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21. 发明授权

US07834097B2 Fluoroelastomers 有权
标题翻译：氟弹性体
公开(公告)号：US07834097B2
公开(公告)日：2010-11-16
申请号：US12162099
申请日：2007-01-15
申请人： Margherita Albano , Milena Stanga , Francesco Triulzi
发明人： Margherita Albano , Milena Stanga , Francesco Triulzi
IPC分类号： C08F14/18
CPC分类号： C08F214/22 , C08F214/222 , C08L27/12 , C08L27/16 , C08L27/18 , F24S23/74 , F24S23/82 , Y02E10/45 , C08L2666/04
摘要： VDF-based curable fluorelastomers, having a glass transition temperature from −10° C. to −35° C., comprising: B) monomer of formula: CF2═CFOCF2OCF3 (a), C) one or more comonomers selected from: tetrafluoroethylene (TFE), per-fluoromethylvinylether (PMVE), perfluoropropene (HFP), and an amount of —COF end groups in the polymer lower than the sensitivity limit of the method which uses the FT-IR spectroscopy described in the present application.
摘要翻译：具有玻璃化转变温度为-10℃至-35℃的基于VDF的可固化氟树脂，其包含：B）式：CF 2 CFCFF 2 OCF 3（a）的单体，C）一种或多种选自以下的共聚单体：四氟乙烯 TFE），全氟甲基乙烯基醚（PMVE），全氟丙烯（HFP）和聚合物中的-COF端基的量低于使用本申请中描述的FT-IR光谱的方法的灵敏度极限。

22. 发明申请

US20090088529A1 FLUOROELASTOMERS 有权
标题翻译：荧光素
公开(公告)号：US20090088529A1
公开(公告)日：2009-04-02
申请号：US12161638
申请日：2007-01-15
申请人： Francesco Triulzi , Margherita Albano , Milena Stanga
发明人： Francesco Triulzi , Margherita Albano , Milena Stanga
IPC分类号： C08L27/16
CPC分类号： C08F214/22 , C08F214/225 , C08F216/1408 , C08F236/20
摘要： VDF-based curable fluoroelastomers, having a glass transition temperature lower than −49° C., preferably lower than −50° C., and having the following composition, as percent by moles: A) from 25% to 50%, preferably from 30% to 45%, of the monomer of formula: CF2=CFOCF2OCF3 (a); B) one or more (per)fluorinated comonomers having at least one unsaturation of ethylene type in amounts from 75% to 50%, preferably from 70% to 55%; said one or more comonomers comprising vinylidene fluoride (VDF) in amounts from 50% to 75% on the total of the monomer moles; the sum of the molar percentages of the monomers being 100%; said fluoroelastomers containing an amount of —COF end groups in the polymer lower than the sensitivity limit of the method reported in the description.
摘要翻译：玻璃化转变温度低于-49℃，优选低于-50℃的VDF基可固化的含氟弹性体，具有如下组成，按摩尔％计：A）25％-50％，优选 30％至45％的式：CF 2 = CFOCF 2 OCF 3（a）的单体; B）一种或多种具有75％至50％，优选70％至55％的乙烯类型的至少一种不饱和度的（全）氟化共聚单体; 所述一种或多种共聚单体包含单体摩尔数总计为50％至75％的偏二氟乙烯（VDF）; 单体的摩尔百分比之和为100％; 所述含氟弹性体在聚合物中含有一定量的-COF端基，低于说明书中报道的方法的灵敏度极限。

23. 发明授权

US07022773B2 Fluoroelastomer compositions 有权
公开(公告)号：US07022773B2
公开(公告)日：2006-04-04
申请号：US10843440
申请日：2004-05-12
申请人： Margherita Albano , Marco Apostolo , Vincenzo Arcella , Enrico Marchese
发明人： Margherita Albano , Marco Apostolo , Vincenzo Arcella , Enrico Marchese
IPC分类号： C08L23/00 , C08L27/04 , C08L27/12 , C08L33/02 , C08L33/14
CPC分类号： C08L27/12 , C08L27/18 , C08L29/10 , C08L2205/02 , C08L2666/04
摘要： Fluoropolymers comprising a fluoroelastomer matrix incorporating therein particles of a semicrystalline fluoropolymer formed of tetrafluoroethylene (TFE) homopolymers or copolymers, wherein the average particle sizes of the semicrystalline fluoropolymer latex range from 10 to 100 nm.

