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21. 发明授权

US06777502B2 Rheology modification of polymers prepared using metallocenes 有权
标题翻译：使用金属茂制备的聚合物的流变改性
公开(公告)号：US06777502B2
公开(公告)日：2004-08-17
申请号：US10347713
申请日：2003-01-21
申请人： Thoi H. Ho , Wendy D. Hoenig , Che-l Kao , Michael E. Rowland , Clark H. Cummins , Michael J. Mullins , H. Craig Silvis
发明人： Thoi H. Ho , Wendy D. Hoenig , Che-l Kao , Michael E. Rowland , Clark H. Cummins , Michael J. Mullins , H. Craig Silvis
IPC分类号： C08C1900
CPC分类号： C08L23/02 , C08G81/02 , C08K5/43 , C08L23/04 , C08L23/06 , C08L23/08 , C08L23/0815 , C08L23/0838 , C08L23/0853 , C08L23/16 , C08L2205/22 , C08L2312/00 , C08L2314/06 , Y10T428/1334 , Y10T428/1352 , Y10T428/1386 , Y10T428/139 , Y10T428/31913 , Y10T428/31917 , C08L2666/04
摘要： Coupled polymers are prepared by a process comprising heating an admixture containing (1) at least one polyolefin comprising ethylene and optionally at least one comonomer and (2) a coupling amount at least one poly(sulfonyl azide) to at least the decomposition temperature of the poly(sulfonyl azide) for a period sufficient for decomposition of at least 80 weight percent of the poly(sulfonyl azide) and sufficient to result in a coupled polymer; particularly where the polyolefin is the product of polymerization of ethylene and optionally at least one other alpha-olefin in the presence of a single site catalyst.
摘要翻译：通过包括加热含有（1）至少一种包含乙烯和任选的至少一种共聚单体的聚烯烃和（2）偶联量的至少一种聚（磺酰基叠氮化物）的聚烯烃至少至少分解温度的混合物来制备偶联聚合物聚（磺酰基叠氮化物）足以分解至少80重量％的聚（磺酰基叠氮化物）并足以产生偶联聚合物的时间; 特别是当聚烯烃是在单一位点催化剂存在下乙烯和任选的至少一种其它α-烯烃聚合的产物时。

22. 发明授权

US06627711B2 Transition metal donor complexes and olefin polymerization process 失效
标题翻译：过渡金属给体络合物和烯烃聚合过程
公开(公告)号：US06627711B2
公开(公告)日：2003-09-30
申请号：US10104807
申请日：2002-03-22
申请人： Michael J. Mullins , Phillip S. Athey , Peter N. Nickias , Jorge Soto , Harold W. Boone , R. Vernon Snelgrove
发明人： Michael J. Mullins , Phillip S. Athey , Peter N. Nickias , Jorge Soto , Harold W. Boone , R. Vernon Snelgrove
IPC分类号： C08F464
CPC分类号： C08F110/02 , C08F4/64106
摘要： A process for polymerization of addition polymerizable monomers with a catalyst composition comprising a Group 4 or 5 metal bis(silane)amido complex corresponding to the formula: where the various substituents are as defined in claim 1.
摘要翻译：一种用于使催化剂组合物聚合的方法，所述催化剂组合物包含对应于下式的第4或5族金属双（硅烷）酰胺基络合物：其中各种取代基如权利要求1所定义。

