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21. 发明申请

US20080019892A1 Multimetal Oxide Containing Silver, Vanadium And A Phosphor Group Element And The Use Thereof 审中-公开
标题翻译：包含银，钒和荧光体组元素的多金属氧化物及其用途
公开(公告)号：US20080019892A1
公开(公告)日：2008-01-24
申请号：US11629379
申请日：2005-06-14
申请人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck , Jurgen Zuhlke
发明人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck , Jurgen Zuhlke
IPC分类号： C01G31/00 , B01J23/00
CPC分类号： C01G31/00 , B01J23/002 , B01J23/682 , B01J27/198 , B01J2523/00 , C01P2002/72 , C01P2002/74 , C01P2006/12 , B01J2523/18 , B01J2523/51 , B01J2523/55
摘要： Multimetal oxides corresponding to the general formula (I), processes for their preparation, precatalysts containing such oxides and catalysts made therefrom for gas phase partial oxidation of hydrocarbons: Aga-cQbMcV12Od.eH2O (I)wherein a represents a number having a value of 5 to 9; Q represents an element selected from the group consisting of P, As, Sb, Bi and mixtures thereof; b represents a number having a value of 0.2 to 3; M represents a metal selected from the group consisting of Li, Na, K, Rb, Cs, Tl, Mg, Ca, Sr, Ba, Cu, Zn, Cd, Pb, Cr, Au, Al, Fe, Co, Ni, Ce, Mn, Nb, W, Ta, Mo and mixtures thereof; c represents a number having a value of less than 1; d represents a number having a value of which is determined by the valency and frequency of Ag, Q, M and V in the formula (I); and e represents a number having a value of 0 to 20; wherein the multimetal oxide has a crystal structure wherein its powder X-ray diffractogram includes reflections at at least 5 interplanar spacings selected from the group of 7.13 Å, 5.52 Å, 5.14 Å, 3.57 Å, 3.25 Å, 2.83 Å, 2.79 Å, 2.73 Å, 2.23 Å and 1.71 Å, each interplanar spacing value±0.04 Å.
摘要翻译：对应于通式（I）的多金属氧化物，其制备方法，含有此类氧化物的预催化剂和由其制备的催化剂用于烃的气相部分氧化：<？in-line-formula description =“In-line Formulas”end =“ 导线“>> Ag C C 其中a表示数值为5〜9的数字，其中a表示0〜5的整数。 Q表示选自P，As，Sb，Bi及其混合物的元素; b表示数值为0.2〜3的数; M表示选自Li，Na，K，Rb，Cs，Tl，Mg，Ca，Sr，Ba，Cu，Zn，Cd，Pb，Cr，Au，Al，Fe，Co，Ni， Ce，Mn，Nb，W，Ta，Mo及其混合物; c表示小于1的数字; d表示数值，其数值由式（I）中Ag，Q，M和V的化合价和频率决定; e表示0〜20的数，其中所述多金属氧化物具有晶体结构，其中其粉末X射线衍射图包括选自7.13，5.52，5.14，3.57，3.25，2.83，2.79，2.73的至少5个面间距的反射 Å，2.23Å和1.71Å，每个晶面间距值±0.04Å。

22. 发明申请

US20070041795A1 Device for the mixing, drying and coating of powdered, granular or moulded bulk material in a fluid bed and method for production of supported catalysts with such a device 审中-公开
公开(公告)号：US20070041795A1
公开(公告)日：2007-02-22
申请号：US10573479
申请日：2004-09-24
申请人： Samuel Neto , Wolfgang Rummel , Sebastian Storck , Jurgen Zuhlke , Frank Rosowski
发明人： Samuel Neto , Wolfgang Rummel , Sebastian Storck , Jurgen Zuhlke , Frank Rosowski
IPC分类号： B65G53/40
CPC分类号： B01J23/002 , B01J2/16 , B01J23/22 , B01J27/199 , B01J35/023 , B01J37/0219 , B01J37/0221 , B01J37/0232 , B01J2523/00 , F26B3/0926 , B01J2523/15 , B01J2523/47 , B01J2523/51 , B01J2523/53 , B01J2523/55
摘要： The invention relates to an apparatus for mixing, drying and coating pulverulent, granular or shaped loose material in a fluidized bed, in particular for use in a process for producing supported catalysts for gas-phase oxidations, which comprises a container (10) for accommodating the loose material, with a bowl-like depression (17) being provided in a lower region (13) of the container (10), a central tube (27) for introducing a gas, with the central tube entering the container in an upper region (12) of the container (10), extending essentially axially downward in the container (10) and opening into the depression (17), an essentially annular deflection shield (29) which is fixed to the central tube (27) in the upper region (12) of the container (10), a guide ring (31) which is located in the lower region (13) of the container (10) and surrounds the central tube (27) essentially concentrically at a distance (L) for part of its length so that a first opening (34) is formed between the wall of the container (10) at the upper edge (22) of the depression and the lower end (33) of the guide ring (31) and a second opening (36) is formed between the deflection shield (29) and the upper edge (35) of the guide ring (31), and means, for example valves (21), for introducing a fluid into the container (10). In the apparatus of the present invention, the outer wall of the central tube (27) is at least partly provided with an adhesion-reducing coating (38). In a preferred embodiment, the distance (L) between the wall of the central tube (27) and the wall of the guide ring (27) is greater than the open height (H3) of the first opening (34). The invention also provides a process for producing supported catalysts using such an apparatus.

