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21. 发明申请

US20080300376A1 Method for the Production of Multimetal Cyanide Compounds 失效
公开(公告)号：US20080300376A1
公开(公告)日：2008-12-04
申请号：US12095805
申请日：2006-11-23
申请人： Michael Triller , Raimund Ruppel
发明人： Michael Triller , Raimund Ruppel
IPC分类号： C08G18/22 , C07F15/06
CPC分类号： B01J27/26 , B01J27/02 , B01J37/0201 , B01J37/30 , C08G18/4866 , C08G65/2663
摘要： Process for preparing multimetal cyanide compounds, which comprises the stepsa) reaction of the aqueous solution of a metal salt of the general formula (I) M1gXn (I) with the aqueous solution of a cyanometalate compound of the general formula (II) M3r[M2(CN)b]d, , (II) if appropriate in the presence of organic ligands, organic additives and/or surface-active agents,to form a multimetal cyanide compound of the general formula (III) M1a[M2(CN)b]d.fM1jXk.h(H2O).eL.zP (III) b) reaction of the multimetal cyanide compound of the general formula (III) with a salt of the general formula (IV) M4sYt , (IV) which is different from (II) whereM1 is a metal ion selected from the group consisting of Zn2+, Fe2+, Fe3+, Co2+, Co3+, Ni2+, Mn2+, Sn2+, Sn4+, Pb2+, Al3+, Sr2+, Cr3+, Cd2+, Cu2+, La3+, Ce3+, Ce4+, Eu3+, Mg2+, Ti4+, Ag+, Rh2+, Ru2+, Ru3+, Pd2+M2 is a metal ion selected from the group consisting of Fe2+, Fe3+, Co2+, Co3+, Mn2+, Mn3+, Ni2+, Cr2+, Cr3+, Rh3+, Ru2+, Ir3+and M1 and M2 are identical or different,X is an anion, selected from the group consisting of halide, hydroxide, sulfate, hydrogensulfate, carbonate, hydrogencarbonate, cyanide, thiocyanate, isocyanate, cyanate, carboxylate, oxalate, nitrate and nitrite (NO2—) or a mixture of two or more of the abovementioned anions or a mixture of one or more of the abovementioned anions with an uncharged species selected from among CO, H2O and NO,Y is an anion which is different from X and is selected from the group consisting of halide, sulfate, hydrogensulfate, disulfate, sulfite, sulfonate, (═RSO3—where R═C1-C20-alkyl, aryl, C1-C2-alkylaryl), carbonate, hydrogencarbonate, cyanide, thiocyanate, isocyanate, isothiocyanate, cyanate, carboxylate, oxalate, nitrate, nitrite, phosphate, hydrogenphosphate, dihydrogenphosphate, diphosphate, borate, tetraborate, perchlorate, tetrafluoroborate, hexafluorophosphate, tetraphenylborate,L is a water-miscible ligand selected from the group consisting of alcohols, aldehydes, ketones, ethers, polyethers, esters, polyesters, polycarbonate, ureas, amides, nitriles, and sulfides and mixtures thereof,P is an organic additive, selected from the group consisting of polyethers, polyesters, polycarbonates, polyalkylene glycol sorbitan esters, polyalkylene glycol glycidyl ethers, polyacrylamide, poly(acrylamide-co-acrylic acid), polyacrylic acid, poly(acrylamide-co-maleic acid), polyacrylonitrile, polyalkyl acrylate, polyalkyl methacrylate, polyvinyl methyl ether, polyvinyl ethyl ether, polyvinyl acetate, polyvinyl alcohol, poly-N-vinylpyrrolidone, poly(N-vinylpyrrolidone-co-acrylic acid), polyvinyl methyl ketone, poly(4-vinylphenol), poly(acrylic acid-co-styrene), oxazoline polymers, polyalkylenimines, maleic acid and maleic anhydride copolymers, hydroxyethylcellulose, polyacetates, ionic surface- and interface-active compounds, bile acids, and their salts, esters and amides, carboxylic esters of polyhydric alcohols and glycosides,anda, b, d, g, n, r, s, j, k and t are integers or fractions greater than zero,e, f, h and z are integers or fractions greater than or equal to zerowherea, b, d, g, n, j, k and r and also s and t are selected so that the compound is electrically neutral,M3 is hydrogen or an alkali metal or alkaline earth metal, andM4 is an alkali metal ion or an ammonium ion (NH4+) or an alkylammonium ion (R4N+, R3NH+, R2NH2+, RNH3+ where R═C1-C20-alkyl).

