Kimura , Yasushi Yamamoto , Masatoshi Arai
发明人： Takashi Matsuda , Takafumi Sakamoto , Shinichi Sato , Noriyuki Koike , Yasuo Tarumi , Tsuneo Kimura , Yasushi Yamamoto , Masatoshi Arai
IPC分类号： C07F7/18 , C07F7/21 , C08G65/00 , C08G65/336 , C08G77/24
CPC分类号： C08G65/007 , C07F7/1836 , C07F7/184 , C07F7/1896 , C07F7/21 , C08G65/336
摘要： A room temperature curable fluoropolymer composition is provided which comprises (A) a straight chain fluoropolymer compound containing, in its backbone chain, at least one structure selected from a perfluoroalkylene structure and a perfluoropolyether structure and having a hydrolyzable silyl group at both ends of its molecular chain, (B) an organic compound having at least one carbonyl group per molecule, and (C) one compound selected from (C-1) an organic compound having at least one primary amino group per molecule and (C-2) a compound having at least one proton per molecule and having an acid dissociation constant (pKa) in water of 2 or less. Another room temperature curable composition is also provided which comprises said (A) component, (B') an organosilicon compound having at least two silanol groups per molecule, and (C') a condensation accelerator. These compositions are not only excellent in heat resistance, weatherability, electrical properties, processability, chemical resistance, solvent resistance and oil repellant properties, but also excellent in fast curability and deep-portion curability. A novel compound which is suitable as said fluoropolymer compound (A) is further provided.
摘要翻译：提供了一种室温可固化含氟聚合物组合物，其包含（A）在其主链中含有至少一种选自全氟亚烷基结构和全氟聚醚结构的结构并且在其分子的两端具有可水解甲硅烷基的直链含氟聚合物化合物链，（B）每分子具有至少一个羰基的有机化合物，和（C）选自（C-1）每分子具有至少一个伯氨基的有机化合物的化合物和（C-2）化合物每分子具有至少一个质子，并且在水中具有2或更小的酸解离常数（pKa）。还提供了另外的室温固化性组合物，其包含所述（A）成分，（B'）每分子具有至少两个硅烷醇基的有机硅化合物和（C'）缩合促进剂。这些组合物不仅具有优异的耐热性，耐气候性，电性能，加工性，耐化学性，耐溶剂性和防油性，而且具有优异的快速固化性和深部固化性。还提供了适合作为所述含氟聚合物化合物（A）的新型化合物。

28. 发明授权

US5705591A Room temperature curable fluoropolymer composition; and fluorine-containing organosilicon compounds, a method of producing the same, and room temperature curable silicone composition containing the same 失效
公开(公告)号：US5705591A
公开(公告)日：1998-01-06
申请号：US654637
申请日：1996-05-29
申请人： Takashi Matsuda , Takafumi Sakamoto , Shinichi Sato , Noriyuki Koike , Yasuo Tarumi , Tsuneo Kimura , Yasushi Yamamoto , Masatoshi Arai
发明人： Takashi Matsuda , Takafumi Sakamoto , Shinichi Sato , Noriyuki Koike , Yasuo Tarumi , Tsuneo Kimura , Yasushi Yamamoto , Masatoshi Arai
IPC分类号： C07F7/18 , C07F7/21 , C08G65/00 , C08G65/336 , C08G77/54
CPC分类号： C08G65/007 , C07F7/1836 , C07F7/184 , C07F7/1896 , C07F7/21 , C08G65/336
摘要： A room temperature curable fluoropolymer composition is provided which comprises (A) a straight chain fluoropolymer compound containing, in its backbone chain, at least one structure selected from a perfluoroalkylene structure and a perfluoropolyether structure and having a hydrolyzable silyl group at both ends of its molecular chain, (B) an organic compound having at least one carbonyl group per molecule, and (C) one compound selected from (C-1) an organic compound having at least one primary amino group per molecule and (C-2) a compound having at least one proton per molecule and having an acid dissociation constant (pKa) in water of 2 or less. Another room temperature curable composition is also provided which comprises said (A) component, (B') an organosilicon compound having at least two silanol groups per molecule, and (C') a condensation accelerator. These compositions are not only excellent in heat resistance, weatherability, electrical properties, processability, chemical resistance, solvent resistance and oil repellant properties, but also excellent in fast curability and deep-portion curability. A novel compound which is suitable as said fluoropolymer compound (A) is further provided.

