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21. 发明申请

US20110152576A1 PROCESS FOR PREPARING CYCLIC KETONES 有权
标题翻译：制备循环克氏酮的方法
公开(公告)号：US20110152576A1
公开(公告)日：2011-06-23
申请号：US13060545
申请日：2009-08-26
申请人： Joaquim Henrique Teles , Wilhelm Ruppel , Ulrike Wegerle , Anton Meier , Thomas Genger , Michael Schelper , Peter Resch
发明人： Joaquim Henrique Teles , Wilhelm Ruppel , Ulrike Wegerle , Anton Meier , Thomas Genger , Michael Schelper , Peter Resch
IPC分类号： C07C45/28 , C07C45/78
CPC分类号： C07C45/28 , C07C45/82 , C07C2601/08 , Y02P20/582 , C07C49/403 , C07C49/395 , C07C49/413
摘要： The present invention relates to a process for preparing at least one monocyclic ketone having from 4 to 20 carbon atoms by reacting a mixture G1 comprising at least one monocyclic olefin having from 4 to 20 carbon atoms with a mixture G2 comprising at least dinitrogen monoxide, wherein said reaction is performed adiabatically.
摘要翻译：本发明涉及一种制备至少一种具有4-20个碳原子的单环酮的方法，该方法是使包含至少一种具有4-20个碳原子的单环烯烃的混合物G1与至少包含一氧化二氮的混合物G2反应，其中所述反应是绝热的。

22. 发明申请

US20080119673A1 PROCESS FOR HETEROGENEOUSLY CATALYZED PARTIAL DEHYDROGENATION OF AT LEAST ONE HYDROCARBON TO BE DEHYDROGENATED 有权
标题翻译：用于异源催化的部分脱氢工艺用于脱氢的一个氢氧化碳
公开(公告)号：US20080119673A1
公开(公告)日：2008-05-22
申请号：US11678362
申请日：2007-02-23
申请人： Claus HECHLER , Wilhelm Ruppel , Wolfgang Gerlinger , Wolfgang Schneider , Klaus Joachim Mueller-Engel
发明人： Claus HECHLER , Wilhelm Ruppel , Wolfgang Gerlinger , Wolfgang Schneider , Klaus Joachim Mueller-Engel
IPC分类号： C07C9/00
CPC分类号： C07C5/48 , C07C45/35 , C07C51/252 , C07C51/43 , C07C11/06 , C07C47/22 , C07C57/04
摘要： A process for heterogeneously catalyzed partial dehydrogenation of a hydrocarbon, in which a reaction gas mixture input stream comprising the hydrocarbon to be dehydrogenated is conducted through a fixed catalyst bed disposed in a shaft and the reaction gas mixture input stream is obtained in the shaft by metering an input gas II comprising molecular oxygen upstream of the fixed catalyst bed into an input gas stream I which comprises molecular hydrogen and the hydrocarbon to be dehydrogenated and is flowing within the shaft toward the fixed catalyst bed.
摘要翻译：烃的非均相催化部分脱氢的方法，其中包含待脱氢烃的反应气体混合物输入流通过设置在轴中的固定催化剂床进行，反应气体混合物输入流通过计量获得在轴中将固定催化剂床上游的分子氧的输入气体II输入到输入气流I中，该输入气流I包括分子氢和要脱氢的烃并且在轴内朝向固定的催化剂床流动。

23. 发明授权

US07087767B2 Method for producing maleic anhydride 有权
公开(公告)号：US07087767B2
公开(公告)日：2006-08-08
申请号：US10522993
申请日：2003-07-22
申请人： Jens Weiguny , Wilhelm Ruppel , Mark Duda
发明人： Jens Weiguny , Wilhelm Ruppel , Mark Duda
IPC分类号： C07D307/60
CPC分类号： C07D307/60
摘要： Process for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of hydrocarbons having at least four carbon atoms by means of oxygen-containing gases at from 350 to 500° C. in the presence of a volatile phosphorus compound over a vanadium-, phosphorus- and oxygen-containing catalyst in a shell-and-tube reactor unit having at least one reaction zone cooled by means of a heat transfer medium, in which the temperature and/or the amount of the heat transfer medium flowing into the first (relative to the feed direction) reaction zone are set so that the mean temperature of the heat transfer medium in the first reaction zone TSB(1st zone), which is calculated as the mean of the inflow temperature and the outflow temperature of the heat transfer medium, is in accordance with the formulae (I) and (II) TSB(1st zone)≦TR(1st zone)−TSafety(1st zone) (I) TSB, Ymax(1st zone)−TA(1st zone)≦TSB(1st zone)≦TSB, Ymax(1st zone)+TB(1st zone), (II) where TR(1st zone) is the runaway temperature of the first reaction zone; TSafety(1st zone) is the safety temperature of the first reaction zone and has a value of 1° C.; TSB, Ymax(1st zone) is the mean temperature of the heat transfer medium in the first reaction zone at which the maximum maleic anhydride yield is achieved in the range TSB(1st zone)≦TR(1st zone); TA(1st zone) is 20° C.; and TB(1st zone) is 10° C.

