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21. 发明授权

US5094831A Process for the dismutation of chlorosilanes 失效
标题翻译：分离氯霉素的方法
公开(公告)号：US5094831A
公开(公告)日：1992-03-10
申请号：US558868
申请日：1990-07-30
申请人： Hans-Juergen Klockner , Peter Panster , Peter Kleinschmit
发明人： Hans-Juergen Klockner , Peter Panster , Peter Kleinschmit
IPC分类号： B01J31/06 , C01B33/04 , C01B33/107 , C07F7/12
CPC分类号： C01B33/10773 , C01B33/043
摘要： A process for the dismutation of chlorosilanes is disclosed in which the latter are in the gas phase for 0.01-100 sec. at 55.degree.-100.degree. C. or in the liquid phase for 1-1000 sec. at 25.degree.-55.degree. C. conducted in the presence of a catalyst, which is either unformed or is present in the form of spherical pellets, and which consists of one of four different organopolysiloxane compounds, optionally cross-linked, which essentially carry an amino or ammonium group as a functional group.
摘要翻译：公开了一种用于歧化氯硅烷的方法，其中后者在气相中为0.01-100秒。在55°-100℃或液相中1-1000秒。在25℃-55℃下，在催化剂存在下进行，该催化剂是未成型的或以球形颗粒的形式存在，并且由四种不同的有机聚硅氧烷化合物之一组成，任选地交联，其基本上携带氨基或铵基作为官能团。

22. 发明授权

US5049690A N,N'-disubstituted and N,N,N'-/N,N', N'-trisubstituted thioureas and method of their preparation (II) 失效
标题翻译： N，N'-二取代和N，N，N' - / N，N'，N'-三取代硫脲及其制备方法（II）
公开(公告)号：US5049690A
公开(公告)日：1991-09-17
申请号：US556544
申请日：1990-07-24
申请人： Ulrich Deschler , Peter Panster , Peter Kleinschmit
发明人： Ulrich Deschler , Peter Panster , Peter Kleinschmit
IPC分类号： C07F7/10 , C07F7/18
CPC分类号： C07F7/1836 , C07F7/182
摘要： N,N'-disubstituted or N,N,N'- or N,N',N'-trisubstituted thioureas with additional organyloxysilyl function and tertiary amine function of the general formula ##STR1## These compounds are prepared as follows: a) Aminoorganylsilanes of the general formula ##STR2## are reacted in an organic, inert solvent with carbon disulfide, b) The dithiocarbamates formed thereby having the general formula: ##STR3## are isolated and combined with at least the equimolar amount of an amino compound of the general formulaH.sub.2 N--(CH.sub.2).sub.n --NR.sup.3.sub.2, this mixture is heated until the reaction is completed and the desired product is subsequently isolated.
摘要翻译： N，N'-二取代的N，N，N'-或N，N'，N'-三取代的硫脲，具有另外的有机氧基甲硅烷基官能团和叔胺官能团，通式如下：a）氨基有机基硅烷通式[IMAGE]在有机惰性溶剂中与二硫化碳反应，b）由此形成的具有以下通式的二硫代氨基甲酸酯：分离并与至少等摩尔量的一般的氨基化合物（CH2）n-NR32，将该混合物加热至反应完成，随后分离所需产物。

23. 发明授权

US4647682A Phenylene group-containing organosilanes and processes for the preparation thereof 失效
标题翻译：含亚苯基的有机硅烷及其制备方法
公开(公告)号：US4647682A
公开(公告)日：1987-03-03
申请号：US865486
申请日：1986-05-21
申请人： Peter Panster , Peter Kleinschmit
发明人： Peter Panster , Peter Kleinschmit
IPC分类号： C07F7/14 , C07F7/12 , C07F7/18 , C08G77/52 , C07F7/08
CPC分类号： C07F7/12 , C07F7/1836 , C08G77/52
摘要： Phenylene group-containing organosilanes represented by the formula: ##STR1## where in each case all three possible isomers in relation to the position of the R.sub.3 Si-R.sup.1 substituents can be present concurrently, R.sup.1 represents --CH.sub.2 --CH.sub.2 -- or CH.sub.3 CH>, and R.sup.2 represents chloride or an alkoxy group. Processes for the production of the organosilanes and the use of these substances for the production of the corresponding organopolysiloxanes are also disclosed.
摘要翻译：由下式表示的含亚苯基的有机硅烷：（1）其中在各种情况下，与R 3 Si-R 1取代基的位置相关的所有三种可能的异构体可以同时存在，R 1表示-CH 2 -CH 2 - 或CH 3 CH 3，，R2表示氯原子或烷氧基。还公开了生产有机硅烷的方法和这些物质用于生产相应的有机聚硅氧烷的用途。

