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21. 发明授权

US4912281A Conversion of methanol and methyl ether to light olefins with ZSM-45 in presence of hydrogen 失效
标题翻译：在氢存在下，用ZSM-45将甲醇和甲醚转化成轻质烯烃
公开(公告)号：US4912281A
公开(公告)日：1990-03-27
申请号：US296405
申请日：1989-01-09
申请人： Margaret M. Wu
发明人： Margaret M. Wu
IPC分类号： B01J29/70 , C07C1/20
CPC分类号： C07C1/20 , B01J29/70 , B01J2229/20 , C07C2529/70 , Y02P20/582 , Y02P30/42
摘要： A process is disclosed for converting a methanol and/or methyl ether-containing reactant feed along with a hydrogen-containing gaseous diluent to a light olefin-containing product over a ZSM-45 aluminosiloicate zeolite based catalyst composition. By using such ZSM-45 zeolite catalysts, methanol and/or methyl ether can be advantageously converted to an olefin-containing hydrocarbon product enriched in C.sub.2 to C.sub.4 olefins. The hydrogen-containing gaseous diluent is co-fed to the conversion reaction zone and the conversion reaction is conducted at a pressure of at least about 3 atmospheres in order to enhance catalyst lifetime.
摘要翻译：公开了一种用于将含甲醇和/或甲基醚的反应物原料与含氢气体稀释剂一起通过ZSM-45铝硅酸盐沸石基催化剂组合物转化成含轻烯烃的产物的方法。通过使用这种ZSM-45沸石催化剂，甲醇和/或甲基醚可以有利地转化为富含C2至C4烯烃的含烯烃的烃产物。将含氢气态稀释剂共同进料至转化反应区，转化反应在至少约3个大气压的压力下进行，以增加催化剂寿命。

22. 发明授权

US4423272A Regeneration of methanol/methyl ether conversion catalysts 失效
公开(公告)号：US4423272A
公开(公告)日：1983-12-27
申请号：US335797
申请日：1981-12-30
申请人： Nancy P. Forbus , Margaret M. Wu
发明人： Nancy P. Forbus , Margaret M. Wu
IPC分类号： B01J29/50 , B01J29/70 , B01J29/90 , B01J38/10 , C07C1/20 , C07C1/24 , B01J29/38
CPC分类号： B01J29/06 , B01J29/70 , B01J29/90 , C07C1/20 , B01J29/50 , B01J38/10 , C07C2529/50 , C07C2529/70 , Y02P20/584
摘要： A process for using hydrogen-containing gas to regenerate a zeolite catalyst comprising at least some crystalline aluminosilicate zeolitic material having pore windows formed by 8-membered rings of oxygen atoms, e.g., ZSM-34, which has been used to promote conversion of methanol and/or methyl ether to light olefins. Contact of such catalysts with hydrogen-containing gas such as hydrogen or synthesis gas at particular regeneration temperatures and pressures can restore the activity of such catalysts either in the presence or absence of organic reactants without forming potentially catalyst-damaging by-products such as water.

23. 发明授权

US09701595B2 Process for producing novel synthetic basestocks 有权
公开(公告)号：US09701595B2
公开(公告)日：2017-07-11
申请号：US13732840
申请日：2013-01-02
申请人： Margaret M. Wu , Steven P. Rucker , Jo Ann M. Canich
发明人： Margaret M. Wu , Steven P. Rucker , Jo Ann M. Canich
IPC分类号： C07C5/03 , C07C2/30 , C08F10/00 , C08F10/14 , C10G50/02 , C10M107/08 , C10M107/10 , C10M111/04 , C08F4/659 , C08F4/6592
CPC分类号： C07C2/30 , C07C5/03 , C08F4/65916 , C08F4/6592 , C08F4/65927 , C08F10/00 , C08F10/14 , C10G50/02 , C10G2300/1088 , C10G2300/302 , C10G2300/304 , C10G2300/703 , C10G2400/10 , C10G2400/22 , C10M107/08 , C10M107/10 , C10M111/04 , C10M2205/0265 , C10M2205/0285 , C10N2220/02 , C10N2220/021 , C10N2220/022 , C10N2220/023 , C10N2220/024 , C10N2220/033 , C10N2270/00 , C08F4/65908 , C08F4/64048
摘要： This disclosure relates to a liquid syndiotactic polyalphaolefin, sPAO, comprising one or more C4 to C24 monomers, said sPAO having: a) an rr triad content of 5 to 50% as measured by 13C NMR; b) an mr triad content of 25 to 60% as measured by 13C NMR, where the mr to mm triad ratio is at least 1.0; c) a pour point of Z° C. or less, where Z=0.0648X−51.2, where X=kinematic viscosity at 100° C. as reported in centistokes (cSt); d) a kinematic viscosity at 100° C. of 100 cSt or more (alternatively 200 cSt or more); e) a ratio of mr triads to rr triad (as determined by 13C NMR) of less than 9; f) a ratio of vinylidene to 1,2-disubstituted olefins (as determined by 1H NMR) of less than 8; g) a viscosity index of 120 or more; and h) an Mn of 40,000 or less. This disclosure further relates to processes to make and use sPAOs, including those having any combination of characterics a) to h).

