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21. 发明授权

US07691633B2 Ultra high molecular weight polyethylene fractions having narrow molecular weight distributions and methods of making and using the same 有权
$Ultra high molecular weight polyethylene fractions having narrow molecular weight distributions and methods of making and using the same$
标题翻译：具有窄分子量分布的超高分子量聚乙烯级分及其制备和使用方法
公开(公告)号：US07691633B2
公开(公告)日：2010-04-06
申请号：US11766518
申请日：2007-06-21
申请人： Chung C. Tso , Melvin Hildebrand , Paul J. DesLauriers , Youlu Yu
发明人： Chung C. Tso , Melvin Hildebrand , Paul J. DesLauriers , Youlu Yu
IPC分类号： C08F210/02 , G01N30/02 , C08F6/12
CPC分类号： C08F6/04 , C08F110/02 , Y10T436/10 , C08L23/04 , C08F2500/01 , C08F2500/03
摘要： Polymer fractions such as polyethylene fractions can be produced that have a PDI less than about 2.3 and a Mw greater than about 1,000,000 g/mol, 3,000,000 g/mol, or 6,000,000 g/mol. Such polyethylene fractions are separated from a UHMWPE parent polymer by first dissolving the parent polymer in a relatively good solvent. The conditions employed for such dissolution are selected to reduce the degradation of the parent polymer. The resulting parent solution is transported into a fractionation column in which a support is disposed. The fractionation column is thereafter operated at conditions effective to form a precipitate on the support comprising the desired polyethylene fraction. The polyethylene fraction may then be recovered from the fractionation column by repeatedly displacing a solvent/non-solvent mixture into the column to dissolve the polyethylene fraction. The relative concentrations of the solvent and the non-solvent are based on a solvent gradient profile of the polyethylene parent polymer.
摘要翻译：可以制备聚合物级分，例如具有小于约2.3的PDI和大于约1,000,000g / mol的Mw，3,000,000g / mol或6,000,000g / mol的聚乙烯级分。通过首先将母体聚合物溶解在相对良好的溶剂中，将这样的聚乙烯部分与UHMWPE母体聚合物分离。选择用于这种溶解的条件以降低母体聚合物的降解。将所得的母体溶液输送到其中设置有支持物的分馏塔。然后分馏塔在有效地在包含所需聚乙烯部分的载体上形成沉淀物的条件下操作。然后可以通过将溶剂/非溶剂混合物重复置换到柱中以溶解聚乙烯部分，从分馏塔中回收聚乙烯部分。溶剂和非溶剂的相对浓度基于聚乙烯母体聚合物的溶剂梯度分布。