22. 发明授权

US08119825B2 Method for the production of multimetal cyanide compounds 失效
标题翻译：生产多金属氰化物的方法
公开(公告)号：US08119825B2
公开(公告)日：2012-02-21
申请号：US12095805
申请日：2006-11-23
申请人： Michael Triller , Raimund Ruppel
发明人： Michael Triller , Raimund Ruppel
IPC分类号： C07F15/00 , C01B21/06 , C08G18/00
CPC分类号： B01J27/26 , B01J27/02 , B01J37/0201 , B01J37/30 , C08G18/4866 , C08G65/2663
摘要： Process for preparing multimetal cyanide compounds, which comprises the steps a) reaction of the aqueous solution of a metal salt of the general formula (I) M1gXn (I) With the aqueous solution of a cyanometalate compound of the general formula (II) M3r[M2(CN)b]d, (II), If appropriate in the presence of organic ligands, organic additives and/or surface-active agents, to form a multimetal cyanide compound of the general formula (III) M1a[M2(CN)b]d.fM1jXk.h(H2O).eL.zP (III) b) reaction of the multimetal cyanide compound of the general formula (III) with a salt of the general formula (IV) M4sYt (IV) which is different from general formula (II) where M1, M2, M3, M4, X, L, P, Y, g, n, r, b, d, a, f, j, k, h, e, z, s, and t are defined in the specification.
摘要翻译：制备多金属氰化合物的方法，其包括步骤a）通式（I）的化合物M1gXn（I）的水溶液与通式（II）的氰基金属化合物的水溶液反应， M2（CN）b] d，（II）如果在有机配体，有机添加剂和/或表面活性剂存在下适当，形成通式（III）的多金属氰化物M1a [M2（CN） b）d.fM1jXk.h（H2O）.eL.zP（III）b）通式（III）的多金属氰化合物与通式（IV）的盐与M4sYt（IV）不同的反应通式（II）其中M1，M2，M3，M4，X，L，P，Y，g，n，r，b，d，a，f，j，k，h，e，z，s和t 在规范中定义。

23. 发明授权

US08362099B2 Method for producing polyrethane soft foam materials 失效
标题翻译：聚氨酯软泡沫材料的制造方法
公开(公告)号：US08362099B2
公开(公告)日：2013-01-29
申请号：US11574898
申请日：2005-09-20
申请人： Kathrin Harre , Inge Rotermund , Raimund Ruppel , Berend Eling
发明人： Kathrin Harre , Inge Rotermund , Raimund Ruppel , Berend Eling
IPC分类号： C08G18/28
CPC分类号： C08G18/4812 , C08G18/12 , C08G18/4072 , C08G18/4837 , C08G18/4866 , C08G65/2663 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G18/40
摘要： Process for producing flexible polyurethane foams in particular molded flexible polyurethane foams, by reacting a) polyisocyanates with b) compounds having at least two hydrogen atoms which are reactive toward isocyanate groups, wherein the component b) comprises b1a) at least one polyether alcohol having an end block of ethylene oxide units which has been added on by means of DMC catalysis and makes up not more than 10% by weight of the weight of the alkylene oxide added on by means of DMC catalysis, and/or b1b) at least one polyether alcohol comprising a terminal mixture of ethylene oxide and propylene oxide which has been added on by means of DMC catalysis and has an ethylene oxide content in the mixture of at least 25% by weight, and also b2a) at least one polyether alcohol or comprising exclusively propylene oxide units, and/or b2b) at least one graft polyether alcohol.
摘要翻译：通过使a）多异氰酸酯与b）具有至少两个对异氰酸酯基团具有反应性的氢原子的化合物来制备柔性聚氨酯泡沫，特别是模制的柔性聚氨酯泡沫的方法，其中组分b）包含b1a）至少一种具有通过DMC催化加成的环氧乙烷单元的末端嵌段，并且通过DMC催化加成不超过10重量％的加成环氧烷烃的重量，和/或b1b）至少一种聚醚醇，其包含环氧乙烷和环氧丙烷的末端混合物，其已经通过DMC催化加入并且其混合物中的环氧乙烷含量为至少25重量％，并且还包含至少一种聚醚醇，或者包括至少一种聚醚醇环氧丙烷单元和/或b2b）至少一种接枝聚醚醇。