23. 发明授权

US06521306B1 Rheology modification of low density polyethylene 有权
标题翻译：低密度聚乙烯的流变改性
公开(公告)号：US06521306B1
公开(公告)日：2003-02-18
申请号：US09129163
申请日：1998-08-05
申请人： Wendy D. Hoenig , Teresa Karjala , Li-Min Tau , Clark H. Cummins , Michael J. Mullins , H. Craig Silvis , Thoi H. Ho
发明人： Wendy D. Hoenig , Teresa Karjala , Li-Min Tau , Clark H. Cummins , Michael J. Mullins , H. Craig Silvis , Thoi H. Ho
IPC分类号： B29D2200
CPC分类号： C08L23/02 , C08G81/02 , C08K5/43 , C08L23/04 , C08L23/06 , C08L23/08 , C08L23/0815 , C08L23/0838 , C08L23/0853 , C08L23/16 , C08L2205/22 , C08L2312/00 , C08L2314/06 , Y10T428/1334 , Y10T428/1352 , Y10T428/1386 , Y10T428/139 , Y10T428/31913 , Y10T428/31917 , C08L2666/04
摘要： The invention includes a process of preparing a coupled polymer characterized by heating an admixture containing (1) at least one ethylene polymer or blend of ethylene polymers having a density of at least about 0.89 g/mL and less than about 0.935 g/mL and a comonomer content between about 0.5 and 50 weight percent of an alpha olefin having greater than 2 and less than 20 carbon atoms per molecule and (2) a coupling amount of at least one poly(sulfonyl azide) to at least the decomposition temperature of the poly(sulfonyl azide) for a period sufficient for decomposition of at least about 80 weight percent of the poly(sulfonyl azide) and sufficient to result in a coupled polymer. The amount of poly(sulfonyl azide) is preferably from about 0.01 to about 5 weight percent of polymers in the admixture. The invention also includes any composition which is the product of any of the processes of the invention and articles made from those compositions, particularly any film of any composition of the invention. Additionally the invention includes a use of any composition of the invention in a process of blowing, casting or calendaring a film. More particularly the invention includes articles of compositions of the invention which are trash bags, agricultural films, construction films, or geomembranes, grocery sacks, sealant layers, tie layers, produce bags, garment bags, shipping sacks, medical films, stretch films, shrink films, agricultural films, greenhouse films, construction films, or stretch hooders.
摘要翻译：本发明包括一种制备偶联聚合物的方法，其特征在于加热含有（1）至少一种乙烯聚合物或密度为至少约0.89g / mL且小于约0.935g / mL的乙烯聚合物的共混物的混合物，共聚单体含量为约0.5至50重量％的每分子具有大于2个且小于20个碳原子的α-烯烃，和（2）至少一个聚（磺酰基叠氮化物）的偶联量至少达到聚（磺酰基叠氮化物）足以分解至少约80重量％的聚（磺酰基叠氮化物）并足够导致偶联聚合物的时间。聚（磺酰基叠氮化物）的量优选为混合物中约0.01至约5重量％的聚合物。本发明还包括任何组合物，其是本发明任何方法的产物和由这些组合物制成的制品，特别是本发明任何组合物的任何薄膜。此外，本发明包括在吹塑，浇铸或压延膜的方法中使用本发明的任何组合物。更具体地，本发明包括本发明的制品，其为垃圾袋，农用膜，建筑膜或土工膜，杂货袋，密封剂层，连接层，生产袋，服装袋，运输袋，医疗膜，拉伸膜，收缩电影，农膜，温室膜，建筑膜或拉伸罩。