22. 发明授权

US5410071A Process for sulfur-containing derivatives of hydroxyphenylbenzotriazoles 失效
标题翻译：羟苯基苯并三唑的含硫衍生物的方法
公开(公告)号：US5410071A
公开(公告)日：1995-04-25
申请号：US197905
申请日：1994-02-17
申请人： Paul J. DesLauriers , Paritosh K. Das , Darryl R. Fahey
发明人： Paul J. DesLauriers , Paritosh K. Das , Darryl R. Fahey
IPC分类号： C07D249/20 , C08G75/02 , C08G85/00 , C08K5/378
CPC分类号： C08K5/378 , C07D249/20 , C08G75/0204 , C08G85/00
摘要： A composition that, when present in a polymer matrix, reduces the deleterious effect of UV light absorption by the polymer is provided, which comprises a sulfur-containing derivative of hydroxyphenylbenzotriazole having the formula of: ##STR1## wherein each X is selected from the group consisting of hydrogen, halogens, cyano, alkyl, phenyl group, biphenyl group, arylthio, amine, ketone, aldehyde, alkoxy, hydroxy, carboxylic acid group, oligomer and combinations thereof and can have carbon atoms up to about 20; n is a whole number from 1 to 5; n' is a whole number from 0 to 4; n" is a whole number from 1 to 2 and each n" can be the same or different; q is an integer from 1 to 10; each Y is selected from the group consisting of --S(O)(O)--, --S(O)--, and --S--; each R can be selected from the group consisting of hydrogen, alkyl group, alkenyl group, aralkyl group, alkaryl group, and combinations thereof and can have 0 to about 10 carbon atoms; each OH group can be at either the 2'- or the 6'-position, or both. Also provided are a composition comprising the sulfur-containing derivative, a process for preparing the derivative, a composition comprising a polymer chemically bonded to the derivative, and a process for preparing the composition which comprises a polymer chemically bonded to the derivative.
摘要翻译：当存在于聚合物基质中时，提供降低由聚合物引起的UV光吸收的有害影响的组合物，其包含具有下式的羟基苯基苯并三唑的含硫衍生物：其中每个X选自由氢，卤素，氰基，烷基，苯基，联苯基，芳硫基，胺，酮，醛，烷氧基，羟基，羧酸基，低聚物及其组合组成，可以具有高达约20的碳原子; n为1〜5的整数; n'是从0到4的整数; n“是从1到2的整数，并且每个n”可以相同或不同; q是1至10的整数; 每个Y选自-S（O）（O） - ， - S（O） - 和-S-; 每个R可以选自氢，烷基，烯基，芳烷基，烷芳基及其组合，并且可以具有0至约10个碳原子; 每个OH基团可以在2'-或6'-位，或两者。还提供了包含含硫衍生物的组合物，制备衍生物的方法，包含与衍生物化学键合的聚合物的组合物，以及包含与衍生物化学键合的聚合物的组合物的方法。

23. 发明授权

US5221534A Health and beauty aid compositions 失效
标题翻译：健康美容助剂
公开(公告)号：US5221534A
公开(公告)日：1993-06-22
申请号：US649196
申请日：1991-02-04
申请人： Paul J. DesLauriers , William J. Heilman
发明人： Paul J. DesLauriers , William J. Heilman
IPC分类号： A61K8/72 , A61K8/00 , A61K8/02 , A61K8/31 , A61K8/37 , A61K8/81 , A61K8/89 , A61K8/891 , A61K8/90 , A61K8/92 , A61K31/74 , A61K47/06 , A61K47/32 , A61Q15/00 , A61Q17/04 , A61Q19/00 , C08F297/02 , C08F297/04
CPC分类号： A61K8/042 , A61K47/06 , A61K47/32 , A61K8/90 , A61K9/0014 , A61Q13/00 , A61Q15/00 , A61Q17/04 , A61Q19/00
摘要： Health and beauty aid compositions comprise one or more health and beauty aid components contained in a gel comprising a mineral oil containing from blends of di- and triblock copolymers based on synthetic thermoplastic rubbers.
摘要翻译：健康和美容助剂组合物包含一种或多种包含在凝胶中的健康和美容助剂组分，其包含矿物油，其含有基于合成热塑性橡胶的二嵌段共聚物和三嵌段共聚物。

24. 发明授权

US08492498B2 Polymer compositions for rotational molding applications 有权
标题翻译：用于旋转成型应用的聚合物组合物
公开(公告)号：US08492498B2
公开(公告)日：2013-07-23
申请号：US13031451
申请日：2011-02-21
申请人： Richard M. Buck , Albert P. Masino , Qing Yang , Paul J. DesLauriers , Steven J. Secora , Elizabeth M. Lanier , Guylaine St. Jean , Jon D. Ratzlaff , Christopher E. Wittner
发明人： Richard M. Buck , Albert P. Masino , Qing Yang , Paul J. DesLauriers , Steven J. Secora , Elizabeth M. Lanier , Guylaine St. Jean , Jon D. Ratzlaff , Christopher E. Wittner
IPC分类号： C08L23/08 , C08F210/16
CPC分类号： C08L23/0815 , B29C41/003 , B29C41/04 , C08F4/6592 , C08L2205/025 , C08L2207/062 , C08L2308/00 , C08L2314/06 , C08L2666/06 , C08F110/02 , C08F2500/04 , C08F2500/09 , C08F4/65904
摘要： A polymer having a density of from about 0.94 g/cm3 to about 0.96 g/cm3 and a primary structure parameter 2 (PSP2 value) of greater than about 8.5, wherein an article formed from the polymer has an environmental stress crack resistance of equal to or greater than about 1000 hours when measured in accordance with ASTM D 1693 condition A. A polymer having at least one lower molecular weight component and at least one higher molecular weight component and having a PSP2 value of equal to or greater than about 8.5, wherein an article formed from the polymer has an environmental stress crack resistance of greater than about 1000 hours when measured in accordance with ASTM D 1693 condition A.
摘要翻译：密度为约0.94g / cm 3至约0.96g / cm 3，一次结构参数2（PSP2值）大于约8.5的聚合物，其中由聚合物形成的制品具有等于或根据ASTM D1693条件A测量时大于约1000小时。具有至少一种较低分子量组分和至少一种较高分子量组分并且PSP2值等于或大于约8.5的聚合物，其中根据ASTM D 1693条件A测量时，由聚合物形成的制品具有大于约1000小时的环境应力抗裂性。