24. 发明申请

US20140323665A1 Polyalphaolefins by Oligomerization and Isomerization 审中-公开
标题翻译：聚α-烯烃通过低聚和异构化
公开(公告)号：US20140323665A1
公开(公告)日：2014-10-30
申请号：US14001990
申请日：2012-02-28
申请人： Margaret M. Wu , Bernie J. Pafford , Kevin B. Stavens
发明人： Margaret M. Wu , Bernie J. Pafford , Kevin B. Stavens
IPC分类号： C08F4/76
CPC分类号： C08F4/76 , B01J21/08 , B01J23/755 , B01J29/7461 , B01J29/7492 , C10G45/60 , C10G50/00 , C10G69/126 , C10G2300/1088 , C10G2300/302 , C10G2300/304 , C10G2400/22 , C10M107/10 , C10M177/00 , C10M2205/0285 , C10N2220/022 , C10N2220/023 , C10N2230/02 , C10N2230/54 , C10N2240/04 , C10N2240/08 , C10N2240/10 , C10N2260/02 , C10N2270/00
摘要： A feedstock of one or more C4 to C24 alpha olefins is oligomerized with a metallocene catalyst system to form a polyalphaolefin product mixture. At least a portion of the polyalphaolefin product mixture is then isomerized in the presence of an acid catalyst to form an isomerized polyalphaolefin. The polyalphaolefin may also by hydrogenated, either simultaneously with isomerization or afterwards. The resulting polyalphaolefin has a kinematic viscosity at 100° C. of between 1 cSt and 20 cSt and reduced pour point in comparison to the pre-isomerized product.
摘要翻译：一种或多种C 4至C 24α-烯烃的原料用茂金属催化剂体系低聚以形成聚α-烯烃产物混合物。然后将至少一部分聚α-烯烃产物混合物在酸催化剂存在下异构化以形成异构化的聚α烯烃。聚α-烯烃也可以通过氢化，同时异构化或之后。得到的聚α-烯烃在100℃下的运动粘度在1cSt和20cSt之间，与预异构化产物相比具有降低的倾点。

25. 发明申请

US20100292424A1 Lubricants from Mixed Alpha-Olefin Feeds 有权
标题翻译：混合α-烯烃饲料的润滑剂
公开(公告)号：US20100292424A1
公开(公告)日：2010-11-18
申请号：US11995297
申请日：2006-07-14
申请人： Margaret M. Wu , Norman Yang , Phil Surana , Anura Patil , Steven P. Rucker , Kuangnan Qian , Shakeel Tirmizi , Mark P. Hagemeister
发明人： Margaret M. Wu , Norman Yang , Phil Surana , Anura Patil , Steven P. Rucker , Kuangnan Qian , Shakeel Tirmizi , Mark P. Hagemeister
IPC分类号： C08F4/76 , C08F210/00 , C08F210/04 , C08F210/14 , C07C2/02
CPC分类号： C10M107/10 , C08F4/65908 , C08F4/65912 , C08F210/00 , C08F210/14 , C08F210/16 , C10G50/02 , C10M2205/0285 , C10N2220/021 , C10N2220/022 , C10N2230/02 , C08F4/65927 , C08F2500/03 , C08F2500/17 , C08F210/08
摘要： This invention discloses an improved process which employs mixed alpha-olefins as feed over activated metallocene catalyst systems to provide essentially random liquid polymers particularly useful in lubricant components or as functional fluids.
摘要翻译：本发明公开了一种改进的方法，其使用混合的α-烯烃作为进料活化的茂金属催化剂体系，以提供特别可用于润滑剂组分或作为功能流体的基本上无规的液体聚合物。