24. 发明授权

US06359073B1 Process of rheology modification of polymers 有权
标题翻译：聚合物流变改性工艺
公开(公告)号：US06359073B1
公开(公告)日：2002-03-19
申请号：US09694649
申请日：2000-10-23
申请人： David A. Babb , Che-I Kao , Wendy D. Hoenig , Michael E. Rowland , Clark H. Cummins , H. Craig Silvis , Michael J. Mullins , Thoi H. Ho
发明人： David A. Babb , Che-I Kao , Wendy D. Hoenig , Michael E. Rowland , Clark H. Cummins , H. Craig Silvis , Michael J. Mullins , Thoi H. Ho
IPC分类号： C08F800
CPC分类号： C08L23/02 , C08G81/02 , C08K5/43 , C08L23/04 , C08L23/06 , C08L23/08 , C08L23/0815 , C08L23/0838 , C08L23/0853 , C08L23/16 , C08L2205/22 , C08L2312/00 , C08L2314/06 , Y10T428/1334 , Y10T428/1352 , Y10T428/1386 , Y10T428/139 , Y10T428/31913 , Y10T428/31917 , C08L2666/04
摘要： The invention includes a process of reacting a poly(sulfonyl azide) with a polymer comprising steps (a) forming a first admixture of a first amount of a first polymer or in a liquid which does not require removal from the polymer and a poly(sulfonyl azide); (b) then forming a second admixture of the first admixture with a second amount of at least one second polymer; and (c) heating the second admixture at lest to the decomposition temperature of the coupling agent for a time sufficient to result in coupling of polymer chains. The invention further includes all compositions obtainable by processes of the invention as well as blends of those compositions with one or more polymers of compositions different from the first or second polymer or the product of a process of the invention. Additionally the invention includes articles made from compositions of the invention, and shaping those articles particularly by processes which comprise shaping the compositions in a melted state into an article, more preferably when the process comprises thermoforming, injection molding, extrusion, casting, blow molding, foaming or blowing as well as the use of the compositions in those processes.
摘要翻译：本发明包括使聚（磺酰基叠氮化物）与聚合物反应的方法，包括步骤（a）形成第一量的第一聚合物的第一混合物或不需要从聚合物中除去的液体和聚（磺酰基叠氮化物）; （b）然后形成第一混合物与第二量的至少一种第二聚合物的第二混合物; 和（c）加热第二混合物至少达到偶联剂的分解温度足以导致聚合物链偶联的时间。本发明还包括可通过本发明的方法获得的所有组合物以及这些组合物与一种或多种不同于第一或第二聚合物或本发明方法的产物的组合物的一种或多种聚合物的共混物。另外，本发明包括由本发明的组合物制成的制品，并且特别通过包括将熔融状态的组合物成型成制品的方法成型那些制品，更优选当该方法包括热成型，注射成型，挤出，浇铸，吹塑成型，发泡或吹塑以及在这些方法中使用组合物。

25. 发明授权

US6013251A Narrow poly-and-mono-dispersed anionic oligomers, and their uses, formulations and processes 失效
标题翻译：窄聚单分散阴离子低聚物及其用途，配方和工艺
公开(公告)号：US6013251A
公开(公告)日：2000-01-11
申请号：US834699
申请日：1997-04-01
申请人： Alan D. Cardin , William A. Fordyce , Michael J. Mullins , Thomas A. Chamberlin , Michael J. Fazio
发明人： Alan D. Cardin , William A. Fordyce , Michael J. Mullins , Thomas A. Chamberlin , Michael J. Fazio
IPC分类号： A61K31/655 , A61K31/17 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/245 , A61K31/66 , A61K31/74 , A61K31/785 , A61K31/795 , A61K31/80 , A61P31/12 , A61P31/18 , C07C69/82 , C07C69/86 , C07C69/96 , C07C309/42 , C07C309/51 , C08G63/16 , C08G63/685 , C08G63/688 , C08G63/692 , C08G64/00 , C08G64/06 , C08G64/08 , C08G69/02 , C08G69/08 , C08G69/10 , C08G69/26 , C08G69/32 , C08G71/02 , A61K31/765
CPC分类号： C08G69/08 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/785 , A61K31/795 , C07C309/51 , C08G63/6856 , C08G63/6886 , C08G63/6926 , C08G64/08 , C08G69/02 , C08G69/10 , C08G69/26 , C08G71/02 , Y10S514/885
摘要： The narrow poly- or mono-dispersed oligomers of the present invention are polyureas, polycarbonates, polyesters or polyamides having a recurring unit of from 3 to 50. These oligomers are water-soluble, preferably have a rigid backbone, have recurring units coupled by carbonyl linking moieties which have anionic groups, display predominantly linear geometry such that regular spacing between anionic groups exists in an aqueous medium, and are pharmaceutically-acceptable. The narrow poly- or mono-dispersed oligomers are useful for the treatment and/or diagnosis of AIDS and/or ARC or HSV.
摘要翻译：本发明的窄聚或单分散低聚物是具有3-50个重复单元的聚脲，聚碳酸酯，聚酯或聚酰胺。这些低聚物是水溶性的，优选具有刚性主链，具有通过羰基连接的重复单元具有阴离子基团的连接部分显示出主要的线性几何形状，使得阴离子基团之间的规则间隔存在于水性介质中，并且是药学上可接受的。窄的聚合或单分散的低聚物可用于治疗和/或诊断AIDS和/或ARC或HSV。