24. 发明授权

US06566471B1 Peroxide curable fluoroelastomers particularly suitable for manufacturing O-rings 失效
标题翻译：过氧化物可固化的含氟弹性体特别适用于制造O型圈
公开(公告)号：US06566471B1
公开(公告)日：2003-05-20
申请号：US08879319
申请日：1997-06-19
申请人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Vito Tortelli
发明人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Vito Tortelli
IPC分类号： C08F21612
CPC分类号： C08F214/18 , C07C17/25 , C07C17/275 , C07C21/17 , C07C19/07
摘要： New fluoroelastomers are described, having iodine atoms in terminal position and monomeric units in the chain deriving from an iodinated olefin of formula: CHR═CH—Z—CH2CHR—I (I) wherein: R is —H or —CH3; Z is a (per)fluoroalkylene radical C1-C18, linear or branched, optionally containing one or more ether oxygen atoms, or a (per)fluoropolyoxyalkylene radical. These products, upon peroxide curing, require extremely short post-curing treatments (around 30-60 minutes at 180°-230° C.) and are characterized by compression set values lower than 25% (measured on O-rings at 200° C. for 70 hours according to ASTM Standard D395 Method B).
摘要翻译：描述了新的含氟弹性体，其末端具有碘原子，并且衍生自下式的碘化烯烃的链中的单体单元：其中：R是-H或-CH 3; Z是直链或支链（任选地含有一个或多个醚氧原子）或（全）氟聚氧亚烷基的（全）氟亚烷基C1-C18。过氧化物固化时，这些产品需要非常短的后固化处理（在180°-230℃下约30-60分钟），其特征在于压缩永久变形值低于25％（在200℃的O形环上测量）根据ASTM标准D395方法B）70小时。

25. 发明授权

US5674959A Peroxide curable fluoroelastomers, particularly suitable for manufacturing O-rings 失效
标题翻译：过氧化物固化的含氟弹性体，特别适用于制造O型圈
公开(公告)号：US5674959A
公开(公告)日：1997-10-07
申请号：US723928
申请日：1996-10-01
申请人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Vito Tortelli
发明人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Vito Tortelli
IPC分类号： F16J15/10 , C07C17/25 , C07C17/275 , C07C21/18 , C07C41/24 , C07C43/17 , C08F14/18 , C08F14/22 , C08F16/14 , C08F214/18 , C08F214/22 , C08F214/26 , C08F216/14 , C09K3/10 , C08F16/24
CPC分类号： C08F214/18 , C07C17/25 , C07C17/275
摘要： New fluoroelastomers are described, having iodine atoms in terminal position and monomeric units in the chain deriving from an iodinated olefin of formula: CHR.dbd.CH--Z--CH.sub.2 CHR--I (I) wherein: R is --H or --CH.sub.3 ; Z is a (per)fluoroalkylene radical C.sub.1 -C.sub.18, linear or branched, optionally containing one or more ether oxygen atoms, or a (per) fluoropolyoxyalkylene radical. These products, upon peroxide curing, require extremely short post-curing treatments (around 30-60 minutes at 180.degree.-230.degree. C.) and are characterized by compression set values lower than 25% (measured on O-rings at 200.degree. C. for 70 hours according to ASTM Standard D395 Method B).
摘要翻译：描述了新的含氟弹性体，其末端具有碘原子，并且衍生自下式的CH 2 CH = CH-Z-CH 2 CHR-I（I）的碘化烯烃链中的单体单元，其中：R为-H或-CH 3; Z是直链或支链（任选地含有一个或多个醚氧原子）或（全）氟聚氧亚烷基的（全）氟亚烷基C1-C18。过氧化物固化后，这些产品需要非常短的后固化处理（在180°-230℃下约30-60分钟），其特征在于压缩永久变形值低于25％（在200℃的O形环上测量）根据ASTM标准D395方法B）70小时。