24. 发明申请

US20080161509A1 Method for Production of Polyether Alcohols 失效
标题翻译：制备聚醚醇的方法
公开(公告)号：US20080161509A1
公开(公告)日：2008-07-03
申请号：US11997589
申请日：2006-08-21
申请人： Thomas Ostrowski , Achim Loffler , Raimund Ruppel
发明人： Thomas Ostrowski , Achim Loffler , Raimund Ruppel
IPC分类号： C08F2/01
CPC分类号： C08G65/2663 , C08G65/2696
摘要： The invention provides a process for preparing polyether alcohols by adding alkylene oxides onto H-functional starter substances using DMC catalysts, which comprises, in a first step, adding propylene oxide or a mixture of propylene oxide and ethylene oxide onto H-functional starter substances and, in a second step, transferring the product thus formed into a tubular reactor in which mixtures of ethylene oxide and propylene oxide are metered in at least two metering points, the proportions of ethylene oxide and propylene oxide in the mixtures metered in in the first and in the second step being different, the proportions of ethylene oxide and propylene oxide in the mixtures metered in at least two metering points in the second step being different, and the mixture metered in in the second step, at least at the last metering point, comprising at least 40% by weight of ethylene oxide.
摘要翻译：本发明提供了一种通过使用DMC催化剂将烯化氧加成到H官能起始物质上制备聚醚醇的方法，该方法包括在第一步骤中将环氧丙烷或环氧丙烷与环氧乙烷的混合物加入到H官能起始物质中，在第二步中，将由此形成的产物转移到管式反应器中，其中在至少两个计量点中计量环氧乙烷和环氧丙烷的混合物，在第一和第二步中计量的混合物中的环氧乙烷和环氧丙烷的比例在第二步是不同的情况下，在第二步中至少两个计量点中计量的混合物中的环氧乙烷和环氧丙烷的比例是不同的，并且在第二步中计量的混合物至少在最后一个计量点，包含至少40重量％的环氧乙烷。

25. 发明授权

US07625954B2 Method for producing polyurethane-soft foam materials 失效
标题翻译：生产聚氨酯软泡沫材料的方法
公开(公告)号：US07625954B2
公开(公告)日：2009-12-01
申请号：US11575165
申请日：2005-09-20
申请人： Kathrin Harre , Raimund Ruppel , Berend Eling
发明人： Kathrin Harre , Raimund Ruppel , Berend Eling
IPC分类号： C08G18/28
CPC分类号： C08G18/4072 , C08G18/10 , C08G18/4837 , C08G18/4866 , C08G18/7664 , C08G65/2663 , C08G65/2696 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G18/48 , C08G18/40
摘要： The invention relates to a process for producing flexible polyurethane foams, in particular molded flexible polyurethane foams, by reacting a) polyisocyanates with b) compounds having at least two hydrogen atoms which are reactive toward isocyanate groups, wherein at least one polyether alcohol bi) which has been prepared by means of a DMC catalyst and has a hydroxyl number in the range from 15 to 35 mg KOH/g, and ethylene oxide content in the range from 5 to 18% by weight, based on the total weight of the polyether alcohol and an end block of ethylene oxide and propylene oxide having an ethylene oxide content of from 25 to 75% by weight, based on the amount of alkylene oxide in the end block, is used as compound b) having at least two hydrogen atoms which are reactive toward isocyanate groups.
摘要翻译：本发明涉及通过使a）多异氰酸酯与b）具有至少两个对异氰酸酯基反应的氢原子的化合物来生产柔性聚氨酯泡沫，特别是模制柔性聚氨酯泡沫的方法，其中至少一种聚醚醇bi）已经通过DMC催化剂制备，羟值为15至35mg KOH / g，环氧乙烷含量为5至18重量％，基于聚醚醇的总重量并且使用环氧乙烷和环氧丙烷的端嵌段，其具有25至75重量％的环氧乙烷含量，基于端嵌段中的环氧烷烃的量，作为具有至少两个氢原子的化合物b），其为对异氰酸酯基反应。