26. 发明授权

US5986044A Narrow poly- and mono-dispersed anionic oligomers 失效
标题翻译：窄聚和单分散阴离子低聚物
公开(公告)号：US5986044A
公开(公告)日：1999-11-16
申请号：US979085
申请日：1997-11-26
申请人： Alan D. Cardin , Michael J. Mullins , William A. Fordyce , Thomas A. Chamberlin , Michael J. Fazio
发明人： Alan D. Cardin , Michael J. Mullins , William A. Fordyce , Thomas A. Chamberlin , Michael J. Fazio
IPC分类号： A61K31/655 , A61K31/17 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/245 , A61K31/66 , A61K31/74 , A61K31/785 , A61K31/795 , A61K31/80 , A61P31/12 , A61P31/18 , C07C69/82 , C07C69/86 , C07C69/96 , C07C309/42 , C07C309/51 , C08G63/16 , C08G63/685 , C08G63/688 , C08G63/692 , C08G64/00 , C08G64/06 , C08G64/08 , C08G69/02 , C08G69/08 , C08G69/10 , C08G69/26 , C08G69/32 , C08G71/02 , A01N33/00
CPC分类号： C08G69/08 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/785 , A61K31/795 , C07C309/51 , C08G63/6856 , C08G63/6886 , C08G63/6926 , C08G64/08 , C08G69/02 , C08G69/10 , C08G69/26 , C08G71/02 , Y10S514/885
摘要： The narrow poly- or mono-dispersed oligomers of the present invention are polyureas, polycarbonates, polyesters or polyamides having a recurring unit of from 3 to 50. These oligomers are water-soluble, preferably have a rigid backbone, have recurring units coupled by carbonyl linking moieties which have anionic groups, display predominantly linear geometry such that regular spacing between anionic groups exists in an aqueous medium, and are pharmaceutically-acceptable. The narrow poly- or mono-dispersed oligomers are useful for the treatment and/or diagnosis of AIDS and/or ARC or HSV.
摘要翻译：本发明的窄聚或单分散低聚物是具有3-50个重复单元的聚脲，聚碳酸酯，聚酯或聚酰胺。这些低聚物是水溶性的，优选具有刚性主链，具有通过羰基连接的重复单元具有阴离子基团的连接部分显示出主要的线性几何形状，使得阴离子基团之间的规则间隔存在于水性介质中，并且是药学上可接受的。窄的聚合或单分散的低聚物可用于治疗和/或诊断AIDS和/或ARC或HSV。

27. 发明授权

US5670143A Anti-HIV pharmaceutical formulations 失效
标题翻译：抗HIV药物制剂
公开(公告)号：US5670143A
公开(公告)日：1997-09-23
申请号：US445192
申请日：1995-05-19
申请人： Alan D. Cardin , Richard L. Jackson , Michael J. Mullins
发明人： Alan D. Cardin , Richard L. Jackson , Michael J. Mullins
IPC分类号： C08G71/02 , A61K20060101 , A61K31/185 , A61K31/74 , A61K31/765 , A61K31/785 , A61K31/795 , A61K49/00 , A61P31/12 , A61P31/18 , C07C309/42 , C07C309/51 , C08G18/00 , C08G18/32 , C08G18/76 , C08G63/02 , C08G63/06 , C08G63/18 , C08G63/19 , C08G63/688 , C08G63/692 , C08G64/00 , C08G64/04 , C08G64/06 , C08G64/08 , C08G64/12 , C08G69/00 , C08G69/26 , C08G69/32 , C08L67/00 , C08L67/02 , C08L69/00
CPC分类号： A61K31/185 , A61K31/785 , A61K31/795 , C07C309/42 , C07C309/51 , C08G63/19 , C08G63/6884 , C08G63/6924 , C08G64/06 , C08G64/081 , C08G64/083 , C08G69/26 , C08G69/32 , C08G71/02 , Y10S514/885
摘要： The preferred oligomers of the present invention are polyureas, polycarbonates, polyesters or polyamides having a number average molecular weight of
摘要翻译：本发明优选的低聚物是数均分子量<10,000的聚脲，聚碳酸酯，聚酯或聚酰胺。这些低聚物是水溶性的，具有刚性主链，具有通过具有阴离子基团的羰基连接部分偶联的重复单元，主要显示出线性几何形式，使得阴离子基团之间的规则间隔存在于水性介质中，并且是药学上可接受的。低聚物可用于治疗和/或诊断AIDS和ARC。

