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21. 发明授权

US07858692B2 Two component coating compositions and coatings produced therefrom 有权
标题翻译：双组分涂料组合物和由其制备的涂料
公开(公告)号：US07858692B2
公开(公告)日：2010-12-28
申请号：US10617585
申请日：2003-07-11
申请人： Donald Albert Paquet, Jr. , Robert John Barsotti , Laura Ann Lewin , Carl Brent Douglas , Michael Charles Grady
发明人： Donald Albert Paquet, Jr. , Robert John Barsotti , Laura Ann Lewin , Carl Brent Douglas , Michael Charles Grady
IPC分类号： C08G18/42 , C08G18/08 , C08L83/00 , C08L51/00 , C08C19/00 , C08F290/06 , C08F220/06 , C08F283/00 , C08F8/30
CPC分类号： C08K5/0025 , C08F2/001 , C08F2/06 , C08F8/30 , C08F2800/20 , C08G18/6229 , C08G18/792 , C08L79/00 , C08L2312/00 , C09D133/04 , C09D133/14 , C08L33/06 , C08L2666/20 , C08F2220/1866
摘要： The present invention is directed to two component coating compositions that cure under ambient conditions and more particularly to those having low VOC (volatile organic content) that are suitable for use in automotive refinish and Original Equipment Manufacturing (OEM) applications. The coating composition includes crosslinkable and crosslinking components, wherein the crosslinkable component includes a low polydispersity, low molecular weight copolymer having on an average 2 to 25 functional groups, such as hydroxyl, carboxyl, acetoacetoxy, primary and secondary amine, and epoxy. The copolymer is polymerized from a monomer mixture that includes one or more non-functional acrylate monomers and one or more functional methacrylate monomers provided with the functional groups. The crosslinking component includes polyisocyanate, polyamine, ketimine, melamine, epoxy, polyacid or a combination thereof. The invention is also directed to coating produced from the coating composition.
摘要翻译：本发明涉及在环境条件下固化的二组分涂料组合物，更具体地涉及适用于汽车修补漆和原始设备制造（OEM）应用的具有低VOC（挥发性有机物含量）的组分涂料组合物。涂料组合物包括可交联和交联组分，其中可交联组分包括具有平均2至25个官能团的低分子量低分子量共聚物，例如羟基，羧基，乙酰乙酰氧基，伯胺和仲胺和环氧基。共聚物由包括一种或多种非官能丙烯酸酯单体和一个或多个配有官能团的官能甲基丙烯酸酯单体的单体混合物聚合。交联组分包括多异氰酸酯，多胺，酮亚胺，三聚氰胺，环氧树脂，多元酸或它们的组合。本发明还涉及由涂料组合物制备的涂料。