24. 发明授权

US4647644A Phenylenesulfonate group-containing organopolysiloxanes, method for their preparation and use thereof 失效
标题翻译：含有苯基磺酸酯基的有机聚硅氧烷，其制备方法和用途
公开(公告)号：US4647644A
公开(公告)日：1987-03-03
申请号：US865490
申请日：1986-05-21
申请人： Peter Panster , Peter Kleinschmit
发明人： Peter Panster , Peter Kleinschmit
IPC分类号： C08G77/00 , B01J39/16 , B01J39/17 , B01J39/18 , C08G77/28 , C08G77/38 , C08G77/48 , C08G77/52 , C08G77/58 , C08G79/00 , C08G77/22 , C07F7/08 , C07F5/06 , C07F7/28
CPC分类号： C08G77/52 , B01J39/165
摘要： Phenylenesulfonate group-containing organopolysiloxanes are disclosed consisting of units represented by the formula: ##STR1## in which R.sup.1 represents --CH.sub.2 --CH.sub.2 -- or CH.sub.3 --CH
摘要翻译：公开了含有苯基磺酸酯基的有机聚硅氧烷，其由下式表示的单元：其中R 1表示-CH 2 -CH 2 - 或CH 3 -CH 2，根据M，X等于1至4的数，并且M表示氢或1-4价金属离子或NH 4，并且氧原子的自由价由另外的式（1）基团的硅原子和/或通过交联剂和/或非磺化亚苯基由下式表示的单元：（2）还公开了一种制备含有机聚硅氧烷的亚磺酸酯基团的方法，以及所述物质作为强酸性阳离子交换剂的用途。

25. 发明授权

US4584395A Method for preparation of 3-chloropropyl-trichlorosilane 失效
标题翻译： 3-氯丙基三氯硅烷的制备方法
公开(公告)号：US4584395A
公开(公告)日：1986-04-22
申请号：US699696
申请日：1985-02-08
申请人： Peter Panster , Rudolf Michel , Wolfgang Buder , Peter Kleinschmit
发明人： Peter Panster , Rudolf Michel , Wolfgang Buder , Peter Kleinschmit
IPC分类号： C07F7/12 , B01J31/00 , C07B61/00 , C07F7/14 , C07F7/08
CPC分类号： C07F7/14
摘要： A method for the preparation of 3-chloropropyltrichlorosilane is carried out by conversion of trichlorosilane with allylchloride in the presence of a platinum containing polymeric organosiloxane-ammonium compound containing units represented by the structural formula: ##STR1## wherein R.sup.1, R.sup.2 and R.sup.3 represent a group of the formula:R.sup.5 --SiO.sub.3/2 (2)wherein R.sup.5 denotes an alkylene group and the free valences of the oxygen atoms are saturated by silicon atoms of further groups of the formula (2), optionally with incorporation of crosslinking agents, R.sup.4 has the same meaning as R.sup.1, R.sup.2 and R.sup.3 or hydrogen, alkyl, cycloalkyl or benzyl, Y.sup.x- represents PtX.sub.4.sup.2- or PtX.sub.6.sup.2- (X is Cl or Br) and can also be an inorganic 1 to 3 functional anion of a protonic acid which yields stable salts with amine bases or the hydroxy group, and x is a number from 1 to 3.
摘要翻译：制备3-氯丙基三氯硅烷的方法是通过在含有由下列结构式表示的含有单元的含铂聚合物有机硅氧烷 - 铵化合物存在下，将三氯硅烷与烯丙基氯反应进行的：其中R1，R2和R3 代表式为R5-SiO3 / 2（2）的基团，其中R5表示亚烷基并且氧原子的游离价被另外的式（2）的基团的硅原子饱和，任选地加入交联剂，R4与R1，R2和R3或氢，烷基，环烷基或苄基具有相同的含义，Yx-表示PtX42-或PtX62-（X是Cl或Br），也可以是质子的无机1至3官能阴离子其与胺碱或羟基产生稳定的盐，x为1至3的数。