26. 发明申请

US20090093657A1 Process for preparing poly alpha olefins and lubricant basestocks from fischer-tropsch liquids 有权
标题翻译：从费 - 托液体制备聚α烯烃和润滑剂基础油料的方法
公开(公告)号：US20090093657A1
公开(公告)日：2009-04-09
申请号：US11973281
申请日：2007-10-05
申请人： John S. Buchanan , Margaret M. Wu , Lorenzo DeCaul
发明人： John S. Buchanan , Margaret M. Wu , Lorenzo DeCaul
IPC分类号： C07C7/00 , C07C1/00
CPC分类号： C10G57/02 , C10G2/32 , C10G69/06 , C10G69/126 , C10M107/10 , C10M2205/0285 , C10M2205/173 , C10N2220/022 , C10N2230/02
摘要： A process for preparing poly alpha olefins from a Fisher-Tropsch product. The process comprising the steps of contacting a C5-C18 fraction of an alpha-olefinic hydrocarbon mixture produced from thermal cracking a C16-C40 Fisher-Tropsch product with an oligomerization catalyst under conditions to produce an oligomerized product; and fractionating the oligomerized product to obtain a fractionated product having an average carbon number greater than 30. A process for preparing lubricant base stocks from a Fisher-Tropsch product is also provided.
摘要翻译：从费 - 托产品制备聚α-烯烃的方法。该方法包括以下步骤：将C16-C40 Fisher-Tropsch产物的热裂解产生的α-烯烃混合物的C5-C18馏分与低聚催化剂在条件下接触以产生低聚产物; 并对低聚产物进行分级以获得平均碳数大于30的分级产物。还提供了由费托产品制备润滑剂基料的方法。

27. 发明申请

US20090043049A1 Plasticized Polyolefin Compositions 审中-公开
标题翻译：增塑聚烯烃组合物
公开(公告)号：US20090043049A1
公开(公告)日：2009-02-12
申请号：US12139738
申请日：2008-06-16
申请人： Bryan R. Chapman , Margaret M. Wu , Wen Li , Mun Fu Tse
发明人： Bryan R. Chapman , Margaret M. Wu , Wen Li , Mun Fu Tse
IPC分类号： C08L23/06 , C08L23/12
CPC分类号： C08L23/02 , C08L23/04 , C08L23/10 , C08L2205/02 , C08L2314/06 , C08L2666/04 , C08L2666/06
摘要： The present invention relates to a polyolefin composition that includes 60 to 99 wt % of one or more polyolefin polymers and 1 to 40 wt % of a regularly branched PAO (“rbPAO”) based on the total weight of the polyolefin polymer(s) and the rbPAO, wherein the rbPAO includes oligomers of one or more C2 to C20 alpha-olefins having a kinematic viscosity at 100° C. (“KV100° C.”) of 3 to 3000 cSt, a Branching Irregularity Index (“BII”) of 0.40 or less, a molar-average carbon number (“CLAO”) of 6 to 14, and a Mw/Mn of less than 2.3.
摘要翻译：本发明涉及一种聚烯烃组合物，其包含60至99重量％的一种或多种聚烯烃聚合物和1至40重量％的基于聚烯烃聚合物总重量的规则支化PAO（“rbPAO”）和 rbPAO，其中rbPAO包括具有3至3000cSt的运动粘度（“KV100℃”）的一种或多种C2至C20α-烯烃的低聚物，分支不规则指数（“BII”）为0.40以下，摩尔平均碳数（“CLAO”）为6〜14，Mw / Mn小于2.3。

28. 发明授权

US5691281A Well fluids based on low viscosity synthetic hydrocarbons 失效
标题翻译：基于低粘度合成烃的井液
公开(公告)号：US5691281A
公开(公告)日：1997-11-25
申请号：US321006
申请日：1994-10-06
申请人： Henry Ashjian , Suzzy C. Ho , Margaret M. Wu
发明人： Henry Ashjian , Suzzy C. Ho , Margaret M. Wu
IPC分类号： C07C5/25 , C09K8/34 , C09K7/02 , C09K7/06
CPC分类号： C09K8/34 , C07C5/2518 , C07C2529/06
摘要： Solid, waxy 1-olefins may be converted to low viscosity liquid products by carrying out a double bond isomerization in the presence of a solid acidic catalyst such as an acidic clay or a zeolite under mild conditions. The olefin isomer products are useful in the formulation of well fluids such as drilling muds, especially useful in offshore drilling. The preferred oils for making up the well fluids are formulated with a hydrocarbon oil blend of the low viscosity olefin isomer together with a C.sub.12 to C.sub.18 paraffinic hydrocarbon of petroleum origin and a C.sub.10 to C.sub.32 olefin such as tetradecene-1. The fluids exhibit good biodegradability and are non-toxic to marine organisms; they also meet viscosity and pour points specifications for formulation into oil based muds.
摘要翻译：固体蜡状1-烯烃可以在温和条件下在固体酸性催化剂如酸性粘土或沸石的存在下进行双键异构化而转化为低粘度液体产物。烯烃异构体产物可用于诸如钻井泥浆的井液制备，特别适用于海上钻井。用于制备井液的优选油用低粘度烯烃异构体的烃油共混物与石油来源的C 12至C 18链烷烃和诸如十四碳烯-1的C 10至C 32烯烃一起配制。液体表现出良好的生物降解性，对海洋生物无毒; 它们也符合粘度和倾点规格，用于配制成油基泥浆。