23. 发明申请

US20060247446A1 Multi-metal oxide containing silver, vanadium and a promoter metal and use thereof 失效
标题翻译：含有银，钒和助催化剂金属的多金属氧化物及其用途
公开(公告)号：US20060247446A1
公开(公告)日：2006-11-02
申请号：US10566019
申请日：2004-07-23
申请人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck
发明人： Samuel Neto , Hartmut Hibst , Frank Rosowski , Sebastian Storck
IPC分类号： C07D307/89 , C07C51/255 , C07C51/16
CPC分类号： C07C51/313 , B01J23/002 , B01J23/682 , B01J23/688 , B01J35/002 , B01J35/1014 , B01J35/1019 , B01J37/0045 , B01J37/0223 , B01J2523/00 , C01G31/006 , C07C51/265 , C07C63/16 , B01J2523/18 , B01J2523/3712 , B01J2523/55 , B01J2523/72 , B01J2523/47
摘要： A multimetal oxide of the formula I, Aga-cQbMcV2Od*eH2O, I where a is from 0.3 to 1.9, Q is an element selected from among P, As, Sb and/or Bi, is from 0 to 0.3, M is a metal selected from among Nb, Ce, W, Mn, Ta, Pd, Pt, Ru and/or Rh, c is from 0.001 to 0.5, with the proviso that (a-c)≧0.1, d is a number which is determined by the valence and abundance of the elements other than oxygen in the formula I and e is from 0 to 20, and also precatalysts and catalysts produced therefrom for the partial oxidation of aromatic hydrocarbons are described.
摘要翻译：式I的多金属氧化物，<？in-line-formula description =“In-line Formulas”end =“lead”？> Ag ？V V V V V * O O O O O，，------------------------------------- 其中a为0.3〜1.9，Q为选自P，As，Sb和/或Bi的元素，为0〜0.3，M为选自Nb， Ce，W，Mn，Ta，Pd，Pt，Ru和/或Rh，c为0.001至0.5，条件是（ac）> = 0.1，d为由化合价描述了式I中的氧以外的元素和e为0至20，并且还描述了由其制备的用于芳族烃的部分氧化的预催化剂和催化剂。

24. 发明申请

US20080312450A1 Method for Start-Up of Oxidation Catalysts 审中-公开
标题翻译：氧化催化剂启动方法
公开(公告)号：US20080312450A1
公开(公告)日：2008-12-18
申请号：US11994516
申请日：2006-06-30
申请人： Samuel Neto , Frank Rosowski , Sebastian Storck , Juergen Zuehlke , Hans-Martin Allmann , Thomas Lautensack , Rainer Steeg
发明人： Samuel Neto , Frank Rosowski , Sebastian Storck , Juergen Zuehlke , Hans-Martin Allmann , Thomas Lautensack , Rainer Steeg
IPC分类号： C07D213/79 , C07C27/10 , C07D307/60 , C07D307/89 , C07C51/16
CPC分类号： C07D307/34 , B01J23/002 , B01J2523/00 , C07C51/265 , C07C51/313 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55 , B01J2523/824
摘要： Methods comprising: providing an oxidation catalyst bed; and starting up the oxidation catalyst at a temperature of 360° C. to 400° C. with an amount of air of 1.0 to 3.5 standard m3/h and a hydrocarbon loading of 20 to 65 g/standard m3, such that a hot spot having a temperature of 390° C. to
摘要翻译：方法包括：提供氧化催化剂床; 并在360℃至400℃的温度下启动氧化催化剂，空气量为1.0-3.5标准立方米/小时，烃装载量为20至65克/标准立方米，使得热点在催化剂床的前7-20％中形成温度为390℃至<450℃的温度。