28. 发明授权

US5571505A Anti-HIV oligomers 失效
标题翻译：抗HIV寡聚体
公开(公告)号：US5571505A
公开(公告)日：1996-11-05
申请号：US445158
申请日：1995-05-19
申请人： Alan D. Cardin , Richard L. Jackson , Michael J. Mullins
发明人： Alan D. Cardin , Richard L. Jackson , Michael J. Mullins
IPC分类号： C08G71/02 , A61K20060101 , A61K31/185 , A61K31/74 , A61K31/765 , A61K31/785 , A61K31/795 , A61K49/00 , A61P31/12 , A61P31/18 , C07C309/42 , C07C309/51 , C08G18/00 , C08G18/32 , C08G18/76 , C08G63/02 , C08G63/06 , C08G63/18 , C08G63/19 , C08G63/688 , C08G63/692 , C08G64/00 , C08G64/04 , C08G64/06 , C08G64/08 , C08G64/12 , C08G69/00 , C08G69/26 , C08G69/32 , C08L67/00 , C08L67/02 , C08L69/00
CPC分类号： A61K31/185 , A61K31/785 , A61K31/795 , C07C309/42 , C07C309/51 , C08G63/19 , C08G63/6884 , C08G63/6924 , C08G64/06 , C08G64/081 , C08G64/083 , C08G69/26 , C08G69/32 , C08G71/02 , Y10S514/885
摘要： The preferred oligomers of the present invention are polyureas, polycarbonates, polyesters or polyamides having a number average molecular weight of
摘要翻译：本发明优选的低聚物是数均分子量<10,000的聚脲，聚碳酸酯，聚酯或聚酰胺。这些低聚物是水溶性的，具有刚性主链，具有通过具有阴离子基团的羰基连接部分偶联的重复单元，主要显示出线性几何形式，使得阴离子基团之间的规则间隔存在于水性介质中，并且是药学上可接受的。低聚物可用于治疗和/或诊断AIDS和ARC。