26. 发明授权

US4410669A Polymeric ammonium compounds with a silica-type backbone, processes for their preparation and use 失效
标题翻译：具有二氧化硅型骨架的聚合铵化合物，其制备和使用方法
公开(公告)号：US4410669A
公开(公告)日：1983-10-18
申请号：US376881
申请日：1982-05-10
申请人： Peter Panster , Peter Kleinschmit
发明人： Peter Panster , Peter Kleinschmit
IPC分类号： B01J41/12 , B01J31/00 , B01J41/08 , C07F7/08 , C07F7/18 , C08G77/00 , C08G77/26 , C08G77/28 , C08G77/38 , C08G77/48 , C08G77/58 , C08F283/00
CPC分类号： B01J41/08 , C07F7/0838 , C07F7/0889 , C07F7/1836 , C08G77/26 , C08G77/38 , C08G77/48
摘要： Polymeric ammonium compounds are disclosed which have a silica-type backbone, comprised of units having the formula: ##STR1## in which R.sup.1 and R.sup.2 represent a group ##STR2## in which R.sup.5 is an alkylene grouping and the free valencies of the oxygen atoms are saturated by silicon atoms of further groups (2), if appropriate with incroporation of crosslinking agents, R.sup.3 and R.sup.4 have the meaning of R.sup.1 and R.sup.2 or represent hydrogen, an alkyl group, cycloalkyl group or the benzyl group, X represents a 1- to 3-valent anion of a protonic acid which forms stable salts with amine bases and x can be a number from 1 to 3. Also disclosed are processes for preparing the polymeric ammonium compounds and to the use of these materials as ion exchange materials.
摘要翻译：公开了具有二氧化硅型主链的聚合铵化合物，其由具有下式的单元组成：其中R 1和R 2表示基团，其中R 5是亚烷基，而自由基氧原子的价态由另外的基团（2）的硅原子饱和，如果合适的话，R3和R4具有R1和R2的意义，或代表氢，烷基，环烷基或苄基， X表示与胺碱形成稳定盐的质子酸的1至3价阴离子，x可以是1至3的数。还公开了制备聚合铵化合物的方法以及将这些材料用作离子交换材料。

