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21. 发明授权

US5218018A Hydroxyl and carboxyl groups-containing resin with alicyclic polyepoxide 失效
标题翻译：含羟基和含羧基的树脂与脂环族聚环氧化物
公开(公告)号：US5218018A
公开(公告)日：1993-06-08
申请号：US635970
申请日：1990-12-31
申请人： Akira Tominaga , Reiziro Nishida , Hiroshi Inoue , Motoshi Yabuta , Yoshio Sasaki , Akira Kasari , Hiroshi Igarashi , Tohru Ozaki
发明人： Akira Tominaga , Reiziro Nishida , Hiroshi Inoue , Motoshi Yabuta , Yoshio Sasaki , Akira Kasari , Hiroshi Igarashi , Tohru Ozaki
IPC分类号： B05D7/00 , C08G59/20 , C08G59/68 , C09D5/38 , C09D163/00 , C09D201/06
CPC分类号： B05D7/532 , C08G59/20 , C08G59/68 , C09D163/00 , C09D201/06 , C09D5/38
摘要： A thermosetting coating composition comprising as essential components:(a) a hydroxyl group-containing base resin,(b) an alicyclic polyepoxide crosslinking agent, and(c) a catalyst selected from the group consisting of a quaternary ammonium hydroxide and a metal chelate.
摘要翻译：一种热固性涂料组合物，其包含作为必要组分的（a）含羟基的基础树脂，（b）脂环族聚环氧化物交联剂和（c）选自季铵氢氧化物和金属螯合物的催化剂。

22. 发明授权

US5756221A Coating method 失效
标题翻译：涂布方法
公开(公告)号：US5756221A
公开(公告)日：1998-05-26
申请号：US785600
申请日：1997-01-17
申请人： Kyoichi Horibe , Hidehiko Haneishi , Masaru Mitsuji , Motoshi Yabuta , Yasumasa Okumura
发明人： Kyoichi Horibe , Hidehiko Haneishi , Masaru Mitsuji , Motoshi Yabuta , Yasumasa Okumura
IPC分类号： B05D1/36 , B05D3/02 , B05D3/10 , B05D5/00 , B05D7/00 , B05D7/24 , C08G18/58 , C09D5/44 , C25D13/06
CPC分类号： B05D7/576 , C08G18/58 , C08G18/584 , C09D5/4473 , Y10T428/12569 , Y10T428/31522
摘要： The present invention provides a coating method which comprises applying, onto a material to be coated, a cationic electrodepositable coating composition comprising (A) a polyurethane-modified epoxy resin-amine adduct obtained by a reaction of (A-1) a polyurethane-compound having one terminal isocyanate group in the molecule, obtained by a reaction of (a) a polyhydroxy compound having a number-average molecular weight of 50-8,000, (b) a polyisocyanate compound, and (c) a compound having one active hydrogen atom in the molecule; (A-2) a bisphenol type epoxy resin having at least two epoxy groups in the molecule; and (A-3) an active-hydrogen-containing amine compound, and (B) a nonionic film-forming resin, the weight ratio of the resin (A)/the resin (B) being 15/85 to 95/5 and the coating composition comprising substantially no pigment, then heat-curing the formed electrocoating film; and thereafter applying, onto the cured electrocoating film, an aqueous coating composition comprising a metallic pigment and/or a coloring pigment and a high-solid-content coating composition comprising (C) a carboxyl group-containing compound, (D) a vinyl type polymer containing, in the molecule, an epoxy group, a hydroxyl group and a hydrolyzable alkoxysilyl group, (E) a reactive organopolysiloxane, and (F) crosslinked polymer fine particles but comprising substantially no pigment, by two-coat two-bake or by two-coat one-bake.
摘要翻译：本发明提供一种涂布方法，其包括在待涂覆的材料上涂布阳离子可电沉积涂料组合物，其包含（A）通过（A-1）聚氨酯化合物（A-1）反应获得的聚氨酯改性的环氧树脂 - 胺加合物通过（a）数均分子量为50-8,000的多羟基化合物（b）多异氰酸酯化合物和（c）具有一个活性氢原子的化合物的反应获得的分子中具有一个末端异氰酸酯基团在分子中（A-2）分子中具有至少两个环氧基的双酚型环氧树脂; 和（A-3）含活性氢的胺化合物和（B）非离子成膜树脂，树脂（A）/树脂（B）的重量比为15/85至95/5，和所述涂料组合物基本上不含颜料，然后热固化所形成的电泳涂膜; 然后在固化的电泳涂膜上涂覆含有金属颜料和/或着色颜料的水性涂料组合物和包含（C）含羧基化合物的高固含量涂料组合物，（D）乙烯基型在分子中含有环氧基，羟基和可水解的烷氧基甲硅烷基的聚合物，（E）反应性有机聚硅氧烷和（F）交联的聚合物细颗粒，但基本上不含颜料，通过双层二烘烤或通过双面单烤。