22. 发明授权

US09206448B2 Extraction solvents derived from oil for alcohol removal in extractive fermentation 有权
标题翻译：萃取溶剂中的萃取溶剂，用于萃取发酵中的酒精去除
公开(公告)号：US09206448B2
公开(公告)日：2015-12-08
申请号：US13162828
申请日：2011-06-17
申请人： Douglas Robert Anton , Jelena Cirakovic , Bruce A. Diner , Michael Charles Grady , Francis J. Woerner
发明人： Douglas Robert Anton , Jelena Cirakovic , Bruce A. Diner , Michael Charles Grady , Francis J. Woerner
IPC分类号： C12P1/00 , C12N9/00 , C12N15/00 , C12N1/14 , C07H21/04 , C12P7/16 , B01D3/00 , B01D21/26 , C07C29/86 , C11B1/02 , C11B13/00 , C12M1/00 , C12P7/64 , C12P7/18
CPC分类号： C12P7/16 , A23K10/38 , B01D3/002 , B01D11/0492 , B01D21/26 , B01D21/262 , C07C29/86 , C11B1/025 , C11B13/00 , C12F3/10 , C12M1/00 , C12M21/12 , C12M45/04 , C12M45/09 , C12N1/14 , C12N15/00 , C12P7/18 , C12P7/6418 , Y02E50/10 , Y02E50/16 , Y02E50/17 , Y02W30/74
摘要： In an alcohol fermentation process, oil derived from biomass is chemically converted into an extractant available for in situ removal of a product alcohol such as butanol from a fermentation broth. The glycerides in the oil can be chemically converted into a reaction product, such as fatty acids, fatty alcohols, fatty amides, fatty acid methyl esters, fatty acid glycol esters, and hydroxylated triglycerides, and mixtures thereof, which forms a fermentation product extractant having a partition coefficient for a product alcohol greater than a partition coefficient of the oil of the biomass for the product alcohol. Oil derived from a feedstock of an alcohol fermentation process can be chemically converting into the fermentation product extractant. The oil can be separated from the feedstock prior to the feedstock being fed to a fermentation vessel, and the separated oil can be chemically converted to a fermentation product extractant, which can then contacted with a fermentation product comprising a product alcohol, whereby the product alcohol is separated from the fermentation product.
摘要翻译：在酒精发酵过程中，将来自生物质的油化学转化成可从发酵液中原位除去产物醇如丁醇的萃取剂。油中的甘油酯可以化学转化成反应产物，例如脂肪酸，脂肪醇，脂肪酰胺，脂肪酸甲酯，脂肪酸二醇酯和羟基化甘油三酸酯及其混合物，其形成发酵产物提取剂，其具有产物醇的分配系数大于产物醇的生物质油的分配系数。来自醇发酵方法的原料的油可以化学转化成发酵产物萃取剂。在将原料进料到发酵容器之前，油可以与原料分离，并且将分离的油化学转化成发酵产物萃取剂，然后可将其与包含产物醇的发酵产物接触，由此产物醇与发酵产物分离。

23. 发明授权

US08828695B2 Method for producing butanol using two-phase extractive fermentation 有权
标题翻译：使用两相萃取发酵生产丁醇的方法
公开(公告)号：US08828695B2
公开(公告)日：2014-09-09
申请号：US12759283
申请日：2010-04-13
申请人： Michael Charles Grady , Mehmedalija Jahic , Ranjan Patnaik
发明人： Michael Charles Grady , Mehmedalija Jahic , Ranjan Patnaik
IPC分类号： C12P7/16 , C12P1/00
CPC分类号： C12P7/16 , Y02E50/10
摘要： A method of making butanol from at least one fermentable carbon source that overcomes the issues of toxicity resulting in an increase in the effective titer, the effective rate, and the effective yield of butanol production by fermentation utilizing a recombinant microbial host wherein the butanol is extracted into specific organic extractants during fermentation.
摘要翻译：一种从至少一种可发酵碳源制造丁醇的方法，其克服了毒性问题，导致通过使用重组微生物宿主发酵的丁醇生产的有效滴度，有效速率和有效产率提高，其中提取丁醇在发酵过程中变成特定的有机萃取剂。

24. 发明申请

US20100261851A1 Recoverable polymer-bound homogeneous catalysts for catalytic chain transfer process 失效
标题翻译：用于催化链转移过程的可回收聚合物结合的均相催化剂
公开(公告)号：US20100261851A1
公开(公告)日：2010-10-14
申请号：US11505270
申请日：2006-08-16
申请人： Henry Edward Bryndza , Michael Charles Grady , Sigridur Soley Kristjansdottir , Christina M. Older , Matthew Arthur Page , Joachim C. Ritter , Wilson Tam
发明人： Henry Edward Bryndza , Michael Charles Grady , Sigridur Soley Kristjansdottir , Christina M. Older , Matthew Arthur Page , Joachim C. Ritter , Wilson Tam
IPC分类号： C08F4/42 , C08F110/00 , C08F120/06 , C08F120/10 , C08F120/56 , C08F120/44 , C08F112/08 , C08F130/08 , C08F114/06 , C08F8/42
CPC分类号： C08F220/18 , C08F2/38 , C08F4/00 , Y10S526/904
摘要： Disclosed herein are novel polymer-tethered ligands, metal complexes comprising these ligands, and the use of these complexes as chain transfer catalysts to control the molecular weight of oligomeric and polymeric materials produced in a radical polymerization process. The materials made by the processes disclosed herein have significantly reduced color, making them suitable for a wide range of color-critical end-uses, including automotive coatings.
摘要翻译：本文公开了新型聚合物 - 束缚配体，包含这些配体的金属络合物，以及这些络合物用作链转移催化剂以控制在自由基聚合方法中生产的低聚物和聚合物材料的分子量的用途。通过本文公开的方法制备的材料具有显着降低的颜色，使得它们适用于广泛的颜色关键性终端用途，包括汽车涂料。