26. 发明授权

US07528288B2 Method for production of polyether alcohols 失效
标题翻译：聚醚醇的生产方法
公开(公告)号：US07528288B2
公开(公告)日：2009-05-05
申请号：US11997589
申请日：2006-08-21
申请人： Thomas Ostrowski , Achim Loeffler , Raimund Ruppel
发明人： Thomas Ostrowski , Achim Loeffler , Raimund Ruppel
IPC分类号： C07C43/00
CPC分类号： C08G65/2663 , C08G65/2696
摘要： The invention provides a process for preparing polyether alcohols by adding alkylene oxides onto H-functional starter substances using DMC catalysts, which comprises, in a first step, adding propylene oxide or a mixture of propylene oxide and ethylene oxide onto H-functional starter substances and, in a second step, transferring the product thus formed into a tubular reactor in which mixtures of ethylene oxide and propylene oxide are metered in at least two metering points, the proportions of ethylene oxide and propylene oxide in the mixtures metered in in the first and in the second step being different, the proportions of ethylene oxide and propylene oxide in the mixtures metered in at least two metering points in the second step being different, and the mixture metered in in the second step, at least at the last metering point, comprising at least 40% by weight of ethylene oxide.
摘要翻译：本发明提供了一种通过使用DMC催化剂将烯化氧加成到H官能起始物质上制备聚醚醇的方法，该方法包括在第一步骤中将环氧丙烷或环氧丙烷与环氧乙烷的混合物加入到H官能起始物质中，在第二步中，将由此形成的产物转移到管式反应器中，其中在至少两个计量点中计量环氧乙烷和环氧丙烷的混合物，在第一和第二步中计量的混合物中的环氧乙烷和环氧丙烷的比例在第二步是不同的情况下，在第二步中至少两个计量点中计量的混合物中的环氧乙烷和环氧丙烷的比例是不同的，并且在第二步中计量的混合物至少在最后一个计量点，包含至少40重量％的环氧乙烷。

27. 发明申请

US20070282028A1 Method for Producing Polyurethane-Soft Foam Materials 失效
标题翻译：聚氨酯软泡沫材料的生产方法
公开(公告)号：US20070282028A1
公开(公告)日：2007-12-06
申请号：US11575165
申请日：2005-09-20
申请人： Kathrin Harre , Raimund Ruppel , Berend Eling
发明人： Kathrin Harre , Raimund Ruppel , Berend Eling
IPC分类号： C08G18/48
CPC分类号： C08G18/4072 , C08G18/10 , C08G18/4837 , C08G18/4866 , C08G18/7664 , C08G65/2663 , C08G65/2696 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G18/48 , C08G18/40
摘要： The invention relates to a process for producing flexible polyurethane foams, in particular molded flexible polyurethane foams, by reacting a) polyisocyanates with b) compounds having at least two hydrogen atoms which are reactive toward isocyanate groups, wherein at least one polyether alcohol bi) which has been prepared by means of a DMC catalyst and has a hydroxyl number in the range from 15 to 35 mg KOH/g, and ethylene oxide content in the range from 5 to 18% by weight, based on the total weight of the polyether alcohol and an end block of ethylene oxide and propylene oxide having an ethylene oxide content of from 25 to 75% by weight, based on the amount of alkylene oxide in the end block, is used as compound b) having at least two hydrogen atoms which are reactive toward isocyanate groups.
摘要翻译：本发明涉及通过使a）多异氰酸酯与b）具有至少两个对异氰酸酯基反应的氢原子的化合物来生产柔性聚氨酯泡沫，特别是模制柔性聚氨酯泡沫的方法，其中至少一种聚醚醇bi）已经通过DMC催化剂制备，羟值为15至35mg KOH / g，环氧乙烷含量为5至18重量％，基于聚醚醇的总重量并且使用环氧乙烷和环氧丙烷的端嵌段，其具有25至75重量％的环氧乙烷含量，基于端嵌段中的环氧烷烃的量，作为具有至少两个氢原子的化合物b），其为对异氰酸酯基反应。