23. 发明授权

US5587426A Process for preparing self-crosslinking resin 失效
标题翻译：自交联树脂的制备方法
公开(公告)号：US5587426A
公开(公告)日：1996-12-24
申请号：US024774
申请日：1993-03-02
申请人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Yoh Sugimura
发明人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Yoh Sugimura
IPC分类号： C08G18/10 , C08G18/62 , C08G18/70 , C08G18/72 , C08G18/80 , C08G81/02
CPC分类号： C08G18/8061 , C08G18/10 , C08G18/6229 , C08G18/6254 , C08G18/728
摘要： The present invention provides:(1) a self-crosslinking resin (I) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (A) having at least two free isocyanate groups in the molecule and an acrylic resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with some of the free isocyanate groups of the polymer (A), and subsequently reacting a blocking agent with all the remaining free isocyanate groups, and(2) a self-crosslinking resin (II) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (C) having a free isocyanate group and a blocked isocyanate group in the molecule and the acrylic resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with all the free isocyanate groups of the polymer (C).
摘要翻译：本发明提供：（1）分子中具有封端异氰酸酯基和羟基的自交联树脂（I），其特征在于，所述树脂由具有至少两个游离异氰酸酯基的乙烯基聚合物（A）在分子中具有至少两个羟基的丙烯酸树脂（B），其中树脂（B）的一些羟基与聚合物（A）的一些游离异氰酸酯基团反应，然后使具有所有剩余的游离异氰酸酯基团的封端剂，和（2）分子中具有封端的异氰酸酯基和羟基的自交联树脂（II），其特征在于，树脂由具有通过使树脂（B）的一些羟基与聚合物中的所有游离异氰酸酯基团反应，分子中的游离异氰酸酯基和封端的异氰酸酯基和分子中具有至少两个羟基的丙烯酸树脂（B）（C）。

24. 发明授权

US5945487A Thermosetting powder coating composition 失效
标题翻译：热固性粉末涂料组合物
公开(公告)号：US5945487A
公开(公告)日：1999-08-31
申请号：US765460
申请日：1997-01-23
申请人： Toshio Ohkoshi , Yugen Kawamoto , Toshio Ogasawara , Motoshi Yabuta , Koji Yamada
发明人： Toshio Ohkoshi , Yugen Kawamoto , Toshio Ogasawara , Motoshi Yabuta , Koji Yamada
IPC分类号： C08G18/62 , C08L63/06 , C09D5/46 , C09D133/04 , C09D133/06 , C09D143/04 , C09D201/06 , C08F16/26 , C08F20/32 , C08F24/00 , C08F116/16
CPC分类号： C09D201/06 , C08G18/6225 , C09D133/04 , C09D133/062 , C09D133/068 , C09D143/04 , C08G2150/20 , C08L63/06
摘要： The invention provides a thermosetting powder coating composition comprising (A) a vinyl copolymer having a number average molecular weight of 1,500 to 6,000, a molecular weight distribution of 1.0 to 1.5 as represented by a weight average molecular weight/a number average molecular weight and a glass transition temperature of 40 to 100.degree. C., the copolymer containing at least one species of functional group selected from the class consisting of epoxy group, carboxyl group and hydroxyl group, and (B) a curing agent. The thermosetting powder coating composition of the invention is superior in any of the finished appearance of coating film and the blocking resistance.
摘要翻译： PCT No.PCT / JP95 / 01469 Sec。 371日期1997年1月23日 102（e）1997年1月23日PCT PCT 1995年7月24日PCT公布。出版物WO96 / 03464 日本特开1996年2月8日本发明提供一种热固性粉末涂料组合物，其包含（A）数均分子量为1,500至6000的乙烯基共聚物，分子量分布为1.0至1.5，以重均分子量/ 平均分子量和40〜100℃的玻璃化转变温度，含有选自环氧基，羧基和羟基中的至少一种官能团的共聚物和（B）固化剂。本发明的热固性粉末涂料组合物在涂膜的完成外观和耐粘连性方面均优异。