25. 发明授权

US07056744B2 Measurement of short chain branching in olefin copolymers using chemometric analysis 有权
标题翻译：使用化学计量分析测量烯烃共聚物中的短链支化
公开(公告)号：US07056744B2
公开(公告)日：2006-06-06
申请号：US10463849
申请日：2003-06-16
申请人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
发明人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
IPC分类号： G01N33/44 , G01N21/00
CPC分类号： G01N21/359 , G01N21/3577 , G01N2021/3595 , Y10T436/21
摘要： A method of determining the proportion of short-chain branching in an olefin copolymer process stream is disclosed. The short-chain branching may also be determined as a function of molecular weight in a sample having a range of molecular weights. In the method, at least two olefin copolymer training samples are provided. The respective samples have different, known proportions of short-chain branching. The infrared (e.g. FT-IR) absorbance spectra of the training samples in a wavenumber range are obtained. Calibration information is determined from the training samples by chemometrically correlating the differences in the infrared absorbance spectra of the training samples to the differences in the degree of short-chain branching in the training samples. This step generates calibration information that allows the degree of short-chain branching in a sample to be determined once its infrared absorbance spectrum is obtained. A method for determining the statistical error in the measurement of short-chain branching in an olefin polymer sample as a function of its molecular weight distribution is also disclosed.
摘要翻译：公开了一种确定烯烃共聚物工艺流中短链支化比例的方法。短链支化也可以在具有分子量范围的样品中作为分子量的函数来确定。在该方法中，提供至少两种烯烃共聚物训练样品。各样品具有不同的已知比例的短链支化。获得波数范围内训练样本的红外（例如FT-IR）吸收光谱。通过化学方法将训练样本的红外吸收光谱的差异与训练样本中短链分支程度的差异化学相关，从训练样本中确定校准信息。该步骤产生校准信息，其允许在获得样品的红链吸收光谱后测定样品中的短链支化度。还公开了用于确定烯烃聚合物样品中短链支化的测量中的统计误差作为其分子量分布的函数的方法。

26. 发明授权

US06632680B1 Measurement of short chain branching in olefin copolymers using chemometric analysis 有权
标题翻译：使用化学计量分析测量烯烃共聚物中的短链支化
公开(公告)号：US06632680B1
公开(公告)日：2003-10-14
申请号：US09667657
申请日：2000-09-22
申请人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
发明人： Paul J. DesLauriers , David C. Rohlfing , Alan D. Eastman , Eric T. Hsieh
IPC分类号： G01N3344
CPC分类号： G01N21/359 , G01N21/3577 , G01N2021/3595 , Y10T436/21
摘要： A method of determining the proportion of short-chain branching in an olefin copolymer process stream is disclosed. The short-chain branching may also be determined as a function of molecular weight in a sample having a range of molecular weights. In the method, at least two olefin copolymer training samples are provided. The respective samples have different, known proportions of short-chain branching. The infrared (e.g. FT-IR) absorbance spectra of the training samples in a wavenumber range are obtained. Calibration information is determined from the training samples by chemometrically correlating the differences in the infrared absorbance spectra of the training samples to the differences in the degree of short-chain branching in the training samples. This step generates calibration information that allows the degree of short-chain branching in a sample to be determined once its infrared absorbance spectrum is obtained. A method for determining the statistical error in the measurement of short-chain branching in an olefin polymer sample as a function of its molecular weight distribution is also disclosed.
摘要翻译：公开了一种确定烯烃共聚物工艺流中短链支化比例的方法。短链支化也可以在具有分子量范围的样品中作为分子量的函数来确定。在该方法中，提供至少两种烯烃共聚物训练样品。各样品具有不同的已知比例的短链支化。获得波数范围内训练样本的红外（例如FT-IR）吸收光谱。通过化学方法将训练样本的红外吸收光谱的差异与训练样本中短链分支程度的差异化学相关，从训练样本中确定校准信息。该步骤产生校准信息，其允许在获得样品的红链吸收光谱后测定样品中的短链支化度。还公开了用于确定烯烃聚合物样品中短链支化测量中的统计误差作为其分子量分布函数的方法。