29. 发明授权

US5512177A Narrow poly- and mono-dispersed anoinic oligomers, and their uses, formulations and process 失效
标题翻译：窄聚和单分散的无嗅低聚物及其用途，配方和工艺
公开(公告)号：US5512177A
公开(公告)日：1996-04-30
申请号：US156329
申请日：1993-11-22
申请人： Alan D. Cardin , Michael J. Mullins , William A. Fordyce , Thomas A. Chamberlin , Michael J. Fazio
发明人： Alan D. Cardin , Michael J. Mullins , William A. Fordyce , Thomas A. Chamberlin , Michael J. Fazio
IPC分类号： A61K31/655 , A61K31/17 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/245 , A61K31/66 , A61K31/74 , A61K31/785 , A61K31/795 , A61K31/80 , A61P31/12 , A61P31/18 , C07C69/82 , C07C69/86 , C07C69/96 , C07C309/42 , C07C309/51 , C08G63/16 , C08G63/685 , C08G63/688 , C08G63/692 , C08G64/00 , C08G64/06 , C08G64/08 , C08G69/02 , C08G69/08 , C08G69/10 , C08G69/26 , C08G69/32 , C08G71/02 , B01D15/08 , B07C9/00
CPC分类号： C08G69/08 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/785 , A61K31/795 , C07C309/51 , C08G63/6856 , C08G63/6886 , C08G63/6926 , C08G64/08 , C08G69/02 , C08G69/10 , C08G69/26 , C08G71/02 , Y10S514/885
摘要： The narrow poly- or mono-dispersed oligomers of the present invention are polyureas, polycarbonates, polyesters or polyamides having a recurring unit of from 3 to 50. These oligomers are water-soluble, preferably have a rigid backbone, have recurring units coupled by carbonyl linking moities which have anionic groups, display predominantly linear geometry such that regular spacing between anionic groups exists in an aqueous medium, and are pharmaceutically-acceptable. The narrow poly- or mono-dispersed oligomers are useful for the treatment and/or diagnosis of AIDS and/or ARC or HSV.
摘要翻译：本发明的窄聚或单分散低聚物是具有3-50个重复单元的聚脲，聚碳酸酯，聚酯或聚酰胺。这些低聚物是水溶性的，优选具有刚性主链，具有通过羰基连接的重复单元具有阴离子基团的连接单元显示出主要的线性几何形状，使得阴离子基团之间的规则间隔存在于水性介质中，并且是药学上可接受的。窄的聚合或单分散的低聚物可用于治疗和/或诊断AIDS和/或ARC或HSV。

30. 发明授权

US5424063A Narrow poly- and mono-dispersed anionic oligomers, and their uses, formulations and process 失效
标题翻译：窄聚和单分散阴离子低聚物及其用途，配方和工艺
公开(公告)号：US5424063A
公开(公告)日：1995-06-13
申请号：US818753
申请日：1992-01-09
申请人： Alan D. Cardin , William A. Fordyce , Michael J. Mullins , Thomas A. Chamberlin , Michael J. Fazio
发明人： Alan D. Cardin , William A. Fordyce , Michael J. Mullins , Thomas A. Chamberlin , Michael J. Fazio
IPC分类号： A61K31/655 , A61K31/17 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/245 , A61K31/66 , A61K31/74 , A61K31/785 , A61K31/795 , A61K31/80 , A61P31/12 , A61P31/18 , C07C69/82 , C07C69/86 , C07C69/96 , C07C309/42 , C07C309/51 , C08G63/16 , C08G63/685 , C08G63/688 , C08G63/692 , C08G64/00 , C08G64/06 , C08G64/08 , C08G69/02 , C08G69/08 , C08G69/10 , C08G69/26 , C08G69/32 , C08G71/02 , A01N33/00
CPC分类号： C08G69/08 , A61K31/185 , A61K31/216 , A61K31/235 , A61K31/785 , A61K31/795 , C07C309/51 , C08G63/6856 , C08G63/6886 , C08G63/6926 , C08G64/08 , C08G69/02 , C08G69/10 , C08G69/26 , C08G71/02 , Y10S514/885
摘要： The narrow poly- or mono-dispersed oligomers of the present invention are polyureas, polycarbonates, polyesters or polyamides having a recurring unit of from 3 to 50. These oligomers are water-soluble, preferably have a rigid backbone, have recurring units coupled by carbonyl linking moieties which have anionic groups, display predominantly linear geometry such that regular spacing between anionic groups exists in an aqueous medium, and are pharmaceutically-acceptable. The narrow poly- or mono-dispersed oligomers are useful for the treatment and/or diagnosis of AIDS and/or ARC or HSV.
摘要翻译：本发明的窄聚或单分散低聚物是具有3-50个重复单元的聚脲，聚碳酸酯，聚酯或聚酰胺。这些低聚物是水溶性的，优选具有刚性主链，具有通过羰基连接的重复单元具有阴离子基团的连接部分显示出主要的线性几何形状，使得阴离子基团之间的规则间隔存在于水性介质中，并且是药学上可接受的。窄的聚合或单分散的低聚物可用于治疗和/或诊断AIDS和/或ARC或HSV。

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