29. 发明授权

US5650540A Method of producing amide compound 失效
标题翻译：酰胺化合物的制备方法
公开(公告)号：US5650540A
公开(公告)日：1997-07-22
申请号：US550234
申请日：1995-10-30
申请人： Takashi Matsuda , Shinichi Sato , Noriyuki Koike
发明人： Takashi Matsuda , Shinichi Sato , Noriyuki Koike
IPC分类号： C07C231/02 , C07C231/24 , C07C235/06 , C07C235/16
CPC分类号： C07C231/24 , C07C231/02 , C07C235/06 , C07C235/16
摘要： Provided is a method of producing a highly pure amide compound in a high yield, wherein a silazane compound and/or a silane compound having at least one silicone-nitrogen bond are added to a reaction mixture obtained by reacting an acylfluoride group-containing compound with an amino compound, wherein the amide compound is present together with hydrogen fluroide and/or the amine hydrofluoride, thereby removing the hydrogen fluoride and/or the amine hydrofluoride from the reaction mixture.
摘要翻译：提供一种以高产率制备高纯度酰胺化合物的方法，其中将含有酰基氟化物的化合物与（Ⅳ）反应得到的反应混合物中加入硅氮烷化合物和/或具有至少一个硅氧烷 - 氮键的硅烷化合物氨基化合物，其中酰胺化合物与氢氟酸和/或胺氢氟酸一起存在，从而从反应混合物中除去氟化氢和/或胺氢氟酸。

30. 发明授权

US5461173A Fluorine-containing organosilicon compound and its manufacture 失效
标题翻译：含氟有机硅化合物及其制造方法
公开(公告)号：US5461173A
公开(公告)日：1995-10-24
申请号：US364448
申请日：1994-12-27
申请人： Shinichi Sato , Takashi Matsuda , Takafumi Sakamoto , Masatoshi Arai
发明人： Shinichi Sato , Takashi Matsuda , Takafumi Sakamoto , Masatoshi Arai
IPC分类号： C07F7/08 , C07F7/10 , C07F7/18
CPC分类号： C07F7/0859 , C07F7/0852
摘要： A fluorine-containing organosilicon compound represented by the following general formula (1): ##STR1## wherein Rf represents a perfluoroalkyl group, a perfluorooxyalkyl group, a perfluoroalkylene group, or a perfluorooxyalkylene group, A represents a bivalent organic group, R.sup.1 represents an unsubstituted or substituted monovalent hydrocarbon group, X represents a hydrolyzable group, Y is 1 in the case where the above group Rf represents a perfluoroalkyl group or a perfluorooxyalkyl group or Y is 2 in the case where the above group Rf represents a perfluoroalkylene group or a perfluorooxyalkylene group, m is an integer of 0 to 2, and n is an integer of 1 to 3, with m+n being 3 or less. Since this compound has an acryloyloxy group(s), the compound when irradiated with ultraviolet light can be easily cured within a short period of time, for example, within about 1 to 2 min in the presence of a photopolymerization initiator.
摘要翻译：由以下通式（1）表示的含氟有机硅化合物：其中Rf表示全氟烷基，全氟氧烷基，全氟亚烷基或全氟氧化烯基，A表示二价有机基团，R1 表示未取代或取代的一价烃基，X表示可水解基团，在上述基团Rf表示全氟烷基或全氟氧烷基或Y为2的情况下，Y为1的情况下，上述基团R f表示全氟亚烷基或全氟氧化烯基，m为0〜2的整数，n为1〜3的整数，m + n为3以下。由于该化合物具有丙烯酰氧基，因此在光聚合引发剂存在下，紫外线照射时的化合物可以在短时间内例如约1〜2分钟内容易地固化。

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