25. 发明申请

US20070093384A1 Gas phase oxidation catalyst with defined vanadium oxide particle size distribution 有权
标题翻译：气相氧化催化剂具有规定的氧化钒粒度分布
公开(公告)号：US20070093384A1
公开(公告)日：2007-04-26
申请号：US10573481
申请日：2004-09-24
申请人： Sebastian Storck , Jurgen Zuhlke , Samuel Neto , Frank Rosowski , Wolfgang Rummel
发明人： Sebastian Storck , Jurgen Zuhlke , Samuel Neto , Frank Rosowski , Wolfgang Rummel
IPC分类号： B01J23/22
CPC分类号： C07C51/313 , B01J23/002 , B01J23/22 , B01J27/198 , B01J35/023 , B01J37/0219 , B01J37/0221 , B01J2523/00 , C07C51/265 , C07C63/16 , B01J2523/15 , B01J2523/47 , B01J2523/53 , B01J2523/55
摘要： A process is described for producing a catalyst for gas-phase oxidations, in which a suspension of TiO2 and V2O5 particles is applied to a fluidized inert support, wherein at least 90% by volume of the V2O5 particles have a diameter of 20 μm or less and at least 95% by volume of the V2O5 particles have a diameter of 30 μm or less. The defined particle size distribution of the V2O5 allows a high coating efficiency.
摘要翻译：描述了一种制备用于气相氧化的催化剂的方法，其中施加TiO 2和V 2 O 5 O 5颗粒的悬浮液涉及一种流化惰性载体，其中至少90％（体积）的V 2 O 5 O 3颗粒的直径为20μm或更小，至少95体积％ V 2 O 5颗粒的直径为30μm或更小。 V 2 O 5 O 5的限定的粒度分布允许高涂层效率。

26. 发明授权

US09067187B2 Catalyst system and method for gas phase oxidation using an upstream layer 有权
标题翻译：使用上游层的催化剂体系和气相氧化方法
公开(公告)号：US09067187B2
公开(公告)日：2015-06-30
申请号：US13586963
申请日：2012-08-16
申请人： Hagen Wilmer , Jürgen Zühlke , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Dobner
发明人： Hagen Wilmer , Jürgen Zühlke , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Dobner
IPC分类号： B01J8/06 , B01J8/04 , B01J23/00 , B01J35/00 , B01J35/02 , C07C51/265 , C07C51/31
CPC分类号： B01J8/067 , B01J8/0496 , B01J23/002 , B01J35/0006 , B01J35/026 , B01J2208/024 , B01J2208/025 , C07C51/265 , C07C51/313 , C07C63/16
摘要： The present invention relates to a process for gas-phase oxidation, in which a gaseous stream comprising an aromatic hydrocarbon and molecular oxygen is passed through two or more catalyst zones. Furthermore, the present invention relates to a catalyst system for gas-phase reaction using a preliminary zone.
摘要翻译：本发明涉及一种气相氧化方法，其中包含芳烃和分子氧的气流通过两个或多个催化剂区。此外，本发明涉及使用预备区域进行气相反应的催化剂体系。

27. 发明授权

US08859459B2 Multilayer catalyst for preparing phthalic anhydride and process for preparing phthalic anhydride 有权
标题翻译：制备邻苯二甲酸酐的多层催化剂及邻苯二甲酸酐的制备方法
公开(公告)号：US08859459B2
公开(公告)日：2014-10-14
申请号：US13173736
申请日：2011-06-30
申请人： Stefan Altwasser , Jürgen Zühlke , Hans-Martin Allmann , Frank Rosowski
发明人： Stefan Altwasser , Jürgen Zühlke , Hans-Martin Allmann , Frank Rosowski
IPC分类号： B01J23/04 , B01J27/186 , B01J35/00 , C07D307/89 , B01J27/198 , B01J21/06
CPC分类号： C07D307/89 , B01J21/063 , B01J27/186 , B01J27/198 , B01J35/0006 , B01J35/0073
摘要： The present invention relates to a multilayer catalyst for preparing phthalic anhydride which has a plurality of catalyst layers arranged in succession in the reaction tube, with the individual catalyst layers having alkali metal contents which decrease in the flow direction. The present invention further relates to a process for the oxidation of naphthalene or o-xylene/naphthalene mixtures over such a multilayer catalyst and the use of such multilayer catalysts for the oxidation of naphthalene or o-xylene/naphthalene mixtures to phthalic anhydride.
摘要翻译：本发明涉及一种制备邻苯二甲酸酐的多层催化剂，其具有在反应管中连续排列的多个催化剂层，各个催化剂层具有在流动方向上减少的碱金属含量。本发明还涉及在这种多层催化剂上氧化萘或邻二甲苯/萘混合物的方法，以及使用这种多层催化剂将萘或邻二甲苯/萘混合物氧化成邻苯二甲酸酐。

