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21. 发明专利

JPH0463812A COPOLYMER HAVING AZOMETHINE GROUP IN SIDE CHAIN 失效
公开(公告)号：JPH0463812A
公开(公告)日：1992-02-28
申请号：JP17455990
申请日：1990-07-03
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： OHASHI TOYOJI , KOJIMA TAKASHI , ITSUBO AKIRA
IPC分类号： C08F220/16 , C08F20/34 , C08F220/10 , C08F220/36
摘要： PURPOSE:To provide the title copolymer suitable as a high-molecular material for various devices used in the optoelectronic fields by preparing a copolymer comprising two specific repeating units and having a specified number-average mol.wt. CONSTITUTION:The title copolymer comprises 5-70mol% repeating units of formula I (wherein R is H or CH3; and R is CH3 or C2H5) and 95-30mol% repeating units of formula II [wherein R is H or CH3; X is 1-20; and A is an electron-accepting group (e.g. NO2, CN)] and has a number-average mol.wt. of 1000-1000000. The copolymer is suitable as a high-molecular material for various devices, e.g. an electro-optic device, a second-harmonic generator, a piezoelectric device, a waveguide, and esp. a film device and a laminate or aggregate device, in the optoelectronic fields such as optical information processing or optical communication.

22. 发明专利

JPS61254390A OPTICAL RECORDING MEDIUM 失效
公开(公告)号：JPS61254390A
公开(公告)日：1986-11-12
申请号：JP9558985
申请日：1985-05-07
申请人： KOBAYASHI HIDEKAZU , MITSUBISHI PETROCHEMICAL CO
发明人： KOBAYASHI HIDEKAZU , OHASHI TOYOJI , MIYABAYASHI MITSUTAKA
IPC分类号： B41M5/26 , G03C1/72 , G11B7/244 , G11B7/245
摘要： PURPOSE:To contrive higher recording sensitivity, higher recording density, higher S/N and non-toxic property, by using an addition polymer of a diethynylbenzene derivative and a benzenedithiol derivative which polymer has a specified group as a recurring unit in an optical recording layer. CONSTITUTION:An addition polymer of a diethynylbenzene derivative and a benzenedithiol derivative which polymer has a group of formula (I) as a recurring unit (aromatic vinylene sulfide polymer) is used as an optical recording layer. The optical recording material is produced by providing a thin film of the aromatic vinylene sulfide polymer on a base, which may be a transparent plastic base, an inorganic material base or the like. The polymer can be synthesized by addition polymerication of compounds of formula (II) and (III). Information is recorded by externally applying energy to the optical recording layer to induce a crystalline-amorphous phase transition, and is reproduced by utilizing the difference in light reflectance or light absorbance between the crystalline phase and the amorphous phase.

23. 发明专利

JPH06279637A COLORED RESIN COMPOSITION 失效
公开(公告)号：JPH06279637A
公开(公告)日：1994-10-04
申请号：JP6796393
申请日：1993-03-26
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： OHASHI TOYOJI , OOYA YUKAKO , ISHIBASHI TOSHIAKI
IPC分类号： C08F8/06 , C08L25/04 , C08L67/00 , C08L67/02
摘要： PURPOSE:To obtain the subject composition having finely and homogeneously dispersed coloring agent and free from surface property deterioration of resin composition by reacting a specific polymer reaction product and a styrene polymer with a thermoplast ic polyester. CONSTITUTION:The objective composition is obtained by compounding (A) a styrene polymer constituting a matrix phase, (B) a thermoplastic polyester constituting a dispersion phase with (C) a polymer reaction product obtained by reacting (i) a styrene polymer having a hydroxyl group at the end of molecular chain with (ii) a thermoplastic polyester having a carboxyl group at the end of molecular chain and containing essentially all amount of coloring agent in composition B.

24. 发明专利

JPH06279635A COLORED RESIN COMPOSITION 失效
公开(公告)号：JPH06279635A
公开(公告)日：1994-10-04
申请号：JP6796193
申请日：1993-03-26
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： OHASHI TOYOJI , OOYA YUKAKO , ISHIBASHI TOSHIAKI
IPC分类号： C08L25/04 , C08G59/32 , C08L63/00 , C08L67/00 , C08L67/02
摘要： PURPOSE:To obtain the subject composition excellent in color homogeneity and protective effect for surface property deterioration and useful for coating, etc., by compounding a styrene polymer, a thermoplastic polyester and a specific polymerization product with a coloring agent contained in a dispersing phase. CONSTITUTION:The objective composition is obtained by heat-melting and kneading (A) styrene polymer constituting a matrix phase, (B) thermoplastic polyester constituting a dispersion phase, (C) polymer reaction product obtained by reacting styrene polymer having an epoxy group with thermoplastic polyester containing a carboxyl group at the end of molecular chain, whose equivalents of epoxy group and carboxy group preferably become identical with each other at the end of reaction and (D) a coloring agent (preferably having larger affinity with component B and smaller particle size than dispersion phase particles, e.g. carbon black and Ferroin yellow). Preferable addition ratios are as follows: component A/component B=55/45-95/5; the amounts of component C and component D based on 100 pts.wt. of the total of component A and component B are respectively 1-20 pts.wt. and 0.5-15 pts.wt.

