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    • 28. 发明授权
    • Method for producing dinitriles
    • 生产二腈的方法
    • US07816551B2
    • 2010-10-19
    • US10586500
    • 2005-01-27
    • Tim JungkampRobert BaumannMichael BartschGerd HaderleinHermann LuykenJens Scheidel
    • Tim JungkampRobert BaumannMichael BartschGerd HaderleinHermann LuykenJens Scheidel
    • C07C253/10
    • C07C253/10C07C255/04
    • An adiponitrile/methylglutaronitrile preparation process includes distilling a reaction stream to obtain stream 3 depleted in pentenenitriles (bottom product) and stream 4 enriched in pentenenitriles (top product); extracting stream 3 obtaining stream 6 enriched with extractant (top product) and stream 7 depleted in extractant (bottom product); distilling stream 6 obtaining stream 8 comprising the catalyst (bottom product) and stream 9 comprising the extractant (top product); distilling stream 7 obtaining stream 10 (bottom product) and stream 11 comprising the extractant (top product); distilling stream 10 obtaining stream 12 comprising catalyst degradation products, at least one promotor, adiponitrile and methylglutaronitrile (bottom product) and stream 13 comprising pentenenitriles (top product); distilling stream 12 obtaining stream 14 comprising catalyst degradation products and the promotor(s) (bottom product) and stream 15 comprising adiponitrile and methylglutaronitrile (top product); distilling stream 15 obtaining stream 16 comprising adiponitrile (bottom product) and stream 17 comprising methylglutaronitrile (top product).
    • 己二腈/甲基戊二腈的制备方法包括蒸馏反应物流以获得贫饱和腈(最终产物)的流3和富含戊烯腈的流4(顶部产物); 提取物流3获得富集萃取剂(顶部产物)的流6和耗尽萃取剂(底部产物)的料流7; 蒸馏流6获得包含催化剂(底部产物)的流8和包含萃取剂的流9(顶部产物); 蒸馏流7获得流10(底部产物)和包含萃取剂(顶部产物)的料流11; 蒸馏流10获得包含催化剂降解产物的流12,至少一种促进剂,己二腈和甲基戊二腈(底部产物)和包含戊烯腈(顶部产物)的料流13; 蒸馏流12获得包含催化剂降解产物和促进剂(底部产物)的流14和包含己二腈和甲基戊二腈(顶部产物)的料流15; 蒸馏流15获得包含己二腈(底部产物)的流16和包含甲基戊二腈(顶部产物)的料流17。