28. 发明申请

US20130039821A1 CATALYST SYSTEM AND METHOD FOR GAS PHASE OXIDATION USING AN UPSTREAM LAYER 审中-公开
标题翻译：催化剂系统和使用上层层气相氧化的方法
公开(公告)号：US20130039821A1
公开(公告)日：2013-02-14
申请号：US13586963
申请日：2012-08-16
申请人： Hagen Wilmer , Jürgen Zühlke , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Dobner
发明人： Hagen Wilmer , Jürgen Zühlke , Thomas Lautensack , Hans-Martin Allmann , Frank Rosowski , Cornelia Dobner
IPC分类号： B01J8/04
CPC分类号： B01J8/067 , B01J8/0496 , B01J23/002 , B01J35/0006 , B01J35/026 , B01J2208/024 , B01J2208/025 , C07C51/265 , C07C51/313 , C07C63/16
摘要： The present invention relates to a process for gas-phase oxidation, in which a gaseous stream comprising an aromatic hydrocarbon and molecular oxygen is passed through two or more catalyst zones. Furthermore, the present invention relates to a catalyst system for gas-phase reaction using a preliminary zone.
摘要翻译：本发明涉及一种气相氧化方法，其中包含芳烃和分子氧的气流通过两个或多个催化剂区。此外，本发明涉及使用预备区域进行气相反应的催化剂体系。

29. 发明授权

US08323610B2 Catalyst for the oxidation of SO2 to SO3 有权
标题翻译：用于将SO2氧化成SO 3的催化剂
公开(公告)号：US08323610B2
公开(公告)日：2012-12-04
申请号：US13084934
申请日：2011-04-12
申请人： Michael Krämer , Markus Schubert , Thomas Lautensack , Thomas Hill , Reinhard Körner , Frank Rosowski , Jürgen Zühlke
发明人： Michael Krämer , Markus Schubert , Thomas Lautensack , Thomas Hill , Reinhard Körner , Frank Rosowski , Jürgen Zühlke
IPC分类号： C01B17/79 , B01J23/22 , B01J27/053 , B01J37/00 , B01J37/02
CPC分类号： B01J27/055 , B01J21/08 , B01J23/22 , B01J35/023 , B01J37/0018 , B01J37/0201 , C01B17/79
摘要： The invention relates to a catalyst for the oxidation of SO2 to SO3. The catalyst contains an active substance which contains vanadium, alkali metal compounds and sulfate applied to a support. The support contains naturally occurring diatomaceous earth, wherein the support contains at least one relatively soft naturally occurring uncalcined diatomaceous earth which has a percentage reduction of at least 35% in its D50 value determined in a particle size determination according to the dry method in comparison with the wet method.
摘要翻译：本发明涉及用于将SO 2氧化成SO 3的催化剂。催化剂含有一种活性物质，其中含有钒，碱金属化合物和硫酸盐。载体含有天然存在的硅藻土，其中载体含有至少一种相对软的天然存在的未煅烧的硅藻土，其在根据干法测定的颗粒尺寸中测定的D50值的百分比降低至少为35％湿法。

30. 发明申请

US20120004425A1 MULTILAYER CATALYST FOR PREPARING PHTHALIC ANHYDRIDE AND PROCESS FOR PREPARING PHTHALIC ANHYDRIDE 有权
标题翻译：用于制备非离子型氢化物的多层催化剂及其制备方法
公开(公告)号：US20120004425A1
公开(公告)日：2012-01-05
申请号：US13173736
申请日：2011-06-30
申请人： Stefan Altwasser , Jürgen Zühlke , Hans-Martin Allmann , Frank Rosowski
发明人： Stefan Altwasser , Jürgen Zühlke , Hans-Martin Allmann , Frank Rosowski
IPC分类号： C07D307/89 , B01J21/06
CPC分类号： C07D307/89 , B01J21/063 , B01J27/186 , B01J27/198 , B01J35/0006 , B01J35/0073
摘要： The present invention relates to a multilayer catalyst for preparing phthalic anhydride which has a plurality of catalyst layers arranged in succession in the reaction tube, with the individual catalyst layers having alkali metal contents which decrease in the flow direction. The present invention further relates to a process for the oxidation of naphthalene or o-xylene/naphthalene mixtures over such a multilayer catalyst and the use of such multilayer catalysts for the oxidation of naphthalene or o-xylene/naphthalene mixtures to phthalic anhydride.
摘要翻译：本发明涉及一种制备邻苯二甲酸酐的多层催化剂，其具有在反应管中连续排列的多个催化剂层，各个催化剂层具有在流动方向上减少的碱金属含量。本发明还涉及在这种多层催化剂上氧化萘或邻二甲苯/萘混合物的方法，以及使用这种多层催化剂将萘或邻二甲苯/萘混合物氧化成邻苯二甲酸酐。

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