27. 发明授权

US06355359B1 Polyethylene film 有权
标题翻译：聚乙烯薄膜
公开(公告)号：US06355359B1
公开(公告)日：2002-03-12
申请号：US09702908
申请日：2000-10-31
申请人： Ashish M. Sukhadia , William R. Coutant , Jim D. Byers , Louis Moore, Jr. , M. Bruce Welch , Syriac J. Palackal , Kiplin D. Cowan , David C. Rohlfing , Jay Janzen , Paul J. DesLauriers , William M. Whitte
发明人： Ashish M. Sukhadia , William R. Coutant , Jim D. Byers , Louis Moore, Jr. , M. Bruce Welch , Syriac J. Palackal , Kiplin D. Cowan , David C. Rohlfing , Jay Janzen , Paul J. DesLauriers , William M. Whitte
IPC分类号： C08F11002
CPC分类号： B32B27/32 , B32B7/02 , B32B27/08 , B32B2323/04 , C08F10/02 , C08F110/02 , C08F210/16 , C08J5/18 , C08J2323/04 , C08L15/02 , C08L23/0815 , C08L27/12 , C08L2314/04 , C08L2314/06 , Y10T428/3154 , Y10T428/31544 , Y10T428/31913 , Y10T428/31938 , C08L2666/04 , C08L2666/08 , C08F2500/12 , C08F2500/03 , C08F2500/14 , C08F2500/10 , C08F210/08 , C08F210/14
摘要： A self supporting film having one or more layers wherein at least one layer has a percent haze of less than 17.8 and the polymer of that layer consists essentially of a polyethylene having a density of at least 0.925 grams per cc, a molecular weight distribution of no more than 4, optionally containing a fluoroelastomer, and methods for making such film are disclosed.
摘要翻译：具有一层或多层的自支撑膜，其中至少一层具有小于17.8的雾度百分比，并且该层的聚合物基本上由密度为至少0.925克/厘米3的聚乙烯组成，分子量分布为无大于4，任选地含有含氟弹性体，并且公开了制备这种膜的方法。