25. 发明授权

US5830581A Method for formation of coating film 失效
标题翻译：涂膜形成方法
公开(公告)号：US5830581A
公开(公告)日：1998-11-03
申请号：US843595
申请日：1997-04-16
申请人： Yutaka Masuda , Akimasa Nakahata , Yoshiyuki Yukawa , Motoshi Yabuta
发明人： Yutaka Masuda , Akimasa Nakahata , Yoshiyuki Yukawa , Motoshi Yabuta
IPC分类号： B05D5/06 , B32B15/08 , B05D3/02
CPC分类号： B05D5/068 , Y10T428/31692 , Y10T428/31699 , Y10T428/31855 , Y10T428/31935
摘要： The present invention provides a method for forming a multi-layer coating film by applying a colored clear coating (B) containing a color pigment and/or a glittering material, on the film of a leafing type aluminum flake-containing metallic coating (A), wherein the colored clear coating (B) also contains a polymer formed from an unsaturated monomer having a phosphoric acid group represented by --O--PO(OH)(R.sub.1) (wherein R.sub.1 is a hydroxyl group, a phenyl group or a C.sub.1-20 alkyl group) and a hydroxyl group-containing unsaturated monomer. The method can form a multi-layer coating film improved in interlayer adhesivity between the metallic coating film and the colored clear coating film, without reducing the excellent effects and metallic feeling provided by a metallic coating film containing leafing type aluminum flake.
摘要翻译：本发明提供一种通过将含有着色颜料和/或闪光材料的着色透明涂层（B）涂覆在含叶片状铝箔金属涂层（A）的膜上形成多层涂膜的方法，，其中着色透明涂层（B）还含有由具有由-O-PO（OH）（R1）表示的磷酸基的不饱和单体形成的聚合物（其中R1是羟基，苯基或C1- 20烷基）和含羟基的不饱和单体。该方法可以形成改善金属涂膜和着色透明涂膜之间的层间粘合性的多层涂膜，而不会降低由含叶片型铝片的金属涂膜提供的优异的效果和金属感。

26. 发明授权

US5414055A Coating resin compositions 失效
标题翻译：涂料树脂组合物
公开(公告)号：US5414055A
公开(公告)日：1995-05-09
申请号：US64650
申请日：1993-05-21
申请人： Yoh Sugimura , Motoshi Yabuta , Yoshiyuki Yukawa , Yasuhiro Fujii
发明人： Yoh Sugimura , Motoshi Yabuta , Yoshiyuki Yukawa , Yasuhiro Fujii
IPC分类号： C08G18/62 , C08G18/10 , C08G18/63 , C08G18/72 , C09D175/00 , C09D175/04 , C08F283/04
CPC分类号： C08G18/728 , C08G18/10 , C08G18/633
摘要： (1) A coating resin composition consisting essentially of a self-crosslinking resin (I) having at least one hydroxyl group and at least one blocked isocyanate group in the molecule wherein the resin (I) is prepared by reacting some of the free isocyanate groups of a vinyl polymer (A) having at least two free isocyanate groups in the molecule with some of the hydroxyl groups of a polyolefin resin (B) having at least two hydroxyl groups in the molecule, and subsequently reacting a blocking agent with the remaining free isocyanate groups, and (2) a coating resin composition consisting essentially of a self-crosslinking resin (II) having at least one hydroxyl group and at least one blocked isocyanate group in the molecule wherein the resin (II) is prepared by reacting all free isocyanate groups of a vinyl polymer (C) having at least one free isocyanate group and at least one blocked isocyanate group in the molecule with some of the hydroxyl groups of a polyolefin resin (B) having at least two hydroxyl groups in the molecule.
摘要翻译：（1）一种基本上由分子中具有至少一个羟基和至少一个封端异氰酸酯基的自交联树脂（I）组成的涂料树脂组合物，其中树脂（I）是通过一些游离异氰酸酯基团的分子中具有至少两个游离异氰酸酯基团的乙烯基聚合物（A），其中在分子中具有至少两个羟基的聚烯烃树脂（B）的一些羟基，然后使封闭剂与剩余的游离的异氰酸酯基，和（2）主要由在分子中具有至少一个羟基和至少一个封端的异氰酸酯基的自交联树脂（II）组成的涂料树脂组合物，其中树脂（II）通过使全部自由基在分子中具有至少一个游离异氰酸酯基和至少一个封端异氰酸酯基的乙烯基聚合物（C）的异氰酸酯基团，其中一些聚烯烃树脂（B）的一些羟基具有至少分子中有两个羟基。