27. 发明授权

US5354831A Shaped organopolysiloxanes containing sulfonate groups, a process for their production and their use 失效
标题翻译：含有磺酸盐基团的有机聚硅氧烷，其生产方法及其用途
公开(公告)号：US5354831A
公开(公告)日：1994-10-11
申请号：US85960
申请日：1993-07-06
申请人： Peter Panster , Peter Kleinschmit
发明人： Peter Panster , Peter Kleinschmit
IPC分类号： B01J31/06 , B01J23/72 , B01J31/02 , B01J31/10 , B01J31/12 , B01J35/00 , B01J35/02 , B01J35/10 , B01J37/00 , B01J37/10 , B01J39/18 , C07B61/00 , C07C1/20 , C07C11/09 , C07C31/04 , C08G77/22 , C08G77/28 , C08G77/32 , C08G77/58 , C08J3/12 , C07F7/08 , C07F5/06 , C07F7/28
CPC分类号： B01J31/124 , B01J31/0225 , B01J31/10 , B01J35/0026 , B01J35/023 , B01J37/0072 , B01J39/185 , C08G77/28 , C08G77/58 , C08J3/12 , B01J2231/49 , B01J23/72 , B01J35/1019 , B01J35/1023 , B01J35/1047 , B01J37/10 , C08J2383/08
摘要： Disclosed are shaped organopolysiloxanes containing sulfonate groups and consisting of units(O.sub.3/2 Si--R.sup.1 --SO.sub.3.sup.-).sub.x M.sup.x+ (I)in which R.sup.1 is an alkylene group, x is a number from 1 to 4 depending on M, and M is hydrogen or a monovalent to tetravalent optionally complex metal ion, and the valencies of the silicon linked oxygen atoms are saturated by silicon atoms of other groups (I) or by crosslinking silicon and aluminum compounds, the ratio of the silicon atoms in (I) to the silicon and aluminum atoms of the crosslinker being from 1:4 to 1:20. The organopolysiloxanes containing sulfonate groups are present in the form of spherical particles with a diameter of 0.01 to 3 mm, a specific surface of 0.1 to 1200 m.sup.2 /g, a specific pore volume of 0.01 to 6 ml/g, and an apparent density of 50 to 1000 g/l. Also disclosed are processes for the production of the shaped sulfonated organopolysiloxanes and to their use as a solid acid catalyst.
摘要翻译：公开了含有磺酸酯基的成型有机聚硅氧烷，其由R 1为亚烷基的单元（O 3 / 2Si-R 1 -SO 3 - ）x M x +（I）组成，x取决于M为1至4，M为氢或一价至四价任选的复合金属离子，并且硅连接的氧原子的价态由其他基团（I）的硅原子或硅和铝化合物的硅原子饱和，（I）中的硅原子与硅并且交联剂的铝原子为1:4至1:20。含有磺酸盐基团的有机聚硅氧烷以直径为0.01〜3mm，比表面积为0.1〜1200m 2 / g，比孔体积为0.01〜6ml / g的球状颗粒的形式存在，表观密度为 50〜1000g / l。还公开了制备成型磺化有机聚硅氧烷的方法及其作为固体酸催化剂的用途。

28. 发明授权

US5061773A Aminoalkyl-substituted organopolysiloxane thiourea derivatives and methods of preparation and use thereof 失效
标题翻译：氨基烷基取代的有机聚硅氧烷硫脲衍生物及其制备和使用方法
公开(公告)号：US5061773A
公开(公告)日：1991-10-29
申请号：US558867
申请日：1990-07-30
申请人： Peter Panster , Ulrich Deschler , Peter Kleinschmit
发明人： Peter Panster , Ulrich Deschler , Peter Kleinschmit
IPC分类号： C02F1/62 , B01J20/26 , C02F1/28 , C08G77/28 , C08G77/48 , C08G77/54 , C08G77/58
CPC分类号： C02F1/285 , B01J20/26 , C08G77/28 , C08G77/54 , C08G77/58
摘要： Aminoalkyl-substituted organopolysiloxane thioureas are disclosed which consist of the units ##STR1## whereby R.sup.1 stands for a group ##STR2## R.sup.5 is an alkylene grouping, R.sup.2 is equal to R.sup.1 or H, R.sup.3 is equal to R.sup.1 or H or a group (CH.sub.2).sub.n --N(R.sup.6).sub.2 (III) (in which n=1-6, R.sup.6 =H or an alkyl group with C.sub.1 -C.sub.5) and R.sup.4 =H or a group of the formula (III), whereby (I) contains at most 2 (III) groups and at most 2 (III) groups and the free valances of the oxygen atoms sitting on the silicon atom are saturated by silicon atoms of other (III) groups, optionally with the insertion of cross-linking agents containing Si, Ti or Zr. The compounds can be random copolycondensates, block copolycondensates or mixed copolycondensates in relation to the optionally present cross-linking agents. In addition, various methods of preparing the compounds are indicated. The compounds can be used especially for the removal of dissolved metals from aqueous or organic phases.
摘要翻译：（I）单元组成的氨基烷基取代的有机聚硅氧烷硫脲，其中R1代表一个基团（II）R5是亚烷基，R2等于R1或H，R3等于R1或 H或基团（CH 2）n N（R 6）2（III）（其中n = 1-6，R 6 = H或具有C 1 -C 5的烷基）和R 4 = H或式（III）的基团，其中（I）含有至多2个（III）基团和至多2个（III）基团，并且位于硅原子上的氧原子的游离价数被其它（III）基团的硅原子饱和，任选地插入含有Si，Ti或Zr的交联剂。所述化合物可以是无规共聚缩合物，相对于任选存在的交联剂阻断共聚缩聚物或混合的共缩聚物。另外，表示了制备化合物的各种方法。该化合物特别用于从水相或有机相中除去溶解的金属。