29. 发明授权

US5136118A High VI synthetic lubricants from cracked refined wax 失效
标题翻译：来自裂化精制蜡的高VI合成润滑剂
公开(公告)号：US5136118A
公开(公告)日：1992-08-04
申请号：US571347
申请日：1990-08-23
申请人： J. Scott Buchanan , Margaret M. Wu
发明人： J. Scott Buchanan , Margaret M. Wu
IPC分类号： C10M107/02
CPC分类号： C10M107/02 , C10M2205/00 , C10M2205/02 , C10N2220/02
摘要： A process is disclosed for the production of synthetic hydrocarbon lubricants having high viscosity index by oligomerizing a mixture of alpha-olefins comprising the reaction product from the thermal cracking of refined wax. The oligomerization is carried out with Lewis acid catalyst or reduced chromium oxide on porous support.
摘要翻译：公开了一种通过使包含来自精制蜡的热裂解的反应产物的α-烯烃的混合物低聚而生产具有高粘度指数的合成烃类润滑剂的方法。低聚反应用多孔载体上的路易斯酸催化剂或还原的氧化铬进行。

30. 发明授权

US4996384A Regeneration of reduced metal oxide oligomerization catalyst 失效
标题翻译：还原金属氧化物低聚催化剂的再生
公开(公告)号：US4996384A
公开(公告)日：1991-02-26
申请号：US481279
申请日：1990-02-20
申请人： Bruce P. Pelrine , Margaret M. Wu
发明人： Bruce P. Pelrine , Margaret M. Wu
IPC分类号： B01J23/92 , B01J38/12 , C07C2/10
CPC分类号： B01J23/92 , B01J38/12 , C07C2/10 , C07C2521/08 , C07C2523/26 , Y02P20/584
摘要： A process for producing oligomers from alpha-olefins, such as 1-decene, in which the olefins are oligomerized over a supported, reduced metal oxide catalyst from Group VIB of the Periodic Table to give oligomers with a branch ratio of less than 0.19. The catalyst, preferably a chromium/silica catalyst the catalyst can be regenerated to allow repeated recycling of the catalyst without a loss in yield of the oligomer product. The regeneration process comprises: (i) purging or stripping the deactivated catalyst with inert gas at elevated temperature to strip unreacted olefin and oligomer product from the catalyst; (ii) contacting the deactivated and purged catalyst with a stream of oxidizing gas while heating to elevated temperature to oxidize the metal component of the catalyst and remove carbonaceous deposits from the catalyst; (iii) cooling the oxidized catalyst and contacting it with a stream of reducing gas to reduce the metal component of the oxidized catalyst to a lower valence state. The oligomerization may be carried out at relatively high temperatures of about 90.degree. to 250.degree. C. to produce liquid lubricant products of high viscosity index, typically above 130, or at lower temperatures from about -20.degree. to about +90.degree. C. to product products of higher molecular weight which may be used as lubricant additives, e.g. VI improvers. The high molecular weight products are generally characterized by a branch ratio less than 0.19, a weight average molecular weight from about 15,000 to 200,000, a number average molecular weight from about 5,000 to about 50,000 and a molecular weight distribution from about 1 to about 5. They are also shear stable under high temperature, high shear rate conditions of 150.degree. C. and a shear rate of 10.sup.6 second.sup.-1.
摘要翻译：从α-烯烃如1-癸烯制备低聚物的方法，其中烯烃在负载型还原的金属氧化物催化剂上从元素周期表VIB中低聚，得到分支比小于0.19的低聚物。催化剂，优选铬/二氧化硅催化剂，催化剂可以被再生以允许催化剂的反复循环而不会使低聚物产物的产率降低。再生方法包括：（i）在升高的温度下用惰性气体吹扫或汽提失活的催化剂，以从催化剂中除去未反应的烯烃和低聚物产物; （ii）在加热至高温以使氧化催化剂的金属组分并从催化剂中除去含碳沉积物的同时使失活和净化的催化剂与氧化气体流接触; （iii）冷却氧化的催化剂并将其与还原气体流接触，以将氧化催化剂的金属组分降至更低的化合价态。低聚反应可以在约90℃至250℃的相对高的温度下进行，以产生高粘度指数（通常在130以上）或在约-20℃至约+90℃的较低温度至可用作润滑剂添加剂的较高分子量的产品，例如 VI改进剂高分子量产物通常的特征在于分支比小于0.19，重均分子量为约15,000至200,000，数均分子量为约5,000至约50,000，分子量分布为约1至约5。它们在150℃的高温，高剪切速率条件和106秒-1的剪切速率下也剪切稳定。

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