27. 发明授权

US5173533A Dispersion of reactive polymer particles 失效
标题翻译：反应性聚合物颗粒的分散
公开(公告)号：US5173533A
公开(公告)日：1992-12-22
申请号：US235573
申请日：1988-07-26
申请人： Motoshi Yabuta , Yasushi Hiramatsu , Chikara Kawamura
发明人： Motoshi Yabuta , Yasushi Hiramatsu , Chikara Kawamura
IPC分类号： C08F2/18 , C08F2/08 , C08F2/14 , C08F2/20 , C08F2/24 , C08F291/00 , C09D5/00 , C09D201/00 , C09J201/00
CPC分类号： C08F2/08
摘要： A dispersion of reactive polymer particles obtained by polymerization of monomer in an organic liquid which dissolves the monomer but does not dissolve a polymer formed from the monomer, in the presence of a dispersion stabilizer composed of a high molecular weight polymer; characterized in that (i) said dispersion stabilizer is a high molecular weight polymer which is obtained by polymerization of an ethylenically unsaturated monomer and soluble in the above organic liquid and which contains a chemically reactive group (A); that (ii) said polymer particles are particles of a high molecular weight polymer which are obtained by polymerization of an ethylenically unsaturated monomer and contain a complementary chemically reactive group (B) capable of mutually reacting with the chemically reactive group (A); and that (iii) the chemically reactive group (A) and the chemically reactive group (B) are present stably in the dispersion. This dispersion is useful in coating compositions such as an adhesive, coating, etc.
摘要翻译：在由高分子量聚合物构成的分散稳定剂的存在下，通过聚合单体在有机液体中溶解单体但不溶解由单体形成的聚合物而获得的反应性聚合物颗粒的分散体; 其特征在于，（i）所述分散稳定剂是通过烯键式不饱和单体的聚合获得并且可溶于上述有机液体并且含有化学反应性基团（A）的高分子量聚合物; （ii）所述聚合物颗粒是通过烯键式不饱和单体的聚合并含有能够与化学反应性基团（A）相互反应的互补的化学反应性基团（B）获得的高分子量聚合物的颗粒; 并且（iii）化学反应性基团（A）和化学反应性基团（B）稳定地存在于分散体中。该分散体可用于涂料组合物如粘合剂，涂料等

28. 发明授权

US4829120A Method of producing dispersion of fine particles of gelled polymer 失效
标题翻译：制备胶凝聚合物细颗粒分散体的方法
公开(公告)号：US4829120A
公开(公告)日：1989-05-09
申请号：US17071
申请日：1987-02-20
申请人： Motoshi Yabuta
发明人： Motoshi Yabuta
IPC分类号： C08F283/00 , C08F2/16 , C08F2/20 , C08F290/00 , C08F290/06 , C08F299/04 , C08L57/00 , C09D151/00 , C09D153/00
CPC分类号： C08F299/0485
摘要： A method of producing a dispersion of fine particles of a gelled polymer, which comprises polymerizing a vinyl monomer mixture containing at least two vinyl monomers having complementary functional groups capable of being bonded to each other by reaction each in an amount of at least 0.5% by weight, or a vinyl monomer mixture containing at least 0.5% by weight of a polyvinyl monomer containing at least two polymerizable double bonds in an organic liquid incapable of dissolving the polymer formed from the monomer mixture, in the presence of a macromer having a number average molecular weight of at least 1,000 resulting from introduction of polymerizable double bonds into a self-condensation product of 12-hydroxystearic acid, the number of the polymerizable double bonds being 0.7 to 1.0 per molecule of the self-condensation product on an average.
摘要翻译：一种制备凝胶聚合物细颗粒分散体的方法，该方法包括将含有至少两个具有互补官能团的乙烯基单体的乙烯基单体混合物聚合，所述乙烯基单体混合物的反应各自以至少0.5％重量或含有至少0.5重量％的含有至少两个可聚合双键的聚乙烯基单体的乙烯基单体混合物，其在不能溶解由单体混合物形成的聚合物的有机液体中，在具有数均分子量的大分子单体存在下通过将可聚合双键引入到12-羟基硬脂酸的自缩合产物中而产生的分子量为1,000以上，每分子自缩合产物的可聚合双键的数目平均为0.7-1.0。