29. 发明授权

US5003024A Organosiloxane amine copolycondensates, method of their preparation and use (I) 失效
标题翻译：有机硅氧烷胺共缩聚物，其制备方法和用途（I）
公开(公告)号：US5003024A
公开(公告)日：1991-03-26
申请号：US431218
申请日：1989-11-03
申请人： Peter Panster , Robert Gradl , Peter Kleinschmit
发明人： Peter Panster , Robert Gradl , Peter Kleinschmit
IPC分类号： B01J20/26 , B01J20/22 , C08G77/26 , C08G77/42 , C08G77/44 , C08G77/48 , C08G77/50 , C08G77/54 , C08G77/58
CPC分类号： B01J20/22 , C08G77/26 , C08G77/54 , C08G77/58
摘要： Organosiloxane amine copolycondensates as statistic or block copolycondensates or mixtures thereof consisting of the units ##STR1## in which R.sup.1 to R.sup.5 is ##STR2## and R.sup.6 is bound directly to the nitrogen atom or the double-bonding X group and is alkylene, cycloalkylene or ##STR3## in which n is 1 to 6 and m 0 to 6. The free valences of the oxygen atoms bound to the silicon atom are saturated by silicon atoms of further groups of formula III, optionally with the inclusion of cross-linking agents, X stands for ##STR4## in which R" is H or alkyl. In addition, preparation methods and the use of the products for the removal of dissolved metals from liquid phase or for the adsorption of gaseous compounds.
摘要翻译：有机硅氧烷胺共缩聚物作为统计或嵌段共缩合物或其混合物，其由其中R 1至R 5为（III）且R 6直接键合到氮原子上的单元（I）和（VI）双键X基并且是亚烷基，亚环烷基或者其中n为1至6且m 0至6的亚环烷基或亚环烷基或者其中n为0至6的键。硅原子结合的氧原子的游离价数被硅原子饱和的另外的式III基团，任选地含有交联剂，X代表其中R“是H或烷基的 + TR 。另外，制备方法和产品用于从液相中除去溶解的金属或用于气态化合物的吸附。

30. 发明授权

US4954599A Formed, polymeric, tertiary or secondary organosiloxane amine compounds, methods of their preparation and use 失效
标题翻译：形成的聚合物，三级或次级有机硅氧烷胺化合物，其制备和使用方法
公开(公告)号：US4954599A
公开(公告)日：1990-09-04
申请号：US295886
申请日：1989-01-11
申请人： Peter Panster , Peter Kleinschmit
发明人： Peter Panster , Peter Kleinschmit
IPC分类号： B01D53/02 , B01J20/00 , B01J20/26 , B01J31/08 , B01J31/12 , C08G77/48 , C08G77/50 , C08G77/54 , C08G77/56 , C08G77/58 , C08J3/12 , C08J7/00 , C08L83/14
CPC分类号： C08G77/58 , B01J20/26 , B01J31/124 , C08G77/54
摘要： Spherical, polymeric, tertiary or secondary organosiloxane amine compounds comprising: ##STR1## units in which R.sup.1 and R.sup.2 stand for a group: ##STR2## R.sup.4 is an alkylene grouping and the oxygen atoms are saturated by silicon atoms of other groups (II), with the optional inclusion of cross-linking agents, R.sup.3 is equal to R.sup.1 and R.sup.2 or stands for hydrogen, an alkyl, cycloalkyl or the benzyl group. Also disclosed is a method for the preparation of the compounds in spherical form and the use of these products for removing acids from liquids and gases as well as for the adsorption of gaseous organic compounds.
摘要翻译：包括：其中R 1和R 2表示一个基团的单元：（II）R 4是亚烷基，氧原子被硅原子饱和，其它基团（II），任选地含有交联剂，R 3等于R 1和R 2，或代表氢，烷基，环烷基或苄基。还公开了制备球形化合物的方法以及这些产物用于从液体和气体中除去酸以及吸附气态有机化合物的用途。

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