26. 发明授权

US5173553A Fluoroelastomers endowed with improved processability and process for preparing them 失效
标题翻译：具有改进的可处理性和制备它们的方法的荧光体
公开(公告)号：US5173553A
公开(公告)日：1992-12-22
申请号：US550308
申请日：1990-07-09
申请人： Margherita Albano , Giulio Brinati , Vincenzo Arcella , Enzo Giannetti
发明人： Margherita Albano , Giulio Brinati , Vincenzo Arcella , Enzo Giannetti
IPC分类号： C08F114/16 , C08F2/38 , C08F14/22 , C08F214/16 , C08F214/22 , C08F214/26
CPC分类号： C08F214/26 , C08F214/22
摘要： Fluoroelastomers characterized by the presence of iodine or bromine atoms at the end of the polymeric chain in an amount equal to or lower than 1 iodine or bromine atom per polymeric chain, and by a bromine content in the chain ranging from 0.05 to 2% by weight referred to the total weight of the monomeric units.Said fluoroelastomers exhibit improved characteristics of processability, particularly as regards the utilization in injection molding processes and the detaching from the molds, as well as of stability to heat.A process for preparing fluoroelastomers containing iodine or bromine atoms at the ends of the polymeric chain, in an amount equal to or lower than 1 iodine or bromine atom per polymeric chain, which process comprises polymerizing mixes of fluorinated monomers (VDF, TFE, HFP, FVE) in bulk, in suspension, in aqueous emulsion, or in solution of organic solvents by means of radical starters, in the presence of compounds capable of providing I.sup.- or Br.sup.- ions in the polymerization medium and conditions.

27. 发明授权

US5585449A Fluoroelastomers comprising monomeric units deriving from a bis-olefin 失效
标题翻译：包含衍生自双烯烃的单体单元的氟弹性体
公开(公告)号：US5585449A
公开(公告)日：1996-12-17
申请号：US361663
申请日：1994-12-22
申请人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Vito Tortelli
发明人： Vincenzo Arcella , Giulio Brinati , Margherita Albano , Vito Tortelli
IPC分类号： C08G65/26 , C08F14/18 , C08F16/14 , C08F16/32 , C08F36/04 , C08F214/18 , C08F214/22 , C08F214/26 , C08F216/12 , C08F216/14 , C08F236/20 , C08K5/00 , C08F16/24
CPC分类号： C08F214/184 , C08F214/18 , C08K5/0025
摘要： New fluoroelastomers are described, comprising monomeric units deriving from a bis-olefin having general formula: ##STR1## wherein: R.sub.1, R.sub.2, R.sub.3, R.sub.4, R.sub.5, R.sub.6, equal or different from each other, are H or alkyls C.sub.1 -C.sub.5 ; Z is an alkylene or cycloalkylene radical C.sub.1 -C.sub.18, linear or branched, optionally containing oxygen atoms, preferably at least partially fluorinated, or a (per)fluoropolyoxyalkylene radical.Such products are endowed with improved processability, especially during calendering of the vulcanization mixture, along with superior mechanical and workability properties during extrusion and injection molding, with a very good mold release.
摘要翻译：描述了新的含氟弹性体，其包含衍生自具有以下通式的双烯烃的单体单元：其中：R1，R2，R3，R4，R5，R6彼此相同或不同的是H或烷基C1 -C5; Z是直链或支链的亚烷基或亚环烷基C1-C18，任选含有氧原子，优选至少部分氟化，或（全）氟聚氧亚烷基。这些产品具有改进的加工性，特别是在硫化混合物的压延过程中，以及在挤出和注射成型期间具有优异的机械和可加工性能，具有非常好的脱模性。