29. 发明授权

US5488089A Curable resin composition 失效
标题翻译：可固化树脂组合物
公开(公告)号：US5488089A
公开(公告)日：1996-01-30
申请号：US323767
申请日：1994-10-17
申请人： Koji Yamada , Motoshi Yabuta
发明人： Koji Yamada , Motoshi Yabuta
IPC分类号： C08F283/02
CPC分类号： C08F283/02
摘要： A curable resin composition, which is not thickened nor gels during storage, can be high solids, cures even at low temperatures and is excellent in electrostatic coating properties, and which contains as main components, a polymer having in one molecule epoxy group(s), and functional group(s) in each of which a carbonate ester group (--O--CO--O--) is directly bound to an aromatic ring; or a mixture of a compound having in one molecule at least two epoxy groups and a compound having in one molecule at least two functional groups in each of which a carbonate ester group (--O--CO--O--) is directly bound to an aromatic ring, and a curing reaction catalyst.
摘要翻译：在保存期间不增稠或凝胶化的固化性树脂组合物可以是高固体，即使在低温下也能固化，静电涂布性能优异，并且作为主要成分含有一分子环氧基的聚合物，和其中碳酸酯基（-O-CO-O-）直接与芳环结合的官能团; 或具有一个分子中的至少两个环氧基的化合物和在一个分子中具有至少两个官能团的化合物的混合物，其中碳酸酯基（-O-CO-O-）直接与芳族环和固化反应催化剂。

30. 发明授权

US5296551A Self-crosslinking resin 失效
标题翻译：自交联树脂
公开(公告)号：US5296551A
公开(公告)日：1994-03-22
申请号：US97236
申请日：1993-07-27
申请人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Kazunori Mayumi
发明人： Yoshiyuki Yukawa , Motoshi Yabuta , Akimasa Nakahata , Kazunori Mayumi
IPC分类号： C08G18/10 , C08G18/42 , C08G18/72 , C08G18/80 , C08G18/81 , C09D175/00 , C09D175/06 , C08G81/02
CPC分类号： C08G18/728 , C08G18/10 , C08G18/42
摘要： The present invention provides(1) a self-crosslinking resin (I) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (A) having at least two free isocyanate groups in the molecule and a polyester resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with some of the free isocyanate groups of the polymer (A), and subsequently reacting a blocking agent with all the remaining free isocyanate groups, and(2) a self-crosslinking resin (II) having a blocked isocyanate group and a hydroxyl group in the molecule and characterized in that the resin is prepared from a vinyl polymer (C) having a free isocyanate group and a blocked isocyanate group in the molecule and the polyester resin (B) having at least two hydroxyl groups in the molecule by reacting some of the hydroxyl groups of the resin (B) with all the free isocyanate groups of the polymer (C).
摘要翻译：本发明提供（1）在分子中具有封端异氰酸酯基和羟基的自交联树脂（I），其特征在于，所述树脂由具有至少两个游离异氰酸酯基的乙烯基聚合物（A）所述分子和通过使所述树脂（B）的一些羟基与所述聚合物（A）的一些游离异氰酸酯基团反应而在所述分子中具有至少两个羟基的聚酯树脂（B）反应，具有所有剩余的游离异氰酸酯基团的试剂，和（2）在分子中具有封端的异氰酸酯基和羟基的自交联树脂（II），其特征在于，树脂由乙烯基聚合物（C）制备，游离异氰酸酯基和分子内的封端异氰酸酯基和分子中具有至少两个羟基的聚酯树脂（B），其中树脂（B）的一些羟基与聚合物的所有游离异氰酸酯基反应 r（C）。

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