24. 发明授权

US06056928A Method of removing nitrogen oxides from a gas flow 失效
标题翻译：从气流中除去氮氧化物的方法
公开(公告)号：US06056928A
公开(公告)日：2000-05-02
申请号：US29833
申请日：1998-03-10
申请人： Thomas Fetzer , Eckhart Wagner , Emil Roth , Wilhelm Ruppel , Hermann Wistuba , Bernhard Otto , Volker Schumacher , Gert Burger
发明人： Thomas Fetzer , Eckhart Wagner , Emil Roth , Wilhelm Ruppel , Hermann Wistuba , Bernhard Otto , Volker Schumacher , Gert Burger
IPC分类号： B01D53/56 , B01D53/77 , B01D53/86 , C01B21/38 , C01B21/40 , C01B21/00 , C01B21/26
CPC分类号： C01B21/38 , B01D53/56 , B01D53/8625 , B01D2257/402 , Y02C20/10 , Y02P20/153
摘要： The invention relates to a process for removing nitrogen oxides from a gas stream containing same, which comprises passing the gas stream(A) through a stage for absorbing the nitrogen oxides other than N.sub.2 O in an absorbent or reacting the nitrogen oxides other than N.sub.2 O with an absorbent at a pressure of from 1,5 to 20 bar, and(B) through a stage for reducing the amount of N.sub.2 O, preferably employing the pressure level of step A, and to apparatus therefor and the use thereof.
摘要翻译： PCT No.PCT / EP96 / 03971 Sec。 371日期1998年3月10日 102（e）1998年3月10日PCT PCT 1996年9月10日PCT公布。公开号WO97 / 10042 日期1997年3月20日本发明涉及一种从含有它们的气流中除去氮氧化物的方法，其包括使气流（A）通过吸收吸收剂中除了N 2 O以外的氮氧化物的阶段，或使氮氧化物压力为1.5〜20巴的吸收剂以外的N2O除外，（B）通过用于减少N 2 O的量的阶段，优选使用步骤A的压力水平，以及其设备及其用途。

25. 发明授权

US5225574A Preparation of phthalic anhydride from o-xylene 失效
标题翻译：从O-XYLENE制备PHTHALIC ANHYDRIDE
公开(公告)号：US5225574A
公开(公告)日：1993-07-06
申请号：US682295
申请日：1991-04-09
申请人： Heinrich Aichinger , Wilhelm Ruppel , Rolf Seubert , Karl-Heinz Boehning , Walter Scheidmeir , Johannes E. Schmidt , Matthias Schwarzmann
发明人： Heinrich Aichinger , Wilhelm Ruppel , Rolf Seubert , Karl-Heinz Boehning , Walter Scheidmeir , Johannes E. Schmidt , Matthias Schwarzmann
IPC分类号： B01J23/18 , B01J23/22 , B01J27/198 , C07B61/00 , C07C51/265 , C07D307/89
CPC分类号： B01J23/002 , B01J23/22 , B01J27/198 , C07C51/265 , B01J2523/00
摘要： Phthalic anhydride is prepared in a multiple tube reactor provided with separate salt baths, the temperature of the salt bath used for cooling the first layer of catalyst, as regarded in the direction of flow of the reaction mixture, being from 2.degree. to 20.degree. C. higher than that of the salt bath(s) associated with the following layer(s).
摘要翻译：在具有单独的盐浴的多管反应器中制备邻苯二甲酸酐，用于冷却第一层催化剂的盐浴的温度，如在反应混合物的流动方向所考虑的，为2至20℃ 高于与下一层相关的盐浴的温度。