25. 发明专利

JPH06212092A PRODUCTION OF PHTHALOCYANINE-TYPE PHOTO-CONDUCTIVE COMPOSITION 失效
公开(公告)号：JPH06212092A
公开(公告)日：1994-08-02
申请号：JP654093
申请日：1993-01-19
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： KOBAYASHI MARIKO , OHASHI TOYOJI , SHIGEMATSU YASUYUKI
IPC分类号： C09B47/04 , C09B67/50 , G03G5/06
摘要： PURPOSE:To obtain the subject composition useful for photosensitive material, etc., giving a high-quality image having sharp edge by stirring phthalocyanine and a phthalocyanine derivative substituted with a specific number of electron- attracting groups in the presence of an organic solvent under application of external mechanical force. CONSTITUTION:The objective composition is capable of outputting a digital signal by inputting analog light as well as digital light, usable as a photosensitive material for digital-recording electrophotography and gives a high-quality image having sharp edge even by using in a photosensitive material for receiving analog light. The composition can be produced by stirring (A) phthalocyanine and (B) a phthalocyanine derivative having halogen atoms or electron-attracting groups substituting the benzene nucleus of the phthalocyanine molecule (e.g. tetranitro-nonmetallic phthalocyanine) in the presence of an organic solvent excluding aromatic organic solvent under application of external mechanical force for >=30min. The ratio of the number of the halogen atoms or the electronattracting groups to the total number of phthalocyanine units of the phthalocyanine and the phthalocyanine derivative is 0.001-0.5.

26. 发明专利

JPH06212090A PHTHALOCYANINE-TYPE PHOTO-CONDUCTIVE COMPOSITION 失效
公开(公告)号：JPH06212090A
公开(公告)日：1994-08-02
申请号：JP653893
申请日：1993-01-19
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： KOBAYASHI MARIKO , OHASHI TOYOJI , SHIGEMATSU YASUYUKI
IPC分类号： C09B47/04 , C09B67/50 , G03G5/06
摘要： PURPOSE:To obtain the subject composition digitally reactive with input light and, accordingly, useful as a sensitive material for digital recording electrophotography by mixing three specific kinds of phthalocyanine derivatives at specific ratios and subjecting the mixture to milling treatment under specific condition. CONSTITUTION:The objective composition is produced by mixing (A) 100 pts.wt. of a compound of formula I (M is H, atom or compound capable of forming covalent bond or coordinate bond with phthalocyanine) with (B) 0.01-5 pts.wt. of a compound of formula II (R to R are H, halogen or nitro and at least one of R to R is not H) and (C) 0.01-10 pts.wt. of a compound of formula III (R to R are H, halogen or electron-attracting group and at least four of R to R are not H) and subjecting the obtained mixture to milling treatment in the presence of an organic solvent excluding aromatic solvent. This composition is produced generally by producing phthalocyanines using a phthalocyanine ring-forming compound and the above raw material compound substituted with halogen or nitro and milling the obtained mixture of the components A and B together with the component C.

27. 发明专利

JPH063844A IMAGE FORMING METHOD 失效
公开(公告)号：JPH063844A
公开(公告)日：1994-01-14
申请号：JP16292692
申请日：1992-06-22
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： OHASHI TOYOJI , KOBAYASHI MARIKO , ITSUBO AKIRA
IPC分类号： C09B67/50 , G03G5/06 , G03G15/04
摘要： PURPOSE:To form a spot-like picture image with high sharpness by spot exposing a photosensitive body to an exposure beam according to digital signals. CONSTITUTION:The photosensitive body 11 consists of a phthalocyanine compsn. prepared by mixing phthalocyanine and phthalocyanine deriv. in an acid which dissolves phthalocyanine, and then precipitating in water or a poor solvent. The phthalocyanine deriv. is obtd. by substituting electron-withdrawing groups for the benzen nucleus of phthalocyanine molecule, and the phthalocyanine and phthalocyanine deriv. are mixed with such a proportion that the number of electron-withdrawing groups is between =0.001 to the total phthalocyanine unit of the phthalocyanine and phthalocyanine deriv. The picture image is formed by electrifying (12) the photosensitive material 11 with positive charges, spot exposing (13) the photosensitive material to beams according to digital signals, and then developing (14).