28. 发明授权

US5446227A Co-production of an alkenyl aromatic compound or precursor thereof and an oxygenated sulfur-containing compound 失效
标题翻译：联合生产烯基芳族化合物或其前体和含氧化合物
公开(公告)号：US5446227A
公开(公告)日：1995-08-29
申请号：US128498
申请日：1993-09-07
申请人： Paul J. DesLauriers , Michael S. Matson
发明人： Paul J. DesLauriers , Michael S. Matson
IPC分类号： C07C1/20 , C07C15/40 , C07C315/02 , C07C409/08 , C07C1/00
CPC分类号： C07C409/08 , C07C1/20 , C07C15/40 , C07C315/02 , C07C407/00
摘要： A process for co-production of an alkenyl aromatic compound such as, for example, styrene and t-butylstyrene, and an oxygenated sulfur-containing compound such as, for example, a sulfoxide or a sulfone is disclosed which comprises: (1) contacting, in the presence or absence of a catalyst, an .alpha.-methyl benzylic hydroperoxide with an organic sulfide compound to produce a mixture of an .alpha.-methyl benzylic hydroxide and an oxygenated sulfur-containing compound; (2) separating the .alpha.-methyl benzylic hydroxide from the sulfur-containing compound; (3) contacting the .alpha.-methyl benzylic hydroxide with a base to convert the .alpha.-methyl benzylic hydroxide to the alkenyl aromatic compound; and optionally, (4) recovering the alkenyl aromatic compound from the oxygenated sulfur-containing compound. The sulfoxide produced can be oxidized to a sulfone. The contacting of the .alpha.-methyl benzylic hydroxide with a base can also be carried out before the .alpha.-methyl benzylic hydroxide is separated from the oxygenated sulfur-containing compound followed by separation of the sulfur-containing compound.
摘要翻译：公开了一种共同制备链烯基芳族化合物如苯乙烯和叔丁基苯乙烯的方法和含氧化的含硫化合物，例如亚砜或砜，其包括：（1）接触在存在或不存在催化剂的情况下，将α-甲基苄基氢过氧化物与有机硫化物混合以产生α-甲基苄基氢氧化物和含氧的含硫化合物的混合物; （2）从含硫化合物中分离α-甲基苄基氢氧化物; （3）使α-甲基苄基氢氧化物与碱反应以将α-甲基苄基氢氧化物转化为链烯基芳族化合物; 和（4）从含氧化合物中回收链烯基芳族化合物。所生成的亚砜可以被氧化成砜。 α-甲基苄基氢氧化物与碱的接触也可以在将α-甲基苄基氢氧化物与含氧的含硫化合物分离，然后分离含硫化合物之前进行。

29. 发明授权

US5438115A Process for preparing poly(arylene sulfide) polymers 失效
标题翻译：制备聚（亚芳基硫醚）聚合物的方法
公开(公告)号：US5438115A
公开(公告)日：1995-08-01
申请号：US159411
申请日：1993-11-30
申请人： Darryl R. Fahey , Owen H. Decker , Carlton E. Ash , Jon F. Geibel , Fernando C. Vidaurri, Jr. , Lacey E. Scoggins , Harvey D. Hensley , Wei-Teh W. Shang , Jimmie J. Straw , Paul J. DesLauriers
发明人： Darryl R. Fahey , Owen H. Decker , Carlton E. Ash , Jon F. Geibel , Fernando C. Vidaurri, Jr. , Lacey E. Scoggins , Harvey D. Hensley , Wei-Teh W. Shang , Jimmie J. Straw , Paul J. DesLauriers
IPC分类号： C08G75/02 , C08G75/14
CPC分类号： C08G75/0259
摘要： A process is provided for producing a poly(arylene sulfide) polymer which employs at least one base as a reactant, wherein the base is contacted with the polymerization reaction mixture incrementally during the polymerization.
摘要翻译：提供一种制备使用至少一种碱作为反应物的聚（亚芳基硫醚）聚合物的方法，其中在聚合过程中碱与聚合反应混合物逐渐接触。

30. 发明授权

US4945017A Rust conversion composition 失效
标题翻译：锈转化成分
公开(公告)号：US4945017A
公开(公告)日：1990-07-31
申请号：US320842
申请日：1989-03-03
申请人： Paul J. DesLauriers , William J. Heilman
发明人： Paul J. DesLauriers , William J. Heilman
IPC分类号： C09D4/00 , C23C22/50
CPC分类号： C23C22/50 , C09D4/00
摘要： A composition for conversion of a rusted metal surface to form a durable coating thereon consists essentially of a reducing agent which reduces an trivalent iron present on the surface, an organic monomer to which is capable of polymerization on the surface in the presence of the reducing agent and a free radical initiator which polymerizes the organic monomer to form the durable coating.
摘要翻译：用于转化生锈的金属表面以形成耐久涂层的组合物基本上由还原剂组成，其还原存在于表面上的三价铁，在还原剂存在下能够在表面上聚合的有机单体以及使有机单体聚合以形成耐久涂层的自由基引发剂。

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