25. 发明申请

US20110288345A1 RECOVERY OF BUTANOL FROM A MIXTURE OF BUTANOL, WATER, AND AN ORGANIC EXTRACTANT 有权
标题翻译：丁醇从丁醇，水和有机提取物的混合物中恢复
公开(公告)号：US20110288345A1
公开(公告)日：2011-11-24
申请号：US12949154
申请日：2010-11-18
申请人： Michael Charles Grady , William D. Parten , Bruce Vrana , Yihui Tom Xu
发明人： Michael Charles Grady , William D. Parten , Bruce Vrana , Yihui Tom Xu
IPC分类号： C07C29/94
CPC分类号： C12P7/16 , C07C29/80 , Y02E50/10 , C07C31/12
摘要： A process for recovering butanol from a mixture comprising a water-immiscible organic extractant, water, butanol, and optionally a non-condensable gas, is provided. The butanol is selected from 1-butanol, 2-butanol, isobutanol, and mixtures thereof. The extractant comprises at least one solvent selected from the group consisting of C7 to C22 fatty alcohols, C7 to C22 fatty acids, esters of C7 to C22 fatty acids, C7 to C22 fatty aldehydes, and mixtures thereof.
摘要翻译：提供了一种从包含与水不混溶的有机萃取剂，水，丁醇和任选的不可冷凝气体的混合物中回收丁醇的方法。丁醇选自1-丁醇，2-丁醇，异丁醇及其混合物。萃取剂包含至少一种选自C7至C22脂肪醇，C7至C22脂肪酸，C7至C22脂肪酸酯，C7至C22脂肪醛及其混合物的溶剂。

26. 发明授权

US08030422B2 Recoverable polymer-bound homogeneous catalysts for catalytic chain transfer process 失效
标题翻译：用于催化链转移过程的可回收聚合物结合的均相催化剂
公开(公告)号：US08030422B2
公开(公告)日：2011-10-04
申请号：US11505270
申请日：2006-08-16
申请人： Henry Edward Brynzda , Michael Charles Grady , Sigridur Soley Kristjansdottir , Christina M. Older , Matthew Arthur Page , Joachim C. Ritter , Wilson Tam
发明人： Henry Edward Brynzda , Michael Charles Grady , Sigridur Soley Kristjansdottir , Christina M. Older , Matthew Arthur Page , Joachim C. Ritter , Wilson Tam
IPC分类号： C08F4/60 , C07F4/70 , C08F4/80
CPC分类号： C08F220/18 , C08F2/38 , C08F4/00 , Y10S526/904
摘要： Disclosed herein are novel polymer-tethered ligands, metal complexes comprising these ligands, and the use of these complexes as chain transfer catalysts to control the molecular weight of oligomeric and polymeric materials produced in a radical polymerization process. The materials made by the processes disclosed herein have significantly reduced color, making them suitable for a wide range of color-critical end-uses, including automotive coatings.
摘要翻译：本文公开了新型聚合物 - 束缚配体，包含这些配体的金属络合物，以及这些络合物用作链转移催化剂以控制在自由基聚合方法中生产的低聚物和聚合物材料的分子量的用途。通过本文公开的方法制备的材料具有显着降低的颜色，使得它们适用于广泛的颜色关键性终端用途，包括汽车涂料。