28. 发明申请

US20070219282A1 Method for Producing Polyrethane Soft Foam Matrials 失效
标题翻译：生产聚氨酯软泡沫材料的方法
公开(公告)号：US20070219282A1
公开(公告)日：2007-09-20
申请号：US11574898
申请日：2005-09-20
申请人： Kathrin Harre , Inge Rotermund , Raimund Ruppel , Berend Eling
发明人： Kathrin Harre , Inge Rotermund , Raimund Ruppel , Berend Eling
IPC分类号： C08G18/00
CPC分类号： C08G18/4812 , C08G18/12 , C08G18/4072 , C08G18/4837 , C08G18/4866 , C08G65/2663 , C08G2101/0008 , C08G2101/005 , C08G2101/0083 , C08G18/40
摘要： Process for producing flexible polyurethane foams in particular molded flexible polyurethane foams, by reacting a) polyisocyanates with b) compounds having at least two hydrogen atoms which are reactive toward isocyanate groups, wherein the component b) or comprises b1a) at least one polyether alcohol having an end block of ethylene oxide units which has been added on by means of DMC catalysis and makes up not more than 10% by weight of the weight of the alkylene oxide added on by means of DMC catalysis, and/or b1b) at least one polyether alcohol comprising a terminal mixture of ethylene oxide and propylene oxide which has been added on by means of DMC catalysis and has a n ethylene oxide content in the mixture of at least 25% by weight, and also b2a) at least one polyether alcohol or comprising exclusively propylene oxide units. and/or b2b) at least one graft polyether alcohol.
摘要翻译：通过使a）多异氰酸酯与b）具有至少两个对异氰酸酯基团具有反应性的氢原子的化合物来制备柔性聚氨酯泡沫，特别是模制的柔性聚氨酯泡沫的方法，其中组分b）或包含b1a）至少一种具有已经通过DMC催化加入的环氧乙烷单元的末端嵌段，并且通过DMC催化加成不超过10重量％的加成的环氧烷烃的重量，和/或b1b）至少一个聚醚醇，其包含通过DMC催化加入的环氧乙烷和环氧丙烷的末端混合物，并且其混合物中的环氧乙烷含量为至少25重量％，并且还包含至少一种聚醚醇，或包含至少一种聚醚醇专用环氧丙烷单元。和/或b2b）至少一种接枝聚醚醇。

29. 发明申请

US20060167209A1 Production of polyether alcohols by usig dmc catalysis 审中-公开
标题翻译：通过使用催化剂生产聚醚醇
公开(公告)号：US20060167209A1
公开(公告)日：2006-07-27
申请号：US10559073
申请日：2004-06-03
申请人： Thomas Ostrowski , Raimund Ruppel , Eva Baun , Kathrin Harre
发明人： Thomas Ostrowski , Raimund Ruppel , Eva Baun , Kathrin Harre
IPC分类号： C08G18/32 , C08G65/30 , B32B27/40
CPC分类号： C08G65/30 , C08G65/2663
摘要： The present invention relates to polyetherols are prepared by a process comprising the reaction of at least one alkylene oxide with at least one initiator compound in the presence of at least one double metal cyanide compound to give a polyetherol and the treatment of the resulting polyetherol with steam or with an inert gas and steam, and the polyetherols obtainable by such a process as well as the use thereof for the synthesis of polyurethanes.
摘要翻译：本发明涉及通过包括至少一种烯化氧与至少一种引发剂化合物在至少一种双金属氰化物化合物的存在下反应以产生聚乙烯醇并用蒸汽处理得到的聚乙烯醇的方法制备的聚醚或惰性气体和蒸汽，以及可通过这种方法获得的聚醚，以及其用于合成聚氨酯的用途。

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