28. 发明专利

JPH0570702A PRODUCTION OF PHTHALOCYANINE COMPOSITION 失效
公开(公告)号：JPH0570702A
公开(公告)日：1993-03-23
申请号：JP26127791
申请日：1991-09-13
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： OHASHI TOYOJI , ISHIBASHI TOSHIAKI , GODA JUNKO , ITSUBO AKIRA , KOYAMA TOSHIYUKI , OZAWA MASATOMI , IIJIMA KATSUTOSHI
IPC分类号： C09B47/06
摘要： PURPOSE:To provide a phthalocyanine composition for use as a digital optical input photoreceptor in electrophotography by mixing to specific phthalocyanine compounds and mixing the mixture with another specific phthalocyanine derivative. CONSTITUTION:100 pts.wt. phthalic anhydride is mixed with 0.001-5 pts.wt. phthalic anhydride having an electron-attracting group (e.g., nitro group), 15-40 pts.wt. metal halide, 100-200 pts.wt. nitrogen donor (e.g., urea), and l-3 pts.wt. catalyst (e.g., ammonium molybdate). This mixture is heated in a solvent (e.g., nitrobenzene) at 180-250 deg.C for 3-8hr. The resulting hot mixture is filtered and the reaction product is purified by treating it with an acid and an alkali, thereby to obtain a mixture (a) of phthalocyanine compounds respectively represented by formulae 3 and 4 (wherein M is H, Cu, etc., and r to R each is H or an electron-attracting group). 0.01-10 pts.wt. phthalocyanine derivative represented by formula 5 (wherein M is H, CU, etc., and R to R each is H or an electron- attracting group) (e.g., a tetranitrophthalocyanine) is added to 100 pts.wt. mixture (a). The resulting mixture is dissolved in an acid (e.g., methanesulfonic acid) and reprecipitated by dilution with water thereby to obtain a phthalocyanine composition.

29. 发明专利

JPH0463815A COPOLYMER HAVING AZOMETHINE GROUP IN SIDE CHAIN 失效
公开(公告)号：JPH0463815A
公开(公告)日：1992-02-28
申请号：JP17455690
申请日：1990-07-03
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： OHASHI TOYOJI , KOJIMA TAKASHI , ITSUBO AKIRA
IPC分类号： C08F220/36 , C08F20/34
摘要： PURPOSE:To provide the title copolymer suitable as a high-molecular material for various devices used in the optoelectronic fields by preparing a copolymer having azomethine groups in the side chains and a specified number--average mol.wt. CONSTITUTION:The title copolymer comprises repeating units of the formula [wherein R is H or CH3; X is 1-20; and A is an electron-accepting group (e.g. NO2, CN)] and has a number-average mol.wt. of 1000-1000000. The copolymer is suitable as a high-molecular material for various devices, e.g. an electro-optic device, a second-harmonic generator, a piezoelectric device, a waveguide, and esp. a film device and a laminate or aggregate device, in the optoelectronic fields such as optical information processing or optical communication.

30. 发明专利

JPH0368926A NONLINEAR OPTICAL ELEMENT 失效
公开(公告)号：JPH0368926A
公开(公告)日：1991-03-25
申请号：JP20373089
申请日：1989-08-08
申请人： MITSUBISHI PETROCHEMICAL CO
发明人： TOKURA YOSHINORI , OHASHI TOYOJI , KOJIMA TAKASHI , ITSUBO AKIRA , TODA HIDEO
IPC分类号： G02F1/35 , C07C47/263 , C07C47/267 , C07C47/27 , C07C47/277 , C07C223/06 , C07C245/06 , C07C255/17 , C07D213/50 , C09K9/02 , G02F1/355 , G02F1/361
摘要： PURPOSE:To obtain the optical element having a large nonlinear optical effect without having inversion symmetry by using the marondialdehyde compd. expressed by prescribed formula. CONSTITUTION:The nonlinear optical element consisting of the marondialdehyde compd. expressed by the formula. In the formula, R is H or the substituent selected from 1 to 20C aliphat. group such as alkyl group, haloalkyl group, hydroxyalkyl group, arylalkyl group and alkoxy group, cyclic group such as cycloalkyl group and cycloalkenyl group, arom. groups such as aryl group, aryloxy group and arylthio group, acyl group such as alkanoil group and aroyl group, alkyl amino group and dialkyl amino group substd. with 1 to 6C alkyl group, aryl amino group substd. with 6 to 8C aryl group, azo group of arom. azo derivatives or halogen atom. The arom. group, pyridyl group and cyclohexyl group having or without having the substituent are more preferable particularly as the substituent R. This material has no inversion symmetry in a bulk state and has the absorption max. on a short wavelength side and the large nonlinear optical characteristic of the molecule.

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