27. 发明申请

US20090305370A1 METHOD FOR PRODUCING BUTANOL USING TWO-PHASE EXTRACTIVE FERMENTATION 审中-公开
标题翻译：使用两相萃取发酵生产丁醇的方法
公开(公告)号：US20090305370A1
公开(公告)日：2009-12-10
申请号：US12478389
申请日：2009-06-04
申请人： Michael Charles Grady , Mehmedalija Jahic , Ranjan Patnaik
发明人： Michael Charles Grady , Mehmedalija Jahic , Ranjan Patnaik
IPC分类号： C12P7/16 , C07C29/74
CPC分类号： C12P7/16 , Y02E50/10
摘要： A method of making butanol from at least one fermentable carbon source that overcomes the issues of toxicity resulting in an increase in the effective titer, the effective rate, and the effective yield of butanol production by fermentation utilizing a recombinant microbial host wherein the butanol is extracted into specific organic extractants during fermentation
摘要翻译：一种从至少一种可发酵碳源制造丁醇的方法，其克服了毒性问题，导致通过使用重组微生物宿主发酵的丁醇生产的有效滴度，有效速率和有效产率提高，其中提取丁醇在发酵过程中变成特定的有机萃取剂

28. 发明授权

US07585924B2 Pressurized high temperature polymerization process and polymerization system used therein 有权
标题翻译：其中使用的加压高温聚合方法和聚合体系
公开(公告)号：US07585924B2
公开(公告)日：2009-09-08
申请号：US10617270
申请日：2003-07-10
申请人： Michael Charles Grady
发明人： Michael Charles Grady
IPC分类号： C09D133/00
CPC分类号： C08K5/0025 , C08F2/001 , C08F2/06 , C08F8/30 , C08F2800/20 , C08G18/6229 , C08G18/792 , C08L79/00 , C08L2312/00 , C09D133/04 , C09D133/14 , C08L33/06 , C08L2666/20 , C08F2220/1866
摘要： The present invention is directed to a novel high temperature polymerization process operating at high pressures for producing a polymer. The process includes conveying hybrid reactor mixtures, which include one or more hybrid reactor monomers and one or more hybrid reactor initiators to one or more hybrid reactors. The hybrid reactors are maintained at effective hybrid polymerization temperatures and sub-reflux polymerization gage pressures to cause polymerization of a portion of the hybrid reactor monomers into the polymer. The process further includes conveying hybrid reactor contents from the hybrid reactors to one or more batch reactors maintained at effective batch polymerization temperatures and reflux polymerization pressures to cause polymerization of a remaining portion of the hybrid reactor monomers into the polymer. The hybrid reactors are smaller in volume than the batch reactors. By utilizing the hybrid/batch reactor combination, the process of the present invention can be operated under safe working conditions. The process of the present invention also allows control of the polydispersity and molecular weight of the resulting polymers. As a result, the polymers made therefrom can be used as binders in compositions, such as coating compositions used in the automotive refinish and OEM applications having desired coating properties. The present invention is also directed to a polymerization system used in the process of the present invention.
摘要翻译：本发明涉及在高压下操作以生产聚合物的新型高温聚合方法。该方法包括将混合反应器混合物输送到一个或多个混合反应器，混合反应器混合物包括一个或多个混合反应器单体和一个或多个混合反应器引发将混合反应器保持在有效的杂化聚合温度和亚回流聚合计压力下，以使一部分混合反应器单体聚合成聚合物。该方法还包括将混合反应器内容物从混合反应器输送到保持在有效分批聚合温度和回流聚合压力下的一个或多个间歇反应器，以使剩余部分的混合反应器单体聚合成聚合物。混合反应器的体积比间歇反应器小。通过利用混合/间歇反应器组合，本发明的方法可以在安全的工作条件下操作。本发明的方法还可以控制得到的聚合物的多分散性和分子量。结果，由其制成的聚合物可用作组合物中的粘合剂，例如用于汽车修补漆的涂料组合物和具有所需涂料性能的OEM应用。本发明还涉及用于本发明方法的聚合体系。

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