26. 发明申请

US20110038763A1 PROCESS FOR CONTINUOUS HETEROGENEOUSLY CATALYZED PARTIAL DEHYDROGENATION OF AT LEAST ONE HYDROCARBON TO BE DEHYDROGENATED 有权
标题翻译：连续异源催化部分去除脱氢脱氢酶的方法
公开(公告)号：US20110038763A1
公开(公告)日：2011-02-17
申请号：US12912127
申请日：2010-10-26
申请人： Claus Hechler , Wilhelm Ruppel , Götz-Peter Schindler , Catharina Klanner , Hans-Jürgen Bassler , Martin Dieterle , Karl-Heinrich Klappert , Klaus Joachim Müller-Engel
发明人： Claus Hechler , Wilhelm Ruppel , Götz-Peter Schindler , Catharina Klanner , Hans-Jürgen Bassler , Martin Dieterle , Karl-Heinrich Klappert , Klaus Joachim Müller-Engel
IPC分类号： B01J8/00
CPC分类号： C07C5/333 , B01J8/067 , B01J19/02 , B01J2219/0236 , C07C51/215 , C22C30/00 , C22C38/40 , Y02P20/52 , C07C11/06 , C07C11/02 , C07C57/04
摘要： A process for continuous heterogeneously catalyzed partial dehydrogenation of at least one hydrocarbon to be dehydrogenated in a reactor which is manufactured from a composite material which consists, on its side in contact with the reaction chamber, of a steel B with specific elemental composition which, on its side facing away from the reaction chamber, either directly or via an intermediate layer of copper, or of nickel, or of copper and nickel, is plated onto a steel A with specific elemental composition, and also partial oxidations of the dehydrogenated hydrocarbon and the reactor itself.
摘要翻译：在反应器中连续不均匀催化的待脱氢烃的部分脱氢的方法，该反应器由复合材料制成，该复合材料在其与反应室接触的一侧由具有特定元素组成的钢B组成，其直接或经由铜或镍或铜和镍的中间层离开反应室的一侧被镀在具有特定元素组成的钢A上，并且还将脱氢烃和反应堆本身。

27. 发明授权

US07211691B2 Heterogeneously catalyzed partial gas phase oxidation of propene to acrolein 有权
标题翻译：将丙烯非均相催化部分气相氧化成丙烯醛
公开(公告)号：US07211691B2
公开(公告)日：2007-05-01
申请号：US10784825
申请日：2004-02-24
申请人： Jochen Petzoldt , Martin Dieterle , Heiko Arnold , Wilhelm Ruppel , Klaus-Joachim Mueller-Engel
发明人： Jochen Petzoldt , Martin Dieterle , Heiko Arnold , Wilhelm Ruppel , Klaus-Joachim Mueller-Engel
IPC分类号： C07C51/16
CPC分类号： C07C45/35 , C07C51/252 , C07C47/22 , C07C57/04
摘要： In a process for heterogeneously catalyzed partial gas phase oxidation of propene to acrolein, the starting reaction gas mixture is oxidized over a fixed catalyst bed which consists of at least two fixed catalyst bed zones and is accommodated in two successive temperature zones A, B, and the transition from temperature zone A to temperature zone B does not spatially coincide with a transition from one fixed catalyst bed zone to another fixed catalyst bed zone.
摘要翻译：在将丙烯非均相催化的部分气相氧化成丙烯醛的过程中，起始反应气体混合物在由至少两个固定的催化剂床区组成的固定催化剂床上被氧化，并被容纳在两个连续的温度区A，B和从温度区A到温度区B的过渡在空间上与从一个固定的催化剂床区到另一个固定催化剂床区的过渡不一致。

28. 发明授权

US06803473B2 Method for producing maleic acid anhydride 有权
标题翻译：马来酸酐生产方法
公开(公告)号：US06803473B2
公开(公告)日：2004-10-12
申请号：US10220746
申请日：2002-09-05
申请人： Jens Weiguny , Sebastian Storck , Andreas Tenten , Wilhelm Ruppel
发明人： Jens Weiguny , Sebastian Storck , Andreas Tenten , Wilhelm Ruppel
IPC分类号： C07D30760
CPC分类号： B01J8/067 , B01J2208/00212 , B01J2208/0053 , C07C51/215 , C07C57/145
摘要： In a process for preparing maleic anhydride by heterogeneously catalyzed gas-phase oxidation of hydrocarbons having at least four carbon atoms using oxygen-containing gases in the presence of a volatile phosphorus compound over a catalyst comprising vanadium, phosphorus and oxygen in a shell-and-tube reactor unit having at least two successive cooled reaction zones, the temperature of the first reaction zone is from 350 to 450° C. and the temperature of the second and further reaction zones is from 350 to 480° C. and the temperature difference between the hottest reaction zone and the coolest reaction zone is at least 2° C.
摘要翻译：在使用含氧气体的挥发性磷化合物存在下，在包含钒，磷和氧的催化剂存在下，通过异构催化气相氧化具有至少四个碳原子的烃来制备马来酸酐的方法，管式反应器单元具有至少两个连续冷却的反应区，第一反应区的温度为350-450℃，第二反应区和其它反应区的温度为350-480℃，温度差为最热的反应区和最冷的反应区为至少2℃