28. 发明授权

US5583190A Polyvinylidenefluoride having high mechanical properties and high thermochemical stability and the preparation process thereof 失效
标题翻译：具有高机械性能和高热稳定性的聚偏二氟乙烯及其制备方法
公开(公告)号：US5583190A
公开(公告)日：1996-12-10
申请号：US534671
申请日：1995-09-27
申请人： Giulio Brinati , Vincenzo Arcella , Margherita Albano
发明人： Giulio Brinati , Vincenzo Arcella , Margherita Albano
IPC分类号： C08F14/22 , C08F4/32 , C08F114/22
CPC分类号： C08F114/22
摘要： A polyvinylidenefluoride (PVDF) having high mechanical properties both at room temperature and at high temperatures, having very good processability and high thermochemical resistance to dehydrofluorination, is prepared by means of a polymerization process of vinylidenefluoride in aqueous emulsion at a temperature comprised between 95.degree. and 120.degree. C., in the presence of a chain transfer agent. In this way it is possible to obtain, using non-hazardous peroxidic initiators (for instance diterbutylperoxide), a PVDF particularly suitable for applications where high mechanical and thermochemical resistance properties are required, such as for instance the manufacture of articles for chemical industry (pipes, valves, fittings, tanks, heat exchangers, membranes, flanges, etc.).
摘要翻译：在室温和高温下具有高机械性能的聚偏二氟乙烯（PVDF），具有非常好的加工性能和对脱氟化氢的高耐热化学性能，是通过聚偏二氟乙烯在水乳液中的温度在95°和 120℃，在链转移剂存在下。以这种方式，可以使用非危险的过氧化物引发剂（例如二叔丁基过氧化物）获得特别适用于需要高机械和耐热化学性能的应用的PVDF，例如用于化学工业的制品（管道，阀门，配件，罐，热交换器，膜，法兰等）。

29. 发明授权

US5264509A Fluoroelastomers based on vinylidene fluoride exhibiting superior resistance to organic bases 失效
标题翻译：基于偏氟乙烯的氟弹性体显示出优异的耐有机碱性
公开(公告)号：US5264509A
公开(公告)日：1993-11-23
申请号：US15063
申请日：1993-02-08
申请人： Vincenzo Arcella , Margherita Albano , Giulio Brinati , Graziell Chiodini , Anna Minutillo
发明人： Vincenzo Arcella , Margherita Albano , Giulio Brinati , Graziell Chiodini , Anna Minutillo
IPC分类号： C08F214/22 , C08F214/26 , C08F16/24
CPC分类号： C08F214/265 , C08F214/225
摘要： Fluoroelastomeric copolymers exhibiting high resistance to bases and alcohols, as well as high mechanical properties and low-temperature resistance, comprising, in moles:4-75% of units of vinylidene fluoride;12-40% of units of hexafluoropropene and/or perfluorovinylether and/or hydropentafluoropropene and/or chlorotrifluoroethylene;2-35% of units of an olefin containing up to 4 carbon atoms;2-60% of units of tetrafluoroethylene, provided that, when the sum of the olefin units and the perfluorovinylether units is equal to or greater than 70%, such copolymers possess a molecular weight sufficiently high to exhibit good mechanical characteristics.
摘要翻译：显示出对碱和醇的高抗性以及高机械性能和耐低温性的氟弹性共聚物，摩尔数：4-75％的偏二氟乙烯单元; 12-40％的六氟丙烯和/或全氟乙烯基醚和/或氢五氟丙烯和/或氯三氟乙烯的单元; 2-35％含有至多4个碳原子的烯烃单元; 2-60％的四氟乙烯单元，条件是当烯烃单元和全氟乙烯基醚单元的总和等于或大于70％时，这种共聚物的分子量足够高以表现出良好的机械特性。

30. 发明申请

US20060189760A1 Fluoroelastomer compositions 审中-公开
公开(公告)号：US20060189760A1
公开(公告)日：2006-08-24
申请号：US11305107
申请日：2005-12-19
申请人： Margherita Albano , Marco Apostolo , Vincenzo Arcella , Enrico Marchese
发明人： Margherita Albano , Marco Apostolo , Vincenzo Arcella , Enrico Marchese
IPC分类号： C08L27/12
CPC分类号： C08L27/12 , C08L27/18 , C08L29/10 , C08L2205/02 , C08L2666/04
摘要： Fluoropolymers comprising a fluoroelastomer matrix incorporating therein particles of a semicrystalline fluoropolymer formed of tetrafluoroethylene (TFE) homopolymers or copolymers, wherein the average particle sizes of the semicrystalline fluoropolymer latex range from 10 to 100 nm.

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