29. 发明授权

US6090977A Continuous heterogeneously catalyzed gas-phase partial oxidation of an organic compound 失效
标题翻译：连续不均匀催化的有机化合物的气相部分氧化
公开(公告)号：US6090977A
公开(公告)日：2000-07-18
申请号：US610888
申请日：1996-03-05
申请人： Werner Hefner , Otto Machhammer , Hans-Peter Neumann , Andreas Tenten , Wilhelm Ruppel , Herbert Vogel
发明人： Werner Hefner , Otto Machhammer , Hans-Peter Neumann , Andreas Tenten , Wilhelm Ruppel , Herbert Vogel
IPC分类号： C07B35/04 , C07B41/06 , C07B41/08 , C07C27/00 , C07C45/35 , C07C47/22 , C07C51/235 , C07C51/25 , C07C51/265 , C07C57/05 , C07D301/08 , C07C27/14
CPC分类号： C07D301/08 , C07C45/35 , C07C51/235 , C07C51/25 , C07C51/252 , C07C51/265
摘要： In a process for the continuous heterogeneously catalyzed gas-phase partial oxidation of an organic compound in an oxidation reactor, whose feed gas mixture comprises, apart from the organic compound to be partially oxidized and molecular oxygen as oxidant, at least one diluent gas which is essentially inert under the conditions of the heterogeneously catalyzed gas-phase partial oxidation, where the essentially inert diluent gas consists partly of combustible gases, after passage through the oxidation reactor, the combustible constituents of the inert diluent gas present in the product gas stream leaving the oxidation reactor are not recirculated to the heterogeneously catalyzed gas-phase partial oxidation, but are put to further use for the purposes of another chemical reaction.
摘要翻译：在氧化反应器中的有机化合物的连续非均相催化气相部分氧化的方法中，其进料气体混合物除了要被部分氧化的有机化合物和分子氧作为氧化剂外，还包含至少一种稀释气体在非均相催化的气相部分氧化的条件下基本上是惰性的，其中基本上惰性的稀释气体部分地由可燃气体组成，在通过氧化反应器之后，存在于产物气流中的惰性稀释气体的可燃组分离开氧化反应器不再循环到非均相催化的气相部分氧化，而是进一步用于另一种化学反应。

30. 发明授权

US5821390A Catalytic gas-phase oxidation of propene to acrolein 失效
标题翻译：丙烯催化气相氧化成丙烯醛
公开(公告)号：US5821390A
公开(公告)日：1998-10-13
申请号：US525011
申请日：1995-09-08
申请人： Wilhelm Ruppel , Ulrike Wegerle , Andreas Tenten , Ulrich Hammon
发明人： Wilhelm Ruppel , Ulrike Wegerle , Andreas Tenten , Ulrich Hammon
IPC分类号： B01J23/88 , B01J8/06 , B01J21/02 , B01J23/16 , B01J23/887 , B01J27/132 , B01J27/192 , C07B61/00 , C07C45/35 , C07C47/22
CPC分类号： B01J27/192 , B01J23/8876 , B01J8/067 , C07C45/35 , B01J2208/00212 , B01J2208/00221 , B01J2219/00777
摘要： A gas-phase mixture of propene and oxygen is catalytically oxidized by passing a reactant gas mixture comprising propene and oxygen through a plurality of catalyst containing contact tubes in a fixed bed reactor and simultaneously passing only one heat-exchange medium at elevated temperature over the exterior surfaces of the contact tubes in a longitudinal flow pattern which is cocurrent with the direction of flow of the reactants through said tube; simultaneously superposing a transverse flow on said longitudinal flow of heat exchange medium by means of an arrangement of successive baffles along the contact tubes which leave passage cross-sections free, thereby resulting in a meandrous flow of the heat-exchange medium through the reactor and setting the flow rate of said heat-exchange medium so that its temperature between the point of entry of the medium into the reactor and its point of exit increases by 2.degree. to 10.degree. C.; and obtaining product acrolein at a selectivity .gtoreq.85 mol % from the reactor at a single pass propene conversion .gtoreq.90 mol %.
摘要翻译：丙烯和氧气的气相混合物通过在固定床反应器中通过包含丙烯和氧气的反应气体混合物通过多个含有接触管的催化剂催化氧化，同时仅使一个热交换介质在高温下通过外部接触管的表面以与通过所述管的反应物的流动方向并流的纵向流动图案; 同时通过沿着接触管的连续挡板的布置使横向流在所述纵向流动的热交换介质上，使得通道横截面自由，从而导致热交换介质通过反应器的蜿蜒流动和设定所述热交换介质的流速使得其进入反应器的入口点和其出口点之间的温度升高2℃至10℃; 并且在单次丙烯转化率为90摩尔％时，以反应器的选择性> 85％摩尔得